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Epoxycedrane was firstly synthesized at home and abroad from α-cedrene by epoxidation of hydrogen peroxide under the catalysis of ruthenium trichloride and pyridine-2, 6-dicarboxylic acid.

以三氯化钌和2,6-二羧基吡啶为催化剂,双氧水为氧化剂,时α-柏木烯进行环氧化反应合成环氧柏木烷。本合成方法在国内外尚未见报道。

Keywords: mast cells;tryptase;chymase;carboxypeptidase;osteoarthritis

中文关键词:类胰蛋白酶;类糜蛋白酶;羧基肽酶;骨关节病

With the molar ratio of cobaltous nitrate, phenanthroline and Pyridine-3,4-dicarboxylic acid is 1∶2∶1,under the condition of pH=5,heating at 50-60℃ and stirring,the ternary complex of cobalt is synthesized in the methanol solution.

将硝酸钴、邻菲罗啉和3,4-二羧基吡啶按1∶2∶1物质的量比计量,在pH=5和50-60℃加热搅拌的条件下,在甲醇溶液中合成了钴的三元配合物,用元素分析、红外光谱、紫外光谱、热重分析和摩尔电导率对配合物进行表征,结果表明该配合物为1∶1型电解质,其组成为[CoⅢ2]NO3.H2O,其中Pydc=

Multi-bioinsecticidal-toxin BtA is a bioconjugation product with multiple acting-sites, formed by biochemical bond-linking reaction between two biotoxins, protoxin of Bacillus thuringiensis and Abamectin, through the amino and carboxyl conjugator EDC. The variation of pest susceptibility to Multi-bioinsecticidal-toxin BtA was evaluated by studying the decline and recovery of susceptibility of Plutella xylostella L.

多位点生物杀虫毒素BtA是通过氨基-羧基偶联剂EDC将两种生物毒素进行键合反应,形成的具有多个作用位点的生物藕合产物。

The invention uses the method of the fusion and direct polymerization to prepare the carboxyl-terminated lactic acid prepolymer and then copolymerize with the aliphatic polycarbonate; then the reaction is done in the twin-screw extruder to screw out the extension chain and the good polylactic acid copolymer is made.

本发明采用熔融直接缩聚的方法制备出羧基封端的乳酸预聚物,接着再与脂肪族聚碳酸酯二元醇进行共聚,然后再在双螺杆挤出机中进行反应挤出扩链,制备性能良好的聚乳酸共聚物。

A small molecule core (TMP-SK3)with three terminal carboxyl groups was synthesized successfully by the reaction of 1,1,1-trihydroxymethylpropane with the excessive sebacic acid diacetic anhydride.

以1,1,1-三羟甲基丙烷与过量癸二酸二乙酸酐反应,制得了端羧基的三官能度小分子核三癸二酸三羟甲基丙烷酯(TMP-SK3)。

The cage effect of Gn potassium aqueous solution calculated by theα-cleavage photoreaction product distribution of substituted dibenzyl ketone was 14%, 18%, 22% and 42% for generations 1-4, respectively, which indicates that G4 takes a more close spherical shape with strong confine ability.

研究结果表明,羧基为末端基团的芳醚树枝形聚合物Gn (n = 1-4)钾盐水溶液笼效应随代数增加而增大,从G1到G4,笼效应分别为14%、18%、22%和42%,树枝形聚合物3代到4代从开放结构变为近乎球形的封闭结构的显著变化使G4表现出明显高于其他三代的笼效应。

AIM: To investigate the effect of PD98059, a specific repressor of extracellular signal regulated kinase1/2 (ERK1/2), on the proliferation of the murine lymphocytes. METHODS: Lymphocytes were isolated from lymphoid nodes of BALB/c mouse. After stained with carboxy fluorescein diacetate, succinimidyl ester, the cells were stimulated with polyclonal activators, concanavalin and phorbol 12,13 dibutyrate plus ionomycin.

分离小鼠淋巴结细胞,藉羧基荧光素乙酰乙酸染色,用多克隆刺激剂刀豆A蛋白或者佛波醇酯加离子霉素刺激,以流式细胞术分析PD98059对淋巴细胞增殖的影响;利用碘化丙锭染色分析PD98059对细胞周期的影响。

Three metal ion bridged self-assembled films of cis -di-bis(2,2'-bipyridyl-4,4'-dicarboxylate) ruthenium were fabricated and characterized by contact angle, UV spectra, cyclic voltammetry and XPS. Their photoinduced electron transfer properties were examined.

本文通过三种金属离子桥联的方式制备了一系列cis-RuL22 (L代表4,4'二羧基-2,2'联吡啶)自组装膜,并利用接触角,UV光谱,循环伏安法以及XPS对自组装功能膜进行了表征。

Our results show that Cd indeed influences the excretion of individual and total dicarboxylic organic acids by roots.

本实验结果显示,土壤中重金属的含量,就镉来说,的确会对根圈土壤中根分泌之双羧基有机酸的含量造成影响,不论是乡个别或总量皆是如此。

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