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Methoxystilbene and 2-methoxy-4'-nitrostilbene were synthesized from benzyl chloride and nitrobenzyl chloride by the Wittig reaction, and used as intermediates for the synthesis of the final product fluorescent whitener FP4,4'-bis(2-methoxystyrylbiphenyl via reduction and diazotisation of the latter followed by reaction with the former in the presence of NaOH.

以氯化苄和对硝基氯苄为原料,经Wittig反应合成中间体:2-甲氧基-二苯乙烯和2-甲氧基-4'-硝基-二苯乙烯。后者经还原反应、重氮化反应后,在氢氧化钠存在下与前者反应生成最终产品荧光增白剂FP4,4'-双-2-(甲氧基苯乙烯基联苯。为该类荧光增白剂的合成开辟了一条新路线

Up to 95.01% yield of 2-amino-2'-hydroxy-1,1'-binaphthyl was obtained in chlorobenzene using the oxidant with 10% FeCl3 loading on the support containing 5% TiO2 at 60 ℃. The activity of the used oxidant was improved by treatment with H2O2, which provided an effective method to regenerate the solid-oxidant.

结果表明:在60 ℃,氯苯作溶剂的情况下,含TiO25%的载体,负载10% FeCl3时2-氨基-2'-羟基-1,1'-联萘的收率最高达到了95.01%;用过的固体氧化剂经H2O2氧化处理后活性明显恢复,证明此法是一条循环再生的有效途径。

Poly{[2-(4-biphenylamino)phenyl]phenylenevinylene} was prep-ared with 4-nitroanline which was coupled with p-xylene,throughreduction、idionization、Ullmann reaction、bromization、condensepolymerizationto get the final product.

本文提出了两条合成聚(2-芳基苯撑乙烯)的新路线,即聚{ 2-[4-苯基]苯撑乙烯}是以对硝基苯胺为原料,其与对二甲苯经改良的Gomberg-Bachmann反应偶联、再通过还原、碘化、Ullmann反应、溴化、缩聚反应得到。

We succeeded in synthesizing two different segments: C〓-C〓 and C〓-C〓, employing Sharpless dihydroxylation reaction, Julia coupling and samarium diiodide mediated reaction as the key steps.

我们从单保护的1,3-丙二醇出发,以Sharpless不对称双羟化反应,Julia偶联反应以及SmI〓参与的反应为关键步骤,经过艰苦的多条合成路线的尝试与探索,成功的得到了Phorboxazole A B的两个不同的边链部分C〓-C〓和C〓-C〓。

During angiographing,3-link chemotherapy medicine was administered through the artery to carcinoma and embolization with proper amount of iodinate oil and gelfoam according to tumor size and posit...

在血管造影的同时,根据肿瘤大小、部位以及肾门淋巴结转移情况,经供瘤动脉给予三联化疗药物,再用适量碘化油乳剂及明胶海绵条给予栓塞。

Major equipment: GermanyKoetzle TRUTZSCHLER DK903, DK788 and HSR1000 and blowing machine, Rieter RIETERE65, E62 combing machine and RSB-D35 and machine, roving machine FL100 Toyota with German zinser Zinser rollers, spindles, SKF cradle frame of F1520, Italy and Germany savio SAVIO ORION thanks Laifu SCHLAFHORST AUTOCONER 338 automatic winder, Italy Savio Savio Litas RITE Twister and yarn singeing machine, Switzerland SSM-song-type winding machine, such as imported equipment, as well as drydevice, automatic single-keung tester, 100,000 meters yarn analyzer and other advanced detection equipment.

德国特吕兹勒TRUTZSCHLER DK903、DK788清梳联和HSR1000并条机,瑞士立达RIETERE65、E62精梳机和RSB-D35并条机,日本丰田FL100粗纱机,配有德国青泽ZINSER罗拉、锭子、SKF摇架的F1520细纱机,意大利萨维奥SAVIO ORION和德国赐来福SCHLAFHORST AUTOCONER 338自动络筒机,意大利萨维奥SAVIO倍捻机和立特RITE纱线烧毛机、瑞士SSM松式络筒机等进口设备,以及瑞士乌斯特条干仪、全自动单强测试仪、十万米纱疵分析仪等先进的检测仪器。

The company has the top advanced PQ35 plat and pre-technology. Among them, the product pack adopts much transport technology and mode of production, such as EHB, auto-operated electric car, slippery skiing that can carry out different types of assembly, new door's cementation technics and so on. The products' paint-pack use the top-grade e-coating, super filter wash, immerse to wash, top-advanced PVC series of material, machinal hand, adding cup type auto static electricity to spray method. The product's welding pack use the manufacturing technology for car body, such as the top-advanced Schottplatt laser check, laser weld, more-square welding, intermediate frequency's welding three-piece plat. The product's stamping use high-speed mechinal arm auto product line, KUKA dismantling robot, optics shoot slab stock orientation, and 800-tun coordinated auto pressure machines.

大众公司拥有着当今世界最先进的 PQ35平台和一大批世界先进的前沿技术,其中产品的总装配采用了可实现不同车型共线装配的滑橇、 EHB 、自动运行的电动小车、全新的车门密封条粘接工艺等输送技术与柔性化生产方式;产品涂装采用了世界一流的电泳、超滤液冲洗、浸洗、沥水和世界最先进的 PVC 系列材料及机械手、加杯式自动静电喷涂方式;产品焊装采用了目前世界最为先进的 Schottplatt 激光检测、激光焊接、大面积机器人焊接、中频焊接三层板、冲联等车身制造技术;产品的冲压采用了高速机械臂全自动生产线、 KUKA 拆垛机器人、光学摄像板料对中定位、及800吨三坐标式多工位自动压力机等。

Novel rod like phenylene thiophene based polyhydroxy amphiphiles, derivatives of gallic acid combining three hydrophilic 2,3-dihydroxypropyloxy groups and one alkyl chain via central aromatic linking units, have been synthesized by using Ni, Pd(0) catalyzed coupling reaction as key steps.

以Ni, Pd (0)催化的C-C偶合反应为关键步骤合成了基于苯联噻吩的棒状型多羟基两亲性分子,它们是以棒状芳香核为中心部分,一端带三重亲水的2,3-二羟基链,另一端为带一条烷基链的没食子酸衍生物。

Affinity chromatography materials for kinase;2. To search a suitable process route of purification of kinase in yeast by affinity chromatography, hexokinase was preparatorily purified by salt preciptation.

为确定一条采用亲和层析技术分离纯化酵母中磷酸激酶的较佳工艺路线,采用分步盐析初步纯化己糖激酶,考察硫酸铵饱争度对盐析效果的影响;以ATP为配基,SESA活化纸纤堆素制备亲和层析剂,确定最佳偶联条件和最佳静态吸附pH值后,将粗酶液直接上亲和层析柱,看分离纯化的效果;在载体和配基之问接上1。

The company provides transmission type of machinery parts, air-cooled diesel engine parts and other machinery and electronic products, main products have all kinds of transmission chain, sprocket; gear, rack; timing belt, wheel; coupling; works towline and other mechanical parts products; electronics, electrical products; also undertake industrial, civilian products produced by the design and manufacture of pipeline; At the same time, provide a related program design, technical and information consulting job.

公司主要提供传动类机械零部件、风冷柴油机配件及其它机电类产品,主要产品有传动系统方面的各种链条、链轮;齿轮、齿条;同步带、轮;联轴器;工程拖链及其它机械零部件产品;电子、电器产品;也承接工业、民用产品生产的流水线的设计与制造;同时,提供与此相关的方案设计、技术和信息咨询等工作。

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It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发,分析对称连杆曲线上鲍尔点的产生条件,提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品,年生产总值3000万美元,产品价廉物美、选料上乘、质量保证,深受国内外客户的青睐

The eˉtiology of hemospermia is complicate,but almost of hemospermia are benign.

血精的原因很,以良性病变为主。