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Ray the average degree of polymerization of bamboo cellulose was determined by viscosimetry method and the crystalline structure were studied by infrared spectra and X ray diffraction respectively .

采用60Coγ射线对高聚合度的造纸用竹纤维素浆粕进行辐照处理,用铜氨溶液法测定辐照前后竹纤维素浆粕的平均聚合度,并采用红外光谱法及X射线衍射法研究其结晶结构的变化。

After irradiation by~(60)Co γ-ray,the average degree of polymerization of bamboo cellulose was determined by viscosimetry method,and the crystalline structure were studied by infrared spectra and X-ray diffraction,respectively.

采用60Coγ射线对高聚合度的造纸用竹纤维素浆粕进行辐照处理,用铜氨溶液法测定辐照前后竹纤维素浆粕的平均聚合度,并采用红外光谱法及X射线衍射法研究其结晶结构的变化。

While all the phenyl groups in tetraphenylphenyl groups or benzophenanthrene groups are not coplanar. At the same time, by density function theory, the electronic energy gap between HOMO and LUMO frontier molecular orbitals of condensed aromatics are calculated and the Eg of acenaphthenyl groups in C_2 gum is the smallest, which explains the reason why C_2 gum has the best radiation protection effects.

利用甲基三氯硅烷和溴苯的格氏反应合成了甲基苯基二氯硅烷,用核磁分析证实了格氏反应中高沸点副产物为甲基二苯基氯硅烷;通过甲基苯基二氯硅烷和二甲基二氯硅烷的共水解,再裂解而制得含Me_2SiO链节的甲基苯基环硅氧烷混合物,进而利用碱胶开环聚合得到甲基苯基硅橡胶生胶;也可通过甲基苯基二氯硅烷水解所得甲基苯基环硅氧烷D_3~(3Ph、D_4~(4Ph_)与D_4开环聚合制得甲基苯基硅橡胶生胶。

The coagulant has high rate of the turbidity when the pH value of the solution is 8~9, the dosage(Fe3+) is 2~5 mg/L and alkalization of PFS is 7%~14% in flocculating experiment by PFS made for the flotation waste water.

用制备的PFS进行絮凝实验,在处理选矿废水时,当溶液的pH值在8~9之间,投加量为2~5mg/L(以Fe3+计)时,聚合度在7%~14%之间时,聚合硫酸铁对废水浊度去除有较好的效果。

Two kinds of polymer-β-cyclodextrin derivatives(PCM-β-CD and PAE-β-CD) with different substition degrees and crosslinked densitiese were synthesized by using epoxychloropropane and Carboxymethyl-β-Cyclodextrin and N-(2- aminoethyl) amidine-β-Cyclodextrin of retaining the amino with different substitution degrees crosslinking polymerization.

论文对含有羧基和氨基的两类β-环糊精聚合物即聚合羧甲基-β-环糊精及聚合N-(2-氨乙基)胺基β-环糊精的合成及其吸附有机污染物碱性品红和苯酚的性能进行了以下研究。1。

Due to the importance of anionic polymerization in polymer ,the dynamics was also discussed by statistics method.

鉴于阴离子型聚合在高分子科学中的特别地位,本文也用了聚合反应的统计理论对本实验体系的动力学与分子量分布进行了初步探讨。

The factors which affect the average molecular weight of the polymer of AM and DMDAAC were investigated. The optimal reaction conditions are as follows: the concentration of monomer AM was 30%, while DMDAAC was 5%; the reaction temperature was 30℃, the amount of initiators at the low temperature stage was 0.05‰(compared to the weight of the monomers joining the polymerization), while V-50 was 0.025‰, the weight ratio of potassium persulphate to sodium bisulphite is 1:1, the amount of carbamide was 40‰, and complexing agent was 0.05‰, besides, aerate nitrogen gas for 8min, then the high molecular weight polymer (M=1.217×10^7) could be got after 16h reaction.

研究了影响AM与DMDAAC共聚物的平均分子量的因素,得到了优化条件为:单体浓度为30%,DMDAAC与AM摩尔比为5:95,聚合温度为30℃,低温段引发剂用量为0.05‰,K2S2O8与NaHSO3质量比为1:1,偶氮二异丁基脒盐酸盐(V-50)用量为0.025‰,尿素用量为40‰,乙二胺四乙酸二钠(EDTA-2Na)用量为0.05‰,在此优化条件下聚合反应16h后得到分子量为1.217×10^7的阳离子型聚丙烯酰胺。

The structure image of polymers were observed by microscopy and scanning electron micrograph. Porogenic solvent mixture was of advantages in the process of forming porous structure polymers during its polymerization. Absorption charateristic of conventional SPE column was proved by catalytic-kinetic spectrophotometric determination of nitrite, which was a system of nitritre-potassium bromate -bromothymol bule.

通过SEM表征了原位聚合法制备的SPE微柱具有多孔网状结构,显微观察法与SEM表征法结合起来,证实在有致孔剂存在的条件下有利于原位聚合反应形成多孔网状结构的SPE微柱。

By the testing means of electron-spectroscopy for chemical analysis , thermogravimetric analysis , differential scanning calorimetry , transmission electronmicroscopy , the results have shown that the emulsion polymerization in situ in the presence of nano-particle of calcium carbonate can happen smoothly and successfully and the surface of nano-particle of calcium carbonate have been capsulated by polymer of acrylates, which prevent from the agglomerating of nano-particles of calcium carbonate. Because the copolymer of acrylate has good compatibility with some plastics such as PVC, ABS, AS and so on, so the dispersion of nano-scale calcium carbonate as nanometer size in these plastics can be reached more easily and the effects of nanometer can happen.

通过X射线光电子能谱、热失重分析、动态扫描量热分析、透射电子显微镜等手段,证实在纳米碳酸钙原生粒子存在下,可以进行丙烯酸酯类的原位乳液聚合,乳液聚合顺利,纳米碳酸钙表面被丙烯酸酯类聚合物所包覆,使纳米碳酸钙粒子间的团聚不易发生,同时由于丙烯酸酯类聚合物与PVC、ABS、AS等极性聚合物具有较好的相容性,从而使纳米碳酸钙在聚合物基体中能达到纳米状态分散,从而发挥纳米效应。

A chemical coagulatory coprecipitation method was used in the treatment of blast-furnace gas washing water.

用化学混凝共沉淀的方法处理高炉煤气洗涤水,实验确定了最佳的药剂为聚合氯化铝钙,工艺的最佳操作条件是聚合氯化铝钙加入量为33mg/L,PAM加入量为0。

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Lugalbanda 是神和被崇拜了一千年多 Uruk古埃及喜克索王朝国王。

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