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羟基苯

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Two new active esters of acrylic acids monomers, N-p-acryloxybenzoyloxy succini-mide and N-p-methacryloxybenzoyloxy succinimide have been synthesized and polymerized.ABOSu and MBOSu were prepared by coupling of p-acryloxybenzoic acid or p-methacryloxybenzoie acid with N-hydroxy succinimide in the presence of dicyclohexylcarbodimide.

新的丙烯酸活性酯,N-(对甲基丙烯酰氧苯甲酰氧基)丁二酰亚胺及N-丁二酰亚胺单体分别由对甲基丙烯酰氧基苯甲酸、对丙烯酰氧基苯甲酸与N-羟基丁二酰亚胺在环已基羰二亚胺存在下经偶联反应合成。

A gelator (G2) synthesized from 1,2,4,5-benzene tetracarboxylic acid and 4-hydroxy pyridine at molar ratio of 1:4 was characterized by 1H-NMR and FT-IR.

采用1H-NMR和FT-IR表征了在摩尔比1:4条件下,由均苯四甲酸和对羟基吡啶合成的一种凝胶因子(G2)。

Compared with G1 synthesized from 1,2,4,5-benzene tetracarboxylic acid and 4hydroxy pyridine at molar ratio of 1:2,G2 gelled water at higher minimum gelator concentration and gave the gel with lower gel-to-sol dissociation temperature at the same concentration.

相对于在摩尔比1:2条件下,由均苯四甲酸和对羟基吡啶合成的凝胶因子G1,在相同浓度下,G2在更高的最低凝胶因子浓度使水凝胶,并且得到的凝胶具有更低的凝胶-溶胶破坏温度。

Tetra-(8-hydroxy-quinolinato) boron complex with tetrahedral-like geometry and 3,3',4,4'-benzophenone tetracarboxylic anion with long-chain structure were successfully intercalated into layered double hydroxides with ion-exchange method.

我们首次选择了两种具有不同构型的光活性物种作为客体,即:具有四面体构型的四-(8-羟基喹啉)硼配合物和具有长链形状的3,3′,4,4′-苯酮四羧酸,得到了两种新的有机无机杂化光功能材料。

Through cyclic hydrogen bonding with motif formed by coordinated water molecules and coordinated hydroxyl groups of dhbd from adjacent tetranuclear units, these adjacent neighbors are connected to afford a 1D supramolecular chain along axis a, which is further extended via aromatic intercalations and other crystallization water molecules into a 3D structure with channels.

毗邻的四核单元通过配位H2O分子和配位羟基O原子形成的 R 22(8)型环形氢键桥的连接,沿a轴方向构建了四核单元交替相连的一维超分子链;链间籍苯环的π-π堆积作用和晶格水分子氢键链的连接进一步扩展为具有隧道的三维结构。

The other type of trimeric product containing 2 ferrocene units has also been synthesized. Its 13C NMR anal.

通过混合三聚反应,也合成了另一类含两个二茂铁化合物, N,N'-二-2-羟基-5-特丁基苯甲二胺。

n thes paper, the oligomers with different molecular weight of monohydroxylpolyethersulfones were synthesized in solution and the optimum condition ofpolymerization was obtained; With phase transfer catalyst method,the oligomerswas obtained and transformed to monovinylpolyethersulfones macromer. Its structure was characterized with IR and 1H-NMR.

本文采用溶液法以单酚(4-氯-4'-羟基二苯砜)为原料合成了不同聚合度的单酚低聚体,得到了控制聚合度的最佳聚合条件;用相转移催化剂法成功地将单酚转化为单烯大分子单体,并用IR、1H—NMR对其结构进行了表征;测定了双键官能度均在1.90以上。

High-pressure liquid chromatography was used to determine the retention time and integral area ratio of every esterified production.

对不同条件下合成的三羟基二苯甲酮酯化215感光剂进行高效液相色谱分析,确定了产物中各酯化产物的保留时间及其在产物中所占的积分峰面积比。

Phenolic agent in alkaline lignin separated fromthe the black liquid can result in a chain etherized reaction on cycloalkanes by alkaline distilling so as to make lignin change its property.

从蒸煮黑液中分离的碱木素苯环上的酚羟基可与环氧烷基胺发生醚化接枝反应,从而使木素胺化改性。

Diamino-dipenylamine-2-sulfonicacid was used as an alternative of benzidine,and reacted withl-hy droxy-8-aminonaphthalene-3,6-dusuifonicacid,m-benzioc-diamine and aniline to synthesize eco-friendly black direct dye s.

报道了以4,4'-酸(4,4'-二氨基-二苯胺-2-磺酸)代替联苯胺,与H酸(1-羟基-8-氨基-3,6-二萘磺酸)、间苯二胺、苯胺等合成无致癌作用的环保型黑色直接染料。

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