耐热的

The conclusions were as follows: theνO-H andνC=O IR absorption maxima shifted towards higher wave numbers after imprinting 17β-estradiol on TFMAA-co-TRIM copolymer with the red shift of theνO-H groups being apparent after precipitation polymerization for 16h while that forνC=O groups being observed after polymerization for 24h. A strong interaction between TFMAA and 17β-estradiol was confirmed by the high selectivity for 17β-estradiol, as indicted by the values of the separation factor of isomers of 17β-estradiol/17α-estradiol (2.28) and the imprinted factor (3.01). Particle diameter of TFMAA-co-TRIM polymer was between 300 nm and 1.5μm, which suited well for solid phase sorbent throughout at low column pressure. The recognition of imprinting TFMAA-co-TRIM polymer for sterol molecules was driven by enthalpy eluted with acetronitile, and low temperature was in favor of the separation of sterol structure analogues on imprinting column. TFMAA-co-TRIM polymer possessed of determinate anti-heat stability, with melting point beginning at 255.84℃, Tp=257.40℃, control TFMAA-co-TRIM polymer and imprinting TFMAA-co-TRIM polymer were respectively decompounded at 267.79℃and 343.11℃, and solid micro-extraction noddle prepared by the special polymerization also showed definite recognition for 17β-estradiol by GC/MS detecting at 270℃. By selection of various washing and elution solvents, elution reagents of close polymerization system were of more advantage in template molecules retention and recognition on molecularly imprinted solid phase extraction column. At a certain extent, progesterone, 17α-estradiol, 17β-estradiol and 4-androstene-3, 17-dione could be intercepted on the MISPE column. Especially, MISPE had high selectivity for progesterone, and imprinting TFMAA-co-TRIM polymer could achieve adsorption balance within 50 min by absorption kinetics test for 17β-estradiol. However, MISPE column showed better selectivity and enrichment property for 17β-estradiol than C18 and CSPE columns according to the data from HPLC and GC/MS analyses. Recovery of 17β-estradiol on MISPE column was up to 85.5% while when prime extracting solution of milk powder was sampled, the recovery of CSPE and C18 columns were 43.7% and 30.7%, respectively.

通过研究阐明：紫外聚合产物TFMAA-co-TRIM中的νO-H振动吸收峰在聚合16h后红移，νC=O振动吸收峰在聚合24h后红移；TFMAA-co-TRIM对雌二醇异构体的印迹因子达到了3.01，α为2.28，优于其它功能单体参与得到的聚合物识别特性；TFMAA-co-TRIM聚合物粒径介于300 nm至1.5μm之间，作为色谱固定相具有良好的通量和低的柱压；在乙腈流动相中，TFMAA-co-TRIM分子印迹固定相的分离过程主要被焓驱动，低温有利于分子印迹固定相分离甾醇结构类似物；TFMAA-co-TRIM分子印迹聚合物在255.84℃时开始熔融，Tp=257.40℃，聚合物CP的降解温度在267.79℃，MIP降解温度在343.11℃，制备的固相微萃取头初步经GC/MS 270℃的耐热性测定；不同的洗提溶剂筛选证明了选择接近聚合溶剂的洗脱体系更有利于MISPE发挥识别效应；分子印迹固相萃取柱对孕酮、17α-雌二醇、17β-雌二醇和雄烯二酮都具有不同程度的保留特性，可作为此类化合物的吸附材料，特别对孕酮强保留的富集特性，可作为孕酮的选择性识别吸附剂，其分子印迹聚合物对17β-雌二醇的吸附动力学测定显示在50 min内基本达到吸附平衡，具有作为传感器核心敏感材料的潜力；对比萃取奶粉中17β-雌二醇性能，MISPE柱比非分子印迹固相萃取柱和C18柱具有更高的保留，回收率依次为85.5%，43.7%和30.7%。

Nanoparticle of an appropriate proportion were homogeneously dispersed in the PI matrix, and the interfacial adhesion between the matrix and the nanoparticle was hence strong owing to the high specific surface area and reactivity of the nanoparticle. Subsequently, the molecular chains of PI attained unchanged or even increased interaction at a proper mass fraction of the nanometer particle, which contributed to improve the wear-resistance of the nanocomposites.

采用PI的原位聚合填充方法，利用聚酰亚胺与无机纳米表面较强的相互作用（如静电作用、较强的范德华力、氢键甚至化学键的形成），用非水悬浮工艺制备了无机纳米/聚酰亚胺纳米复合材料，率先用大型分析仪器全面地表征了复合材料的结构，采用原位聚合填充法制备的聚酰亚胺复合材料中，无机纳米分散状态良好；无机纳米氧化物/聚酰亚胺复合材料的结构表征显示出PI有机相和SiO〓无机相之间形成了键联型复合体系，两相相互影响；在复合体系中，单相本体的结晶结构并未发生改变；在摩擦过程中纳米氧化物没有发生价态的转变；无机纳米氧化物的加入，提高了聚酰亚胺的耐热等级；适量纳米氧化物并不影响复合材料的机械性能， 2。

The matrix is the material component, such as plastic, epoxy cement, rubber, or metal, that surrounds the fibers or particles.

随着合成物应用的越来越多，实际上，它们已经成为目前以及不久的将来使用的主要材料；因为它们可以被设计成更强的，更轻的，更硬的以及更好的耐热性的材料，而且拥有单一的天然材料不具备的工艺特性。

The purpose of this article is to review and discuss and current preventive and healable measures of heat illness and abstract scientific programs to prevent and cure heat illness.In order to suit with the PLA"s current fight direction and to improve the army"s capacity and levels of the rear service, to keep soldiers healthy and strong in the heat stress environment, by the way of systemic evaluation, we collect a series of successful work and research experience about the heat illness prevent and treatment. After analyzing and comparing these results, then based on the theories of the preventive medicine, we have try out further adaptable programs to prevent heat illness. It consists of 5 chapters, such as "heat acclimatization, water and electrolyte supplement, regulated work/rest cycle limits, lower temperature equipment, drug preventing heat stress".

为有效降低热环境因素对部队的威胁，提高部队的战斗力和应急保障水平，有针对性地形成热区部队中暑防治保障预案，与目前特定的作战方向相适应，我们根据部队当前状况，立足部队应用，大量收集了有关文献，通过应用系统的评价方法，对耐热锻炼、水盐补充、调整作息制度、防暑降温装置和药物防暑这几项主要防暑措施的实施方法进行了全面分析比较和评价，提出了更进一步的修正意见，提炼出了适合当前部队应用的方法，使其更加适于部队的应用；同时，还对中暑急救与治疗方面的有关文献也进行了概括和总结，并根据中暑的发病特点和救治重点，为部队中暑的救治设计了现场急救装置。

The results showed that the m-PUE had better heat-resistant properties, lower glass transition temperature, higher thermal decomposition temperature and better damping property. The internal friction peak was changed from 10 ℃ to -10 ℃, while the tan δ was changed from 0.28 to 0.46. The hardness, tensile strength and tear strength of m-PUE decreased with the increase of the THEIC content. However, the swelling ratio of PUE was increased meaning a deteriorated solvent resistance property.

结果表明，引入IS环后，PUE的耐热性能有提高；IS改性的PUE的内耗峰比未改性的窄，峰位由10℃移到-10℃，且内耗峰值增大（tanδ由0.28增大到0.46），玻璃化温度降低，而阻尼性能得到提高；引入IS环的PUE的硬度和其它力学性能比未改性的PUE有所降低；随着固化剂中THEIC用量的增加，PUE的溶胀率增大，即IS改性PUE的耐溶剂性变差。

The results show that: the tensile strength, flexural strength and flexural modulus increase by about 10.4%, 62.1% and 122.3% respectively when the mass fraction of the aluminum powder increases from 0 to 50%, while elongation at break and impact strength decrease by about 65.0 and 74.4% respectively; the tensile strength, elongation at break and impact strength all increase with decreasing the particle sizes of the aluminum powders.b Nylon-12 coated metal powders for the indirect SLS process were prepared by the dissolution precipitation process. The coated powders have only 1.0 wt% nylon-12, and their SLS green parts have sufficient strength for features as small as 1.0 mm to be built and post-processed and high dimensional accuracy. The green parts were subjected to the post processing processes including binder decomposition and infiltration of epoxy resin, and then the metal/polymer composite parts with relatively high strength and accuracy were formed.At present, micron-scale inorganic fillers have been widely used to reinforce nylon SLS parts.

将该法制备的尼龙12覆膜金属粉末用于以下两个方面：a使用铝粉增强尼龙12的SLS成形件，通过溶剂沉淀法制备尼龙12覆膜铝复合粉末，研究了铝粉含量及粒径对SLS成形件性能的影响，结果表明：铝粉分散均匀，并与基体有良好的界面粘接；当铝粉含量从0增加到50wt％时，成形件的拉伸强度、弯曲强度、弯曲模量分别提高10.4％、62.1％和122.3％，冲击强度和断裂伸长率下降65.0％和74.4％，耐热性及尺寸精度也得到提高；断裂伸长率、冲击强度及拉伸强度均随着铝粉粒径的减小而增大。b使用溶剂沉淀法制备了间接法SLS用尼龙12覆膜金属粉末，该覆膜粉末中聚合物粘接剂的含量仅为1.0 wt％，其SLS初始形坯具有较高的精度以及足够满足后处理要求的强度，最小精细结构的尺寸达1.0 mm。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。