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XPS and FTIR spectroscopy analysis indicated that chemical bonds were formed between maleic rosin and wood flour through the esterification reaction of anhydride groups and hydroxyl groups on wood surface.

FTIR与XPS分析表明,马来松香分子中的酸酐基团与木粉表面的羟基发生了酯化反应,并且马来松香是以单酯的形式接枝到木粉表面,同时产生-游离羧基。

In connection with the character of Boc L-Glutamic Acid and aminoacetic acid structures, the reaction of aminoacetic acid acylated via Boc Anhydride has been studied on the condition of CH3OH in the paper. The yield of the derivatives is characterized by the melting point, the content of carboxylgroup and the product purity. The results showed that the best experiment condition is followed.

本论文以甲醇作为均相反应介质,Boc酸酐与谷氨酸为原料,在碱性条件下,以产物的熔点,羧基含量以及产物纯度作为产物质量确定的指标,最终得出N-Boc-谷氨酸的合成最优条件。

With the molar ratio of cobaltous nitrate, phenanthroline and Pyridine-3,4-dicarboxylic acid is 1∶2∶1,under the condition of pH=5,heating at 50-60℃ and stirring,the ternary complex of cobalt is synthesized in the methanol solution.

将硝酸钴、邻菲罗啉和3,4-二羧基吡啶按1∶2∶1物质的量比计量,在pH=5和50-60℃加热搅拌的条件下,在甲醇溶液中合成了钴的三元配合物,用元素分析、红外光谱、紫外光谱、热重分析和摩尔电导率对配合物进行表征,结果表明该配合物为1∶1型电解质,其组成为[CoⅢ2]NO3.H2O,其中Pydc=

The invention uses the method of the fusion and direct polymerization to prepare the carboxyl-terminated lactic acid prepolymer and then copolymerize with the aliphatic polycarbonate; then the reaction is done in the twin-screw extruder to screw out the extension chain and the good polylactic acid copolymer is made.

本发明采用熔融直接缩聚的方法制备出羧基封端的乳酸预聚物,接着再与脂肪族聚碳酸酯二元醇进行共聚,然后再在双螺杆挤出机中进行反应挤出扩链,制备性能良好的聚乳酸共聚物。

Methods: The model of evaluating T cell proliferation stimulated with polyclonal activators, ConA was established by vital dye carboxyl fluorescin diacetate succinmidyl ester labeling technique. The effect of a specific inhibitor for p38 MAPK, SB253580, on T cell proliferation on different doses and in different time was estimated by flow cytometry. At the same time, the percentage of proliferating T cells and proliferation index were measured by CellQuest and SPSS10.0 for Windows softwares.

以活体染料羧基荧光素乙酰乙酸琥珀酰亚胺酯染色,建立了在多克隆刺激剂刀豆蛋白A刺激下评价小鼠T细胞增殖的模型,通过流式细胞术分析p38丝裂原活化蛋白激酶的特异性抑制剂SB203580在不同剂量、不同时间对T细胞增殖的作用,并应用CellQuest和SPSS10.0 for Windows软件分析增殖细胞各代所占比例和增殖指数。

Chemically, fluoroquinlones are an amphoterics molecule processing major ionizable groups, a basic piperazine amine and acidic carboxyl. The form of drugs was greatly affected by the acidity in aqueous solution. Thus the effect of pH values in aqueous solution on the fluorescent properties of fluoroquinolones was studied in details, the spectral properties of each form was characterized. It was found that the fluoroquinolones exhibit weak fluorescence in strong basic solution.

氟喹诺酮类药物分子结构中既有羧基,又有哌嗪氨基,它们所处环境的pH值对其存在型体有很大影响,因此我们详细研究了水溶液的pH值对该类药物光谱特性的影响,并对于各型体光谱特征进行归属,发现强碱性溶液中其发光较弱。

With the varying of potential the adsorption behavior of picolinic acid is invariant,while the adsorption behavior of isonicotinic acid and nicotinic acid may change.

分析表明在电极电位负移过程中皮考酸分子一直采取通过羧基和苯环上的N原子侧立吸附在银电极表面,与之不同的是,异烟酸分子和烟酸分子在表面的吸附状态都随电位改变发生了变化,我们对此进行了分析和解释。

With the varying of potential the adsorption behavior of picolinic acid is invariant, while the adsorption behavior of isonicotinic acid and nicotinic acid may change. The probable reasons are given.

分析表明在电极电位负移过程中皮考酸分子一直采取通过羧基和苯环上的N原子侧立吸附在银电极表面,与之不同的是,异烟酸分子和烟酸分子在表面的吸附状态都随电位改变发生了变化,我们对此进行了分析和解释。

The alkaline-earth metal complexes with mucic acid was successfully prepared via gel formation and characterized by elemental analysis,FT-IR measurements.

结果表明,粘液酸的两个羧基和四个羟基均能参与配位键的形成,而中心离子 Ca~(2+)、Sr~(2+)、Ba~(2+)与配体粘液酸的配位状况存在着一定差异。

Biochemical and Biological Properties of 4-(3-phenyl-[1,2,4] thiadiazol-5-yl)-piperazine-1-carboxylic acid phenylamide, a Mechanism-Based Inhibitor of Fatty Acid Amide Hydrolase Technical Communication

4--哌嗪-1-羧基酸苯胺的生化和生物学属性,脂肪酸氨基水解酶的一个基于机制的抑制剂

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