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Bromooctane was synthesized from potassium bromide(by-product of synthesizing 2-hydroxy-4-octyloxybenzophenone) and n- octanol using concentrated sulfuric acid as a catalyst.

以生产2-羟基-4-正辛氧基二苯甲酮的副产物溴化钾和正辛醇为原料,浓硫酸为催化剂,合成了溴代正辛烷。

The integrated analytical results show that the novel ligand coexists in ketoform and enolform structures under the measuring conditions, the ketoform structure may change into the enolform structure during the coordination and bonds with the central ion by two O atoms of the enolized hydroxyl group of pyrazolone ring and H2O and the N atom of the imine group and the N atom containing H of benzimidazole ring by losing the proton. And the coordination number of these complexes is four.

综合各种分析结果显示:配体在测试条件下以酮式和烯醇式结构共存,配位时酮式可能转化为烯醇式结构,按去质子的方式以吡唑啉酮环羟基和H2O上的两个O原子以及亚胺基上的N原子和苯并咪唑环上的含氢N原子与中心离子成键,配合物的配位数为4。

By using a mixture of aromatic hydrocarbon and water as a binary solvent,reaction of pyrogallol with PhCCl 3 was carried out in the presence of a catalyst(ZnCl 2?AlCl 3 or SOCl 2).2,3,4-Trihydroxybenzophenone was obtained in yields of 80%-87% with the advantages of easy control,stable yield,high product quality and low cost.

以焦性没食子酸为起始原料,在惰性气体保护和催化剂(ZnCl2、AlCl3或SOCl2)的存在下,在芳香烃与水组成的二元混合溶剂中,与三氯甲苯反应,经过芳香烃溶剂的后处理,可以得到2,3,4-三羟基二苯酮,产率最高达87%。

OH was produced by Fenton reaction and super oxide radical (O-2.) was produced by the oxidation of pyrogallol.

羟基自由基由Fenton体系产生,超氧阴离子自由基(O-2·)由邻苯三酚自氧化体系产生。

The method has been successfully applied to the determination of salicylic acid and resorcinol in Dermatitis Clear Tincture and p-hydroxybenzoic acid in apple juices.

应用此方法,成功测定了皮炎呤酊剂中的间苯二酚和水杨酸以及苹果汁中的对-羟基苯甲酸。

The results show that the second - order derivative peak potential of 2,4 - dihydrobenzophenone is - 1.20 V

实验表明,在pH4.30的B—R缓冲溶液中,2,4-二羟基二苯甲酮的二阶导数峰电位为-1.20V

Using 1-amino-2-phenoxy-4-hydroxyanthraquinone, chlorosulfonic acid ,thionyl chloride,and 3-ethoxypropylamine as raw materials and sodium carbonate as acid-binding agent,C.

以1-氨基-2-苯氧基-4-羟基蒽醌、氯磺酸、氯化亚砜、3-乙氧基丙胺为原料及Na2CO3为缚酸剂合成了C.I。分散红92。

Some preparation methods of galanthanime including extraction and organic synthesis were summarized, such as extraction from narcissus, galanthus woronawii losink, and lycoris radiate and countereurrent chromatography refining, and enzymatic extraction from hyacinths orientalis, as well as the organic synthesis using 3,4-dimethoxybenzaldehyde, methyl 3,4,5-trihydroxybenzoate, isovanilin and tyramine as raw material.

概述了加兰他敏从黄水仙、沃氏雪花莲中提取、石蒜中提取及逆流色谱法精制、喇叭水仙酶法中提取的方法、工艺;以3,4-二甲氧基苯甲醛、3,4,5-三羟基苯甲酸甲酯和异香草醛和酪胺为起始原料合成加兰他敏的方法。

The results showed that there were 8 kinds of aliphatic, 5 kinds of esters, 2 kinds of aldehydes, 2 kinds of nitrogen sulfur heterocyclic rings and one kind of hydrocarbon, alcoholics, ketone, lactones respectively in the analyzed 21 kinds of aroma components, and the content of furfural,β-methyl valeric acid, palmitic acid, nicotine, neohytadiene were higher, next were acetyl ethyl propionate, caleric acid, phenyl ethyl acetate, hydroxylic diethyl succinate.

结果表明,在分析出的21种香气成分中,分别有脂肪酸类8种,酯类5种,醛类2种,氮硫杂环类2种,烃类、醇类、酮类、内酯类各l种,其中相对含量较高的物质成分是糠醛、β-甲基戊酸、十六碳酸、烟碱、新植二烯,其次是乙酰丙酸乙酯、异戊酸、苯乙酸乙酯、羟基丁二酸二乙酯等。

Resveratrol(trans-3,4',5-trihydroxystilbene) is a phytochemical which was synthesized in various plant species such as grapes, Veratrum and Polygonum cuspidatum.

白藜芦醇,化学名称为3,5,4'-三羟基反苯二烯,是一种主要存在于葡萄、藜芦、虎杖等植物中的多酚类化合物。

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