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Hydroxyl octanoic acid(1) was synthesized from heptaldehyde by a four-step reaction of nucleophilic substitution,displacement reaction,acid hydrolysis and deaminization.

以正庚醛为原料,经过亲核取代、置换反应、酸水解及碱化脱氨等4步反应合成了制备3,6-二己基-1,4-二氧杂-2,5-二酮的中间体——α-羟基辛酸(1);1经对甲苯磺酸催化脱水得辛交酯。

The blend has following properties with 10 parts compatibilizer. The tensile intensity and elongation at break reach 35.66MPa and 23.58%, respectively, improving by 26.6% and 65.7% respectively compared with 0 part compatibilizer; The characteristic absorption peak of carbonyl at 1725~1800cm-1 disappear and the characteristic absorption peak of hydroxide at 3438~3440cm-1 increase induce the formation of hydrogen bond; The decalescence peak of blend increase by 2℃compared with the blend containing 0 part compatibilizer near 100℃; Lignin can be dispersed homogeneously to avoid reuniting of lignin particle.

2当共混材料中增容剂含量为10份时,共混材料表现出如下特性:拉伸强度和断裂伸长率分别达到35.66MPa及23.58%,较未加增容剂分别提高了26.6%和65.7%;从1725~1800cm-1范围内羰基特征吸收峰接近消失以及3438~3440cm-1范围内的羟基波数的增加暗示了共混材料中氢键缔合的发生;共混物在100℃附近的吸热峰较未加增容剂时降低了近2℃,相容性得到了提高;木质素在基体中进一步分散,结晶度增加,从而阻止木质素的团聚,增加了两相的相容性。

Part 4: Synthesis of (5α)-3-Hydroxy-18-Nor-C-Homo-13a-Azaandrostanes 1-Azabicyclo [5, 3, 0] decane (6) is a core skeleton of stemonine (7) and its derivatives, which are a group of bio-active natural products.

四、(5α)-3-羟基-18-nor-C-homo-13a-氮杂雄甾烷的合成 1-氮杂双环[5.3.0]癸烷(6)是天然产物百部生物碱(7)类分子的骨架结构,许多该类化合物都具有重要的生物活性。

Chapter two 4-Hydroxybenzoic acid is connected with PEG6000 through defoliant DCC at rooom temperature, then the product is refluxed with chloroacetic acid in acetone to afford PEG-bound phenyloxyacetic acid, which is reacted with thionyl chloride, ammonium thiocyanate and arylamines in turn to give PEG-bound disubstituded thioureas. After the cleavage with sodium methoxide in methanol, the eleven disubstituted thioureas are obtained.

第二章 利用PEG6000作载体,通过脱水剂DCC在室温下将对羟基苯甲酸以酯键连接在PEG6000上,再与氯乙酸在较温和的条件下生成PEG6000支载的芳氧乙酸,然后,依次与亚硫酰氯、硫氰酸铵、芳胺反应,生成PEG6000支载的硫脲,最后用甲醇钠的甲醇溶液切割PEG,得到了十一种1,3-二取代硫脲。

There were only a few complications such as postoperative dehiscence of bulber conjunctiva and part exposure of the implants.

眶内二期羟基磷灰石义眼台植入术,是眼球丧失后疗效较好的眼眶充填手术。

The yeast generating MT can antagonize ultraviolet ray and cobalt 60 radiation, eliminate hydroxyl free radicals and detoxicate heavy metals.

产MT酵母菌具有拮抗紫外线、60Co辐射、消除羟基自由基和重金属解毒能力。

In addition, when the modified PVA resins fulfilled requirements in the following: 1 the acetalization degree varied from 60 mol% to 80 mol%, 2 the esterification degree varied from 10 mol% to 20 mol%, 3 the amount of hydroxyl group was 5-25 mol%, 4 the range of value of B/P(the mass ratio of the binder to diazo resin) was from 4 to 4.5,5 the range of its molecular weight was from 4×10^5 to 8×10^5, the negative PS plate obtained had excellent sensitivity, hydrophobic property, good developability, good ink receptivity and good scratch resistance.

因此其分子量、酯化度和缩醛度的确定,必须综合考虑各项性能之间的平衡。缩醛度为60-80 mol%,酯化度10-15mol%,羟基5-25 mol%,分子量约为4-8万,B/P为4-4.5时,制得的阴图PS版的感度、显影性、着墨性和耐磨性都较好。

This diad or model compound (FL4) is adsorbed on TiO_2 colloid through the phenolic function of the fluorescein moiety.

发现荧光素蒽醌甲酯与荧光素丁酯均可通过酚羟基较好地吸附在TiO_2胶体上。

The title compound showes weak semiconducting behaviors diamagnetism.

本文报道了8-羟基喹啉与H6As2Mo18O62形成的电荷转移盐的合成、结构和性质。

A water soluble polyhydroxy derivative of1,4| diazine has been isolated from Panax pseudoginseng var notoginseng for the first time.

从三七水溶性成分中首次分离得到一个多羟基吡嗪衍生物。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。