考察

First, the preparation of l,2-dichloro-4-nitrobenzene, which l-chloro-4-nitrobenzene reacted with chlorine in a self-designed chlorinator, in presence of Lewis acid catalyst,.was investigated. By means of the Orthogonal Experiments design and single factor experiments, the influence of several reaction variables on the yield were examined and the optimum reaction conditions under the intervallic operation were obtained, the yield of l,2-diehloro-4-nitrobenzene was 83.26%.

为此，本文首先在自行设计的塔式氯化器中，以对硝基氯苯为原料，路易氏酸作催化剂，分子氯氯化合成3，4-二氯硝基苯(合成3-氯-4-氟-硝基苯的原料)，根据该氯化过程特征，利用正交试验设计方法结合单因素实验考察了有关因素对氯化过程的影响，优化得到了最佳的氯化工艺条件，3，4—二氯硝基苯的收率可达83.26％。

First, a chlorinator was self-designed in this paper, and dichloride of 2-methyl-1-propene was synthesized by 2-methyl-1-propene reacted with chlorine fast in this reactor. By means of the Orthogonal Experiments design and single factor experiments, the influence of several reaction variables on the yield were examined and the optimum reaction conditions under the intervallic operation were obtained, the yield and selectivity of dichloride of 2-methyl-1-prop-ene were more than 65% and 80% respectively. Second, the preparation of 2-methylene-1, 3-propanediol, which dichloride of 2-methyl-1-propene reacted with alkali was investigated. By means of the Orthogonal Experiments design and single factor experiments, the influence of several reaction variables on the yield were examined and the optimum reaction conditions under the intervallic operation were obtained, the conversion of dichloride of 2-methyl-1-propene was 100%. Moreover the preparation of MPO, which 2-methylene-1, 3-propanediol reacted with hydrogen, in presence of Al_2O_3-Pd catalyst, was gotten, and the product was appraised.

本文在氯化反应过程中，自行设计制作出了氯化管式反应器，在该反应器中异丁烯和氯气迅速混合反应生成二氯异丁烯，根据该氯化反应特征利用正交试验和单因素试验考察了有关因素的影响并优化得到了最佳工艺条件，二氯异丁烯的总收率达65％以上，选择性达80％；接着，对二氯异丁烯进行水解反应制得了2-甲烯-1，3-丙二醇，讨论了相关因素对水解反应的影响，并通过正交试验和单因素试验得到了较佳工艺条件，二氯异丁烯的转化率达100％；同时还对制备的2-甲烯-1，3-丙二醇在常压下采用三氧化二铝负载钯催化剂催化加氢得目的产物MPO，并对产品进行了鉴定，从而打通了整个工艺路线。

Furthermore, the effect of temperature and contact time on toxicity of chlorine dioxide was observed.

以水厂原水为试验水样，研究了二氧化氯对摇蚊不同龄期幼虫的毒性效果（24 h），并考察了温度和接触时间对二氧化氯毒性效果的影响。

Effects of various factors on the yield and chlorine content were investigated.

考察了诸因素对产物得率和氯含量的影响。

Catalytic activities of phosphotungstic acid for liquid-phase nitrations of benzene,toluene and chlorobenzene were studied.

研究了磷钨酸对苯、甲苯和氯苯液相硝化反应的催化活性，考察了反应温度、反应时间、硝酸与芳烃摩尔比对芳烃转化率和产物选择性的影响。

P-nitrophenoxy ethanol is synthesized with p-nitrophenol and chlorohydrin in the presence of water solution of KOH,with better quality and high yield of the product,and with much lower costs over the reported methods.

以对硝基苯酚和氯乙醇为原料，在KOH的水溶液中进行反应，以较高收率合成了对硝基苯氧乙醇，此方法成本低、纯度高，同时考察了多种因素对产率影响。

The chloromethane -containing waste gas was treated by catalytic oxidation process and the affecting factors were studied.

用催化氧化法处理氯甲烷废气，考察了各种因素对催化氧化处理效果的影响。

Alkylations of benzene with dodecene and/or chloromethane in the room temperature ionic liquid 1-methyl-3-butylimdazole chloride-aluminium chloride as catalyst have been investigated with high conversion and selectivity.

首次研究了在氯铝酸室温离子液体系中二甲苯与苯乙烯的烷基化反应制1-苯基1-二甲苯基乙烷及其衍生物。考察了离子液体催化剂量和反应条件的不同对产物组成及副产物数量的影响。

Chlorophenol(2-CP) and 4-chlorophenol(4-CP) were treated respectively in coupled ultrasound/ electrocatalysis systems.

采用超声波-电催化联合技术处理2-氯酚(2-CP)和4-氯酚(4-CP)，探讨了电催化氧化和超声氧化的协同效应，考察了影响声电联合降解氯酚化合物的条件因数。

Chlorophenol (4-CP) solution was treated by US/UV synergetic catalysis technology and the major influencing factors such as the sound intensity, initial pH value of solution, initial 4-CP concentration, the amount of catalyst and medium temperature were examined in this paper.

选择掺杂过渡金属离子Fe3 +的纳米TiO2 为催化剂，研究了US UV协同催化氧化水中对氯苯酚(4 CP)的降解效果，考察了对氯苯酚的起始浓度、超声波声强、溶液初始pH、饱和气体种类、反应温度和催化剂投加量对氯苯酚降解速率的影响。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。