胶体

With increasing the concentration of the mixture of antimony oxide from 10 % to 20 %, the reaction time decreases from 90 min to about 30 min, but the optimized range of molar ratio of H3PO4 to antimony increases. The reaction temperature is not the main factor on particle size with the existence of H3PO4, the average particle size is c.a. 160nm without obviously variety in the temperature range from 60 °C to 90°C.

氧化锑混合物浓度从10%增加到20%时，反应达到平衡的时间从90min下降到30min左右，形成小粒径胶粒所需磷酸与锑摩尔比的最佳范围也随之上升；在稳定剂磷酸存在的条件下，温度不再是对胶体粒子粒径的主要影响因素，在60～90℃之间，形成的胶体五氧化二锑的粒径无明显变化，在160nm左右。

It was concluded that no aging time was the most beneficial to form colloid, when molar ratio of phosphoric acid to antimony was in the range from 0.8 to 1.0 and 1.0 to 1.3, the particle sizes of sol with the concentration of 10 % and 15 % antimony pentoxide by weight are both smaller, and with the molar ratio of 1.0, the average particle sizes are (36±5.6)nm nm and (164±32)nm respectively.

结果表明：氧化锑混合物不进行陈化对胶体五氧化二锑的形成最有利；磷酸与锑的摩尔比分别为0.8～1.0和1.0～1.3时，10%和15%的胶体五氧化二锑胶粒粒径较小，当摩尔比为1.0时，粒径分别为(36±5.6)nm和(164±32)nm。

The preparation of colloidal antimony pentoxide has been investigated during recent years, but most of colloidal dispersions of antimony pentoxide are quite complicated, costly and unstable because of the problem caused by preparing methods or dispersion medium.

近年来，虽然已有一些胶体五氧化二锑的研制工作，但由于制备方法、分散介质和添加剂的不同，一些胶体五氧化二锑体系比较复杂、成本较高和不稳定。

Nanoparticles encapsulating PPA HCl were prepared using the solid jelly pulverization technique. The size of the PPA HCl - hydrogel nanoparticles was assessed using a LS particle size analyzer and scanning electron microscopy. The rheological properties of suspensions are characterized by Cone and Plate Viscometer. In addition, any drug-polymer interactions were assessed using a differential scanning calorimeter.

奈米微粒包覆PPA HCl是以固态凝胶研磨技术来完成，负载PPA HCl之亲水胶体奈米微粒以雷射粒径分析仪与扫瞄式电子显微镜来检测其粒子大小，悬液之流体特性是以Cone and Plate黏度计来评估，此外，药物与胶体聚合物间之交互作用则是以热卡式分析仪来检视。

Nanoparticles encapsulating PPA HCl were prepared using the solid jelly pulverization technique. The size of the PPA HCl – hydrogel nanoparticles was assessed using a LS particle size analyzer and scanning electron microscopy. The rheological properties of suspensions are characterized by Cone and Plate Viscometer.

奈米微粒包覆PPA HCl是以固态凝胶研磨技术来完成，负载PPA HCl之亲水胶体奈米微粒以雷射粒径分析仪与扫瞄式电子显微镜来检测其粒子大小，悬液之流体特性是以Cone and Plate黏度计来评估，此外，药物与胶体聚合物间之交互作用则是以热卡式分析仪来检视。

Two new methods about preparation of nano-inorganic coated polymer microsphere have been found. The research mainly focused on controlled precipitation of inorganic precurdors onto the polymer microspheres, technique of preparation and size distribution of transition metal oxides and sulfides emulsion particles, nano-paticles''surface modification and the HLB values adjustment, emulsification of oil-soluble monomer in inorganic colloid and emulsion stability, emulsion polymerization that inorganic particles act as medi-phase, the preparation of inorganic nano-particle/polymer hybrid microspheres, preparation of hybrid materials in inverse emulsion, inverse emulsion polymerization of acrylamide and its phase behavior. Inorganic nano-particles we studied concerning TiO2、SiO2、Fe3O4、ZnO、ZnS、Ag and black carbon. Also we studied the morphology and capability of the hybrid materials.

主要内容有：无机物在高分子乳胶模板体系的界面定位沉积研究；过渡金属氧化物、硫化物纳米胶体粒子的制备工艺与胶粒尺寸分布研究；纳米粒子的表面修饰及其亲水亲油平衡值的调制；油溶性单体在无机胶体中的乳化行为与乳液稳定性研究；以无机纳米粒子做中介相的乳液聚合与无机纳米粒子/高分子复合微球制备研究；反相体系中杂化材料的制备；丙烯酰胺水溶液反相乳液聚合、相行为与稳定性；丙烯酰胺反相体系中无机粒子的制备研究；涉及到TiO2、SiO2、Fe3O4、ZnO、ZnS、Ag、碳黑等纳米无机物，系统考察了相关材料的形态与性能，为其应用开发奠定了基础。

Two array fashions, hexagonal and square arrays of the colloids were observed by SEM images.

同时在所制备的胶体晶体中观察到了四方排列和六方排列两种排列方式，分析了这两种排列的转化主要是受温度和胶体晶体中缺陷的影响。

The CD54 colloid gold particles were labeled on the cell surface or projections of tumor cell membrane in each 2 cases of SCC and BCC; and in one case of SCC, CD54 colloid gold particles were also detected on tonofilament desmosome complex.

在3例鳞癌和3例基癌中，各 2例癌细胞表面及突起处观察到CD54胶体金颗粒的存在；其中1例鳞癌张力微丝-桥粒复合体处还可见CD54胶体金颗粒分布。

Then, we prepare His-Pxa2pC2-HA by the same way, but dialyse with Triton-X 100 to increase its solubility and skip nicole's column purification step. We analysed the molecular size of this His-Pxa2pC2-HA protein by FPLC.

接著，以同样的方式表现His-Pxa2pC2-HA蛋白，并在透析时加入Triton-X 100，再以胶体过滤层析法分析，发现Triton-X 100会干扰胶体过滤层析法的分析。

Different size of the colloidal gold particle was prepared by reducing the gold chloride with sodium citrate heated by microwave oven.

采用柠檬酸三钠还原氯金酸法，用微波炉加热，制备了不同粒径的胶体金，以17.5nm左右的胶体金标记抗克百威多克隆抗体的显色效果较好。

The concept of equivalent rotationally rigidity is offered and the formula of rotationally rigidity is obtained.

主要做了如下几个方面的工作：对伸臂位于顶部的单层框架—筒体模型进行分析，提出了等效转动约束的概念和转动约束刚度的表达式。

Male cats normally do not need aftercare with the exception of the night after the anesthetic.

男猫通常不需要善后除了晚上的麻醉。