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Some preparation methods of galanthanime including extraction and organic synthesis were summarized, such as extraction from narcissus, galanthus woronawii losink, and lycoris radiate and countereurrent chromatography refining, and enzymatic extraction from hyacinths orientalis, as well as the organic synthesis using 3,4-dimethoxybenzaldehyde, methyl 3,4,5-trihydroxybenzoate, isovanilin and tyramine as raw material.

概述了加兰他敏从黄水仙、沃氏雪花莲中提取、石蒜中提取及逆流色谱法精制、喇叭水仙酶法中提取的方法、工艺;以3,4-二甲氧基苯甲醛、3,4,5-三羟基苯甲酸甲酯和异香草醛和酪胺为起始原料合成加兰他敏的方法。

The Surface composition of grafted PET fiber was characterized by ATR-FTIR. THE results showed that there were no obvious differences between ungrafted and graft PET fiber in the spectra ,except that the typical peak of-OH in 3100cm~(-1) appeared in both Citric acid treated PET fiber and Acrylic acid treated PET fiber indicated citric acid and acrylic acid had been successfully grafted on the surface of PET fiber.

对样品的接枝效果进行红外光谱表征,发现无论是经过丙烯酸接枝处理,还是柠檬酸接枝处理,处理前后纤维的红外吸收光谱图都没有明显的区别,说明接枝前后纤维的主体性质没变,但是,二者在3100cm~(-1)处都出现了羟基的特征吸收峰,说明柠檬酸和丙烯酸都已经接枝上了PET纤维表面。

ConclusionThe HCPT-SSLN has high entrapment efficiency and drug loading, uniform particle size, good stability, which provides an extensive prospect for clinical application of HCPT.

结论所制备的HCPT-SSLN包封率和载药量较高,粒径分布均匀,稳定性良好,为羟基喜树碱的临床应用提供了更广阔的前景。

The silicone rubber based on PDM-MVS/PMMA blend had microphase-separated structure consisting of PMMA domains uniformly dispersed within a continuous PDM-MVS matrix.

结果表明,随着PDM-MVS中乙烯基质量分数的增加,共混物的黏度逐渐增大;由PDM-MVS/PMMA共混物制备硅橡胶的物理机械性能明显优于α,ω-羟基聚二甲基硅氧烷/PMMA共混物制备的硅橡胶;制得的硅橡胶具有微观相分离结构,PMMA分散相均匀地分布于PDM-MVS连续相中,两相的相容性良好。

In DMSO, the polymerization of methyl methacrylate could be carried out efficiently. However the photopolymerization was inhibited in acetonitrile. It was ascribed to the complex formed between coumarin 1 and HTIB photolyzed to unreactive species after irradiation in acetonitrile.

在一般极性溶剂中如DMSO中能有效地引发甲基丙烯酸甲酯光聚合,而在电子受体性质的极性溶剂如乙腈中,光聚合反应受阻,这归结于香豆素1与羟基苯基碘鎓盐形成络合物,使得光反应后生成不具活性的产物。

The array consisted of 8 piezoelectric crystal sensors, each coated with an adsorptive material with unselective, but different response characteristics. The frequency shift data obtained from the array as the response to mixed vapour of common organic solvents of small molecular size were treated by using stepwise discrimination analysis, and five coatings that provided the maximum level of analyte discriminating ability were selected. The array constructed from these solvents was applied to recognizing alcoholic hydroxyl, carbonyl from other organic functional groups. The principal component analysis was applied to the original and autoscalled data. The two-dimensional display of the data showed well-defined clusters for solvents containing different functional groups separated from each other. The array was applied to identifying spirits and beverages.

该阵列由八个压电晶体传感器组成,每个传感器涂以具有广谱响应性能的不同吸附活性材料,阵列对常见小分子有机溶剂混合蒸气的响应频移数据采用逐步判别分析处理,选出五个供信能力最佳的判别变量,以此构成的阵列用于小分子有机溶剂混合蒸气中醇羟基、羰基与其它官能团的识别,并采用主成分分析法降维投影,在二维空间含相同官能团的物质聚为一类;阵列可用于酒类、软饮料的识别。

But urushiol has a poor resistance to alkali because phenol hydroxyl of urushiol shows weak acidity. Meanwhile, inherent brittleness of urushiol has limited its development and application.

但是,由于漆酚的酚羟基显弱酸性,使得漆酚耐碱性较差;同时,漆酚清漆固有的脆性等也限制了其发展和应用。

UFP/MPA/TiO2 nanocomposite coating was prepared with urushiol formaldehyde polymer and multihydroxyl polyacrylate via sol-gel process. Its structure and dynamic mechanical properties were characterized by PT-IR, TEM and DMTA. The physico-mechanical and ultraviolet resistant properties of the coating film were also investigated.

采用Sol-Gel法制备了漆酚缩甲醛聚合物/多羟基丙烯酸树脂/TiO2纳米复合涂料(UFP/MPA/TiO2),并用透射电镜、动态机械热分析、红外光谱和其它手段对复合涂膜进行测试。

The results showed that there were 8 kinds of aliphatic, 5 kinds of esters, 2 kinds of aldehydes, 2 kinds of nitrogen sulfur heterocyclic rings and one kind of hydrocarbon, alcoholics, ketone, lactones respectively in the analyzed 21 kinds of aroma components, and the content of furfural,β-methyl valeric acid, palmitic acid, nicotine, neohytadiene were higher, next were acetyl ethyl propionate, caleric acid, phenyl ethyl acetate, hydroxylic diethyl succinate.

结果表明,在分析出的21种香气成分中,分别有脂肪酸类8种,酯类5种,醛类2种,氮硫杂环类2种,烃类、醇类、酮类、内酯类各l种,其中相对含量较高的物质成分是糠醛、β-甲基戊酸、十六碳酸、烟碱、新植二烯,其次是乙酰丙酸乙酯、异戊酸、苯乙酸乙酯、羟基丁二酸二乙酯等。

N L-Leucine Producer,Strain No .145,was obtained from mutants resistant to α-amino-β-hydroxyl valeric acid and rifampin by mutagenizing Brevibacterium Tianjinese T6-13 with ul-traviolet rays,It produced L-Leucine up to 32mg/mL on shaker and 21.8mg/mL of L-Leucine was produced in 16 liter fermentor in 60 hours.

以天津短杆菌T6~13为出发菌株,采用紫外线进行诱变处理,筛选α-氨基-β-羟基戊酸和利福平抗性突变株,获得一株L-亮氨酸产生菌No.145,L-亮氨酸摇瓶产量可以达32.1mg/mL。在16L发酵罐中培养60h,L-亮氨酸产量可以达21.8mg/mL葡萄糖转化率可以达20%。

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This one mode pays close attention to network credence foundation of the businessman very much.

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Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

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