羟基苯

Two solid complexes of terbium with phenylacetic acid(L1) and phenyl-hydroxylacetic acid(L2) were synthesized by solid state reaction at low temperature,and the complexes were characterized by chemical analysis.

以两种不同结构的羧酸苯乙酸和苯基羟基乙酸与氯化铽为原料，采用低温固相反应合成了两种羧酸铽配合物。

In Chapter 3, the separation of Fe〓, Co〓, Ni〓, Zn〓, Cu〓 by CE in the presence of imidazole or phenylamine as UV-absorbing background electrolyte and α-hydroxybutyric acid as the complexing agent with indirect UV absorbance was investigated.

在第三章，研究了以咪唑或苯甲胺为背景吸收电解质，α-羟基异丁酸为络合剂，采用毛细管离子电泳间接紫外法测定了镍矿石中Ni，Co，Cu的含量。

"Half-water-hydrolysis"method is used to modify the preaminolysis of phenylenediamine in"step coupling polymerization". First, dehydrochlorination polycondensation between Si-OH and Si-Cl group during polycondensation reaction is employed instead of dehydration reaction between Si-OH groups before, which avoids the disconnection of Si-N bond destreyed by isolated water and improves the H-bonding template effect of the bridged-phenylenediamine.

探索用&半水水解-脱氯化氢缩聚&法对我组过去提出的&全水水解法&的预胺解法加以改进，经&半水水解&得到的含硅羟基和硅氯基的单体再以脱氯化氢代替脱水的方法减少了极性溶剂存在下游离水断裂梯撑模板的硅-氮键的可能性，有效地提高了对苯二胺梯撑中氢键的模板作用。

In this work,the new kind of polyurethane have been prepared from Bis(4—β—hydroxyphnyl)sulphone,polyhydrofuran, 4,4′—di—phenylmethane diisocyanate,by one—step reaction metho -d and block copolymerizatiano.

本文用一步反应法，由双(4-β-羟基乙氧基苯)砜，聚四氢呋喃，4，4′—双苯基甲烷二异氰酸，采用嵌段共聚法，制成了一种新型聚氨酯。

Study of polarographic behavior of 2, 4 - dihydroxybenzophenone

防晒剂2，4-二羟基二苯甲酮的极谱行为研究

Amoung 10 compounds (polyhydroxy substituted N-benzoylserotonin derivatives), compound 4 shows the highest number of ε. The ε of compound 4 is high up to 11.43 × 103㎝-1M-1, which is the 2.84 times of the ε of control group, octyl salicylate. Moreover, compound 4 can absorb all the wavelength if UVB (280 nm - 320 nm), so compound 4 can provide the best protection from UVB. Additionally, this study also discovers that the compound 5 not only can absorb UVB, but also can absorb UVA.

而本研究所合成之多羟基取代N-色洛冬宁苯甲醯胺衍生物（化合物1 ~ 10）莫耳吸收系数最高者为化合物4，其在波长306 nm的莫耳吸收系数达11.43 × 103㎝-1M-1，为对照组水杨酸辛酯的莫耳吸收系数的2.84倍，且化合物4的吸收波长涵遝蒤紖VB波长(280 ~ 320 nm)的范围，故化合物4能提供UVB波长的最佳防护；另外化合物5除了具有UVB波长的吸收外，还具有UVA波长的吸收作用。

In the study of testing the overall ability of anti-oxidation, polyhydroxy substituted N-benzoylserotonin derivatives (compound 1-10) still have the better overall ability of anti-oxidation than control group, trolox. The IC50 values of compound 1-10 range 2.49 to 3.92, while the IC50 value of trolox is 5.23 μg/ml. Compound 10 is still the best derivative which has the best overall ability of anti-oxidation; IC50 value is 2.49 μg/ml.

而在总抗氧化能力结果显示，相较於对照组水溶性维生素E之IC50值5.23 μg/ml，多羟基取代之N-色洛冬宁苯甲醯胺衍生物（化合物1 ~ 10）之总抗氧化能力效果IC50值介於2.49 ~ 3.92 μg/ml之间，十种醯胺化合物的总抗氧化效果皆比对照组水溶性维生素E的抗氧化效果还要来得优越，其中效果最强的仍为化合物10，其 IC50值为 2.49 μg/ml。

In the study of UV absorbing test, polyhydroxy substituted N-benzoylserotonin derivatives (compound 1-10) shows better ability to absorb UV and shows wider range of absorbing UVB than control group, octyl salicylate. With respect to octyl salicylate, octyl salicylate can abosorb the highest wavelength up to 306 nm under UVB (wavelength ranges 280 nm ~320 nm), and the ε is 4.03 × 103 ㎝-1M-1. However, the ε of polyhydroxy substituted N-benzoylserotonin derivatives (compound 1-10) under 306 nm range 4.14 × 103 ~ 11.45 × 103㎝-1M-1. It is reasonable that the compounds in this study can not only absorb the individual wavelength amoung the wavelenght of UVB, but also absorb wider range of wavelength.

在紫外线可见光吸收测试结果显示，相较於对照组水杨酸辛酯在UVB波长(280 ~ 320 nm)范围最大吸收波长为306 nm，其莫耳吸收系数为4.03 × 103 ㎝-1M-1，而多羟基取代之N-色洛冬宁苯甲醯胺衍生物（化合物1 ~ 10）在306 nm的莫耳吸收系数介於4.14 × 103 ~ 11.45 × 103㎝-1M-1，其吸收紫外线的效果皆优於对照组水杨酸辛酯，且其在UVB波长的范围吸收波长的光谱也较宽广，可知每个化合物并非只是对UVB波长范围内的单一波长有吸收度，而是对UVB波长范围具有较宽广的光谱吸收。

In the present paper,the use of 8-hydroxyquinolinecomplexs in precipitate flotation to separate and preconcentrate Cu and Mn,using SDBS as collector,followed by AAS spectrophotometric determination is proposed.

提出了以8-羟基喹啉为沉淀剂，十二烷基苯磺酸钠为浮选剂，沉淀浮选预分离富集与火焰原子吸收光谱法联用测定痕量Cu和Mn的新方法。

Cooking at the course functional groups of residual lignin changes, methoxyl content decreased, from 15.42% dropped to 12.35%, the phenolic hydroxyl group content and carboxyl content has increased, from 2.08% rosed to 3.17%, carboxyl content from 5.36% rosed to 5.99%.

木质素研究指出：甜竹原料木质素中C9单元式甲氧基含量与青皮竹比较相近、分子量主要集中在小于4000组分(占50.5%)而大于16000只占少量、甲氧基含量为15.42%、酚羟基含量2.08%、羧基含量5.36%、硝基苯氧化结果摩尔比为

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。