联甲苯

Under high dilution,the cross-coupling reactions of 4,5-dicyano-1,3-dithiol-2-one(6) and dithia crown-ether annulated tetrathiafulvalenes(3a～3c) in toluene gave asymmetrical dicyano tetrathiafulvalene derivatives(7a～7c) in the presence of triethyl phosphite.The compounds 7a～7c were characterized by(~1HNMR,EA,MS and IR.

在甲苯溶液中，在亚磷酸三乙酯存在下，采取高度稀释的方法，使4，5-二氰基-1，3-二硫杂环戊二烯-2-酮分别和多缩硫杂冠醚进行交叉偶联反应，成功地得到了不对称的2，3-二氰基四硫富瓦烯衍生物。

This paper deals with making stop bleeding sponge with dried small shrimps. Firstly breaking away with inorganic salt and proteir in the dried small shrimps with acid and NaOH, secondly, taking off vinyl-in the chitin with 50% NaOH, temperature is 110 ℃. the last, reacting with chitosamine and PVA-124 make stop bleeding sponge were produced, catalyst is PdCl 2. The sponge film and sparkce is setatisfaction.

用虾壳经除盐，去蛋白处理后，用50％的NaOH溶液在110℃的温度下脱乙酰基制备壳聚糖；以1∶9的稀醋酸溶作溶剂，氯化钯作催化剂，甲苯二异氰酸酯作发泡剂、交联剂，使壳聚糖与PVA－124进行交联成膜，发泡用氨水洗成中性后在80℃的红外灯烘箱下烘干，制得止血海棉

Factory engaged in medicine, veterinary medicine, agricultural chemicals and raw materials development and production of intermediates, the series of export products: 2,2 - bipyridine, 2,6 - dihydroxy toluene, propiconazole intermediates, phenol line P , Fluometuron, fluorine pyronaridine oxadiazon, oxadiazon pyronaridine fluorine intermediates, Robenidine hydrochloride and so on.

本厂从事医药、兽药、农用化学品原料药及中间体的研制与生产，系列出口产品：2，2-联吡啶，2，6-二羟基甲苯，丙环唑中间体，酚线磷，伏草隆，氟咯草酮，氟咯草酮中间体，盐酸氯苯胍等等。

Dimethylamino)ethyl methacrylate was polymerized using PS-CH_2Cl as macroinitiator and CuCl/ 2,2 '-Bipyridyl as catalyst in toluene to acquire amphiphilic brush-type copolymers of PS-g-PDMAEMA.

再以氯甲基化的聚苯乙烯(PS-CH_2Cl)为大分子引发剂，在CuCl和2，2′-联吡啶(2，2′-Bipyridyl，bpy)存在下，以甲苯为溶剂，进行甲基丙烯酸N，N-二甲胺基乙酯2-(Dimethylaminoethyl methacrylate，DMAEMA的ATRP聚合，得到两亲性的梳状共聚物PS-g-PDMAEMA。

In this work , 1,8-octodiol, the starting material, reacted with 40% hydrobromic acid to produce 8-bromooctan-1-ol, with the catalytic action of PPTs, its hydroxyl group was protected by 2,3-dihydropyran. Then it coupled with 1-heptaalkyne, by means of P-2 nickel as catalyst, stereoselectivity catalysis hydrogenated, with the catalytic action of acid to take off extremital 2, 3-dihydropyran which protected hydroxy group, then used PCC to oxidize alcohol into corresponding aldehyde.

以1，8-辛二醇为原料，与40%氢溴酸进行单溴代反应，得到8-溴-1-辛醇，在对甲苯磺酸吡啶盐的催化下与2，3-二氢吡喃反应，保护分子中的羟基，再与1-庚炔进行偶联，以P-2镍为催化剂立体选择性催化加氢，酸性条件下脱末端的2，3-二氢吡喃对羟基的保护，使用氯铬酸吡啶盐将醇氧化成醛。

For the production of reactive polyurethane cross-linkinger and curing agents, 2, 4-diisocyanate toluene terpolymer, which possesses the rigid structures of hexatomic ring and three reactive functional groups, was synthesized and characterized by the Fourier transform infrared, the gel permeation chromatography and the chemical analysis methods.

为了制备高活性聚氨酯交联固化剂，用2，4-二异氰酸基甲苯三元聚合反应合成了具有3个活性异氰酸根的六元环结构异氰脲酸酯。

The results showed that intermidiate 1, 2-propanediol-sebacate of low relative molecular mass was synthesized with toluene-p-sulfoinc acid as catalyst, benzene as watercarrying agent, and of mole ratio of sebacic acid to 1, 2-propanediol of 1:4. The glass-transition temperatures of PPSC were below 0 ℃ which confirmed that PPSC would be in a high-elastic state of ambient temperature and human body temperature. PPSC was a elastomer with moderate crosslinkage, low module and high elongation, and had rapid degradation ratio (degradation degree more than 50%) in phosphate (pH value 7.4) at 37℃.

结果表明，以对甲苯磺酸为催化剂、苯为带水剂，在酸醇比为1，4的条件下可合成较低相对分子质量的中间体癸二酸聚酯二元醇；PPSC弹性体的玻璃化转变温度在0℃以下，于室温及人体温度下处于高弹态；PPSC为适度交联的、低模量高伸长的弹性体，其在37℃、pH值为7.4的磷酸盆缓冲溶液中具有较快的降解性（降解度超过50%）。

The method of activating hydroxyls of fullerenols using 2-fluoro-l-methylpyridinium p-tolu- ene sulphonate to covalently linking with bovine serum albumin and further its effect on BSA was studied.

考察了2-氟-1-甲基吡啶对甲苯磺酸盐对富勒醇羟基的活化方法，以便将富勒醇通过共价交联的方法与牛血清白蛋白连接，进而研究富勒醇修饰对BSA所造成的影响。

To estimate the bioconcentration factor of benzene derivatives in fish by gas chromatography retention time, this paper measured the BCF of chlorobenzene, o-chloro-toluene, p-dichlorobenzene, m-dichlorobenzene, 1,2-dichlorobenzene, nitrobenzene, p-chloro-aniline, p-chloro-nitrobenzene, and 4-chlorodiphenyl in grass crap, and the t_R of test derivatives on the stationary phases of six kinds polarity.

为了用气相色谱保留时间估算取代苯类化合物在鱼体内的生物富集系数，测定了草鱼对氯苯、邻氯甲苯、对二氯苯、间二氯苯、邻二氯苯、硝基苯、对氯苯胺、对硝基氯苯、4-氯联苯9种取代苯类化合物的BCF和不同取代苯化合物在6种不同极性固定相上的tR，建立了tR与BCF的一元回归方程及tR一阶分子连接性指数(1XV)与BCF的二元回归估算方程。

Research on thermodynamics and kinetics of pyrolysis reaction mechanism Kinetic and thermodynaimic research of the pyrolysis reaction mechanism of toluene was conducted at different temperature range 298-1223K. The result shows that the pyrolysis reaction firstly occurs at the methyl on the benzene ring, and produces benzyl.

裂解机理的热力学与动力学研究在298K-1223K的温度范围内对甲苯热解机理的热力学和动力学研究结果表明，热解首先发生在苯环甲基C-H键上并生成卞基自由基，主要产物为联二甲苯，反应的活化能ΔE〓=402.27kJ/mol。

They weren't aggressive, but I yelled and threw a rock in their direction to get them off the trail and away from me, just in case.

他们没有侵略性，但我大喊，并在他们的方向扔石头让他们过的线索，远离我，以防万一。

In slot 2 in your bag put wrapping paper, quantity does not matter in this case.

在你的书包里槽2把包装纸、数量无关紧要。