羟基苯

IR studies of Co metal ion complexes with salicylaldehyde benzoyl hydrazone in solid state brings out the deprotonation of phenol in the formation of Co in pH 5—6 solution.On the contrary,the phenol is protonated in the formation of Co 2 in pH 8—10 solution,which is the same as the result of Zn 2 formation.

水杨醛苯甲酰腙钴络合物在固态的红外光谱分析表明，p H约 5— 6时，生成的络合物Co中的酚羟基脱质子，当 p H控制在 8— 10时，生成的络合物 Co 2 酚羟基质子化，即酚羟基未脱除质子，与络合物 Zn 2 的 IR结果相同。

It includes the following steps: polymerizing 2, 4-dihydroxyl metaphenylene diamine hydrochloride, diamine monomer and dipic acid anhydride to gain the polyimide that contains hydroxy on the molecule chain, making the hydroxyl take esterification reacting with acyl chloride and acrylic acid to gain polyimide photosensitive material that has negative photonasty.

该聚酰亚胺光敏材料以2，4-二羟基间苯二胺盐酸盐，二胺单体和二酸酐为原料进行聚合，得到分子链上含羟基的聚酰亚胺，然后使羟基与丙烯酸及其衍生物的酰氯发生酯化反应，得到具有负性感光性能的聚酰亚胺光敏材料。

A novel liquid crystalline compound named p-phenylenediamine di 4-[2- benzamide] was synthesized from allyl 2-hydroxyethylether, ethyl 4-hydroxybenzoate and p-phenylenediamine.

以乙二醇单烯丙基醚、对羟基苯甲酸乙酯、对苯二胺为原料合成了末端为不饱和双键的芳香聚酰胺溶致型液晶化合物——二对烯丙氧基乙氧基苯甲酰对苯二胺，最佳合成的摩尔比为∶羧酸∶对苯二胺∶吡啶=2。

First,from molecular aspect,a novel copolymer-PPBES has successfully been synthesized by nucelophilic substitution reaction with biphenol,4-(4-hydroxyphenyl)-phthlazin-1(2H)-one and 4,4\'-dichlorodiphenylsulfone,which has both twisted and linear molecular structures in the backbone.

本文从分子设计出发，首先选用联苯二酚与4-(4-羟基苯基)-2，3-二氮杂萘-1-酮和4，4′-二氯二苯砜为共聚单体，采用溶液亲核取代逐步缩聚合方法，合成了一系列含有杂萘联苯结构和联苯结构的新型共聚芳醚砜。

As compared to isop, the coexistence of electron-donating -OH,-C(CH_3_3 or electron-withdrawing groups (-NO_2) groups in the dicarboxylate derivatives has a significant effect on the molecular self-assembly.

同间苯二甲酸相比较，含有取代基的5-羟基间苯二甲酸、5-硝基间苯二甲酸和5-叔丁基间苯二甲酸在一定程度上影响着配位聚合物的自组装。

A method for the preparation of microcellular elastomeric polyurethane foams from a reaction mixture comprising a polyisocyanate component containing at least 85% by weight of 4,4'-diphenylmethane diisocyanate or a variant thereof, a polyol composition comprising at least one polyoxyalkylene polyol having an average nominal hydroxyl functionality of from 2 to 6, an average hydroxyl equivalent weight of at least 1300 and an average oxyethylene content of between 50 and 85% by weight, water, a chain extender having an average hydroxyl equivalent weight of from 15 to 250 and optionally a crosslinking agent, the hardblock-content being more than 45% by weight.

本发明是有关一种制备微孔弹性聚氨基甲酸酯泡沫体的方法，其反应混合物包括：一种含至少85重量％的4，4′－二苯甲烷二异氰酸酯或其变体的聚异氰酸酯组分，一种多元醇组合物，其包含至少一种平均标称羟基官能度从2至6、平均羟基当量至少1300且平均氧乙烯含量介于50至85重量％之间的聚氧亚烷基多元醇，水，一种平均羟基当量为15至250之增链剂，以及视需要使用的交联剂，该硬性嵌段－含量（hardblock-content）大于45重量％。

Professional sales companies operating bromide products: sodium bromide, sodium bromide, potassium bromide, potassium bromate, Tetrabromobisphenol A, Deca-BDE, ten PBDEs, DBDPE, hexabromodiphenyl Central dodecane, dibromo neopentyl glycol, neopentyl bromide three alcohols, three bromine phenol, octabromodiphenyl ether, brominated polystyrene, bromide, calcium bromide, dibromo succinic acid, dibromo-D ene glycol, bromide surfactants series: Dodecyl trimethyl ammonium bromide, tetradecyl trimethyl ammonium bromide, cetyltrimethyl ammonium bromide, octadecyl trimethyl ammonium bromide dodecyl trimethyl ammonium chloride, tetradecyl trimethyl ammonium chloride, cetyl trimethyl ammonium chloride, octadecyl trimethyl ammonium chloride, tetrabutyl ammonium bromide wholesale sales: dimethylolpropionic acid, DL-malic acid, isophthalic acid PIA, glycolic acid, adipic acid.

公司专业经营销售溴化物系列产品：溴化钠、溴酸钠、溴化钾、溴酸钾、四溴双酚A、十溴二苯醚、十溴联苯醚、十溴二苯乙烷、六溴环十二烷、二溴新戊二醇、三溴新戊醇、三溴苯酚、八溴醚、溴化聚苯乙烯、溴化铵、溴化钙、二溴丁二酸、二溴丁烯二醇、溴化表面活性剂系列：十二烷基三甲基溴化铵、十四烷基三甲基溴化铵、十六烷基三甲基溴化铵、十八烷基三甲基溴化铵、十二烷基三甲基氯化铵、十四烷基三甲基氯化铵、十六烷基三甲基氯化铵、十八烷基三甲基氯化铵、四丁基溴化铵批发销售：二羟甲基丙酸、DL-苹果酸、间苯二甲酸 PIA、羟基乙酸、己二酸。

Ib was synthesized by condensation of phthalic anhydride with 2-methylresorcinol in fused AlCl〓/NaCl (5∶1), followed by selective acetylation, methylation, NBS bromination and condensation with sodium ethoxide.

邻苯二甲酸酐在熔融的三氯化铝-氯化钠(5：1)中和-2，6-二羟基甲苯环合得1，3-二羟基-2-甲基蒽醌〓后经选择性乙酰化、甲基化、NBS溴化、乙醇钠缩合得1-甲氧基-2-乙氧甲基-3-羟基蒽醌。

They were two new compounds, [cyclo(Pro-Val-Phe-Phe-Pro-Val-Phe-Ser-Leu),7],[2-N-(1-methoxycarbonylethyl)guanosine, 10], and eight known compounds,(p-hydroxybenzoic acid, 1),(methyl succinate, 2),(russulaceramide, 3),(phenylalanine, 4),(guanine, 5),(β-carboline, 6),(uridine, 8), and (adenosine, 9). All the compounds were isolated from Amanita exitialis for the first time.

分别为：对羟基苯甲酸(p-hydroxybenzoic acid，1)、丁二酸二甲酯(methyl succinate，2)、神经酰胺(russulaceramide，3)、苯丙氨酸（phenylalanine，4）、鸟嘌呤核苷(guanine，5)、β-咔啉(β-carboline，6)、环（脯氨酸-缬氨酸-苯丙氨酸-苯丙氨酸-脯氨酸-缬氨酸-苯丙氨酸-丝氨酸-亮氨酸） [cyclo(Pro-Val-Phe-Phe-Pro-Val-Phe-Ser-Leu)，7]、尿嘧啶核苷(uridine，8)、腺嘌呤核苷(adenosine，9)、2-N-(1-甲氧羰基乙基)鸟苷[2-N-(1-Methoxycarbonylethyl)guanosine， 10]。10个化合物均为首次从致命鹅膏中分离得到，其中化合物7和10为新化合物。

By utilizing three benezenemulticarboxylate derivatives (H2chdc, H2aip, NaH2sip), we obtain 12 coordination polymers. Especially, compelexes 1 and 2 are based on one-dimensional ···OHInOHIn···chains as building units, while complex 3 is based on double four-ring [In8(μ2-O)4(μ2-H2O)8]16+, complex 4 is based on trinuclear In3(μ3-O)(CO2)6, complexes 11 and 12 are both based on nested bistranded helices.

选择了三类取代苯羧酸配体： 2，5-二羟基-1，4-对苯二甲酸(2，5-H2chdc)； 5-氨基间苯二甲酸(5-H2aip)； 5-磺酸基间苯二甲酸钠盐(5-NaH2sip)和InCl3反应合成了十二个配位化合物：其中1、2以···OHInOHIn···链为构筑单元， 3以双四元环[In8(μ2-O)4(μ2-H2O)8]16+为构筑单元，4以棱柱状三核铟In3(μ3-O)(CO2)6为构筑单元，而11、12以嵌套的双股螺旋链为构筑单元。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。