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聚酰胺

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Polyamic acidsolution were synthesized from pyromellitic dianhydrideand 4,4"-diaminodiphenylusing solution polycondensation with N,N"-dimethylacetamideas a solvent.

采用均苯四甲酸酐和4,4'-二氨基二苯醚作为单体,合成聚酰亚胺的前驱体聚酰胺酸。

Surface-treated aluminum hydroxide and magnesium hydroxide mixture, linear low density polyethylene and polyethylene grafted by maleic anhydride were melt-kneaded and extruded to produce a flame-retardant masterbatch, and then was extruded with polyamide 6(PA6) to yield PA6/SAMH/PE(50/30/20 by mass ratios)ternary composite.

采用表面处理过的氢氧化铝与氢氧化镁混合物(质量比2:1)、线型低密度聚乙烯、马来酸酐接枝聚乙烯共混挤出制成母料,然后与聚酰胺6(PA6)共混挤出即母料法制备了PA6/SAMH/PE三元复合材料。

The sebacic acid is a kind of important organic chemical material which can be widely used to produce the polyamide plastics, high temperature lubricant, cold plasticizer, resin and so on.

癸二酸是一种重要的有机化工原料,广泛应用于生产聚酰胺工程塑料、耐高温润滑油、耐寒增塑剂、树脂等方面。

Methods:(1) Silica column chromatography and LH-20 were used in phytochemistry study.(2) Based on the extraction ratio of arctiin, the best extraction procedure was acheived under the direction of L9(34) orthogonal experimental design. From 10 types of resins, the one with the maximal binding ability for Arctii was selected and silica-column choramatograpy was used in its seperation and purification procedure.(3) The animal diabetic experimental model in Wistar rats was established with streptozotocin and many biochemical factors were used to indicate the pharmacological effects of arctiin, including glycosylated hemoglobin, serum creatinine, seralbumin, monoxide nitrogen, glycerin trilaurate, cholesterol, HDL-ch, LDL-ch, Blood urea nitrogen, creatinine, SOD, ET, MDA, total Urine protein and albuminuria.

(1)采用硅胶柱层析、聚酰胺层析、LH-20等方法对牛蒡子的化学成分进行研究;(2)采用正交实验设计方法,以牛蒡子苷为指标,确定了牛蒡子乙醇回流提取的最佳工艺;对10种类型大孔吸附树脂进行筛选,筛选出对牛蒡子苷吸附效果最佳的树脂;采用硅胶柱层析法,对牛蒡子苷进一步分离纯化;(3)建立实验性糖尿病大鼠模型,以GLU、TC、TG、HDL-ch、LDL-ch、TB、ALB、BUN、CREA、GHbAlc、NO、SOD、ET、MDA和尿液中TB、ALB为指标,研究牛蒡子苷药理活性;(4)以差速消化法纯化Wistar大鼠的主动脉内皮细胞并进行传代培养,测定牛蒡子苷对高糖条件下RAECs活性、RAECs释放LDH、MDA和NO的变化以及RAECs表达内皮型一氧化氮合酶表达的影响。

Methods The determination was carried out over a Symmetry C18 column at 25℃. Methods tetrahydrofuran: 0.2% citric acid (14∶1∶85) was used as mobile phase at a velocity of 1 ml.min-1 and the detection wavelength was set at 360nm. ResultsRutin was found in SFE extract of Sparganium Stoloniferum.

方法在聚酰胺膜上点样,以80%乙醇作为展开剂鉴别芦丁,采用Symmetry C18色谱柱,以乙腈-四氢呋喃-0.2%枸橼酸(14∶1∶85)为流动相,柱温25℃,在流速为1.0 ml.min-1,360 nm的检测波长下,测定芦丁含量。

Methods tetrahydrofuran: 0.2% citric acid (14∶1∶85) was used as mobile phase at a velocity of 1 ml·min-1 and the detection wavelength was set at 360nm. ResultsRutin was found in SFE extract of Sparganium Stoloniferum.

方法在聚酰胺膜上点样,以80%乙醇作为展开剂鉴别芦丁,采用Symmetry C18色谱柱,以乙腈-四氢呋喃-0.2%枸橼酸(14∶1∶85)为流动相,柱温25℃,在流速为1.0 ml·min-1,360 nm的检测波长下,测定芦丁含量。

The coated gloss right from the start of the resin natural resins, to nitrocellulose, styryl, chloroethylene, polyamic, sour, polyurethane, acrylic resin, a wide variety of resin application ever.

涂布光油所用的树脂从一开始的天然树脂,到硝化棉、苯乙烯、氯乙烯、聚酰胺、酸、聚氨酯、丙烯酸树脂等,各种各样的树脂都得到了应用。

The negatively charged sulfonic acid groups was readily introduced through the reaction of the terminal anhydride groups of the anhydride-terminated hyperbranched poly precursor with the amino groups of sulfanilic acid before chemical imidization.

研究表明,在聚合过程的聚酰胺酸阶段,采用过量的邻苯二甲酸酐或苯胺对超支化聚酰亚胺的端氨基或端酸酐基团进行的封端改性切实可行,改性反应可进行地相当彻底。

The results demonstrate that this novel polyamide has an obvious liquid crystalline behavior when being heated into molten state, and is a typical kind of thermotropic liquid crystal.

结果表明,该聚酰胺在熔融状态下具有明显的液晶态结构,属于典型的主链型热致液

Although it is certain that the flower of Trollius chinensis is a good antibacterial medicine, there are no studies on its effective substances and quality standard.The 60% ethanol elution through polymide was determined as antibacterial and antivirus portion according to pharmacological study. The chemical experiment isolated 18 compounds and identified 13 structures.

本课题通过对金莲花提取物的药效学试验,确立了聚酰胺60%乙醇洗脱部位为其抗菌、抗病毒有效部位;继而对该部位进行了化学研究,分离出单体化合物18个,鉴定化学结构13个,其中有7个是从金莲花中首次发现的新化合物,有4个是从金莲花属植物首次分离得到,所分离的化合物大部分是黄酮类,还有有机酸等。

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