羟基酸

Results Ten known constituents were isolated and their structures were identified as 23-hydroxyursoIic acid (1), alphitolic acid (2), ursolic acid (3), dihydro-β-cyclopyrethrosin (4), sesamin (5),β-sitosterol (6), clauslactone-K (7), betulinic acid (8), lingueresinol (9), ent-isolariciresinol (10), respectively.

结果：从上述三种植物中共分离鉴定了10个化合物，其分别是：23-羟基熊果酸(1)、alphitolic acid(2)、熊果酸(3)、二氢-B-环除虫菊精(4)、芝麻素(5)、β-谷甾醇(6)、clauslactone-K(7)、白桦脂酸(8)、lingueresinol(9)和ent-isolariciresinol(10)。

Calcium carbonate and soluble glass and so on were confected as alkaline antifouling agent. The Infrared Spectrometry results showed that 2275-2250 cm~(-1) diagnostic absorb wave crest in part A and 3390-3200 cm~(-1) in part B and 1730 cm~(-1) in coating film strongly proved polymers reacted just as the reacting mechanism, that means polysiloxane which offer low-surface-energy property linked Polyurethane system by —OH groups reacting with —NCO groups. Relative molar mass of part A and part B was determined by Gel Permeation Chromatography and the results were appropriate. Surface-energy was determined and results were between 33.6-47.17 mN/m and it increased when alkaline antifouling agent was put into the coating. Alkaline antifouling agent was releasing steadily when the coating film was dipped in seawater. As time gone, the pH value of seawater was increasing. Solubility parameter and results showed that there was no corrasive phenomenon between the polyethylene strand and the coating.

红外光谱分析结果表明，出现在A组分中的2275～2250cm~(-1)处的异氰酸酯特征吸收峰、B组分中的3390～3200cm~(-1)处硅羟基的特征吸收峰及出现在固化后涂膜中的1730cm~(-1)处氨基甲酸酯基团的特征吸收峰证明了涂料成膜物质交联固化符合本文的设计要求，即赋予涂膜低表面能特性的有机硅组分通过—OH基团与—NCO基团的反应已经链接到聚氨酯体系中；凝胶渗透色谱结果表明，成膜物质的A、B组分均为低分子量，符合预聚物的要求；涂膜表面能的测算结果表明，涂膜的表面能在33.6～47.17mN／m之间；加入碱式防污剂后涂膜的表面能略有升高；碱式防污剂的释放平稳，随着涂膜在海水中浸泡时间的增长，pH值有增加的趋势；用溶解度参数原则来评价涂料与网绳的涂装，结果表明，本试验研制的防污涂料对聚乙烯网绳无溶蚀作用。

The results showed that hydrogen peroxide, silanols species and TiO〓 didn't have solvolysis activity of propylene oxide. While framework Al, coordinatively unsaturated Ti〓 ions as Lewis acid sites in the framework, Ti-OH and the five member ring active titanium species formed by TS-1, hydrogen peroxide and solvent can catalyze the solvolysis of propylene oxide.

研究结果表明：原料双氧水和TS-1沸石上的SiOH和TiO〓对环氧丙烷溶剂解反应无催化活性；而下列物种对环氧丙烷溶剂解反应具有催化活性：TS-1中的骨架铝，沸石骨架中配位不饱和的Ti〓形成的L酸中心，TS-1水解产生的钛羟基和由TS-1，双氧水和溶剂相互作用所生成的五元环中间活性钛物种。

aim: to establish qualitative and quantitative analysis methods of 7, 4′ bihydroxylisoflavone 3′ sulfonate.

目的：建立7，4′二羟基异黄酮 3′磺酸钠的定性和定量分析方法。

In the experiment, the variousfactors which influenced the synthesization of 3-hydroxybutic acid were studied.

对影响3-羟基丁酸合成的各种因素进行了考察。

The hydroxyethylidene diphosphonic acid was prepared by phosphorus trichloride ,acetic acid with water.

用三氯化磷、冰醋酸和水合成了羟基乙叉二膦酸。

hydroxy-2-acetonaphthene was obtained by the hydrolysis of 6-methoxy- 2-acetonaphthene in the presence of HCl (36%) and triethylamine as a catalyst.

摘 要：采用6 甲氧基 2 乙酰萘与浓盐酸在缚酸剂三乙胺存在的条件下进行水解反应制得6 羟基 2 乙酰萘。

Reactions of 2,6-pyridinedicarboxylic acid or 2,6-dibromomethyl pyridine with 5-(4-hydroxyphenyl)-10,15,20-triphenyl porphyrin, 5-(4-aminophenyl)-10,15,20 triphenyl porphyrin gave three novel bridged diporphyrins 3-5, respectively.

通过将2，6-吡啶二羧酸或2，6-二溴甲基吡啶分别与5-(4-羟基苯基)-10，15，20-三苯基卟啉(1)和5-(4-氨基苯基)-10，15，20-三苯基卟啉(2)反应，合成了3种新型的双卟啉化合物3~5。

N L-Leucine Producer,Strain No .145,was obtained from mutants resistant to α-amino-β-hydroxyl valeric acid and rifampin by mutagenizing Brevibacterium Tianjinese T6-13 with ul-traviolet rays,It produced L-Leucine up to 32mg/mL on shaker and 21.8mg/mL of L-Leucine was produced in 16 liter fermentor in 60 hours.

以天津短杆菌T6～13为出发菌株，采用紫外线进行诱变处理，筛选α－氨基－β－羟基戊酸和利福平抗性突变株，获得一株L－亮氨酸产生菌No.145，L－亮氨酸摇瓶产量可以达32.1mg／mL。在16L发酵罐中培养60h，L－亮氨酸产量可以达21.8mg／mL葡萄糖转化率可以达20％。

Poly β hydroxybutyric acid; Zoogloea ; op timized optimal culture medium ; fermentation conditions

聚β－羟基丁酸；动胶菌；优化培养基；发酵条件

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。