羟基

It showed that the yield of hydroxyacetic acid reached above 99.5%, the extracting efficiency was over 97%,and the product with purity of more than 96% was obtained. Extractant and solvent also can be reused.

实验结果表明：羟基乙酸合成的反应产率达99.5%以上，羟基乙酸萃取率达97%以上，最终收率达96%，萃取剂与溶剂均可循环使用。

Those biodegradable materials finally form into CO2 and H2O via culture of tricarboxylic acid cycle, which can be excreted from lung, kidney, and skin. Hydroxyacetic acid is a metabolic product of amino acids. Therefore, velocity of bioldegradable materials can be controlled in vivo. The recent contraception focuses on discover a sustained release system of biodegradable materials.

生物可降解材料包括聚乳酸、聚ε-己内酯、乳酸-羟基乙酸共聚物等，这些材料有很好的生物相容性，植入体内后可经生物降解成乳酸单体，经三羧酸循环后最终成为CO2和H2O，经肺、肾、皮肤排泄，羟基乙酸也是机体氨基酸代谢产物，而且生物可将解材料在体内降解速度是可控的，用生物降解聚合物作为药物载体的缓释避孕系统是目前材料学以及避孕节育研究的一大重点。

Toxicity and species difference are the other problems of CPTs. Homocamptothecins , a novel CPT analog which contain an expanded seven-membered β-hydroxylactone, have shown elevated antitumor activity and improved stability without species difference.

高喜树碱是近年来刚刚出现的一类CPT类似物，其特征是将α—羟基内酯环改造成七元的β—羟基内酯环，不仅活性明显提升，而且体内代谢稳定性也大大提高，并且不存在种属差异现象。

The recombinant hygrophilous aeromonad producing copolymer PHBHHx of HB and HHx contains beta-keto thiolase gene phhA and acetoacetyl-CoA reductase gene phhB.

本发明公开了一株产3-羟基丁酸和3-羟基己酸的共聚物PHBHHx的重组嗜水气单胞菌及其构建方法与应用。

Xinquan HuTwo new chiral backbones R-- and S--2-amino-2"-hydroxy-4,4",6,6"-tetra methyl-1,1"-biphenyl were synthesized via nitration, diazotation/iodination, Ulhnann coupling, selective reduction, diazotation/hydrolysis, hydrogenation and resolution from 2,4-dimethyl-aniline in seven steps.

以2，4-二甲基苯胺为起始原料，经过硝化反应、重氮化碘代反应、Ullmann缩合反应、选择性双硝基单还原反应、重氮化水解反应、催化氢化反应和拆分，首次合成了--2-氨基-2'-羟基-4，4'，6，6'-四甲基-1，1'-联苯和--2-氨基-2'-羟基-4，4'，6，6'-四甲基-1，1'-联苯两个对映体。

Racemic backbones 2-amino-2'-hydroxy-6,6'-dimethyl-l,l'-biphenyl la and 2-amino-2'-hydroxy-4,4',6,6'-tetramethyl-l,1'-biphenyl 1b were synthesized from o-methylaniline and 2,4-dimethylaniline via nitration, diazotation/iodination, Ullmann coupling, selective reduction, diazotation/hydrolysis and hydrogenation.

从邻甲苯胺及2，4-二甲基苯胺出发，经过硝化，重氮化-碘代，偶联，单还原，重氮化-水解及还原反应合成了消旋体骨架2-氨基-2'-羟基-6，6'-二甲基-1，1'-联苯1a和2-氨基-2'-羟基-4，4'，6，6'-四甲基-1，1'-联苯1b。

Results:From the extraction of 95% in the green peel of Juglans Mandshurica,we got five compounds,which were respectively:β-sitosterol;juglone;3,5-dimethoxy-4-hydroxybenzoic acid;regiolon;succinic acid 4-oxyethyl-5-hydroxide-β-tetralone;...

结果：从核桃楸的乙醇提取物中分离鉴定了5个化合物，分别是：β-谷甾醇；胡桃醌；3， 5-二甲氧基-4-羟基苯甲酸；regiolon；琥珀酸；4-乙氧基-5-羟基-β-四氢萘酮；胡桃酮。结论：化合物Ⅲ、Ⅶ、Ⅵ为首次从核桃楸青皮中分离得到，Ⅶ、Ⅵ为新的天然化合物。

A method combining HPLC, a post-column derivation device and a fluorescent detector was used to determine residues of ten carbamate pesticides （aldicarb sulfoxide, aldicarb sulfone, oxamyl, methomyl, 3-hydroxy carbofuran, aldicarb, propaxur, carbofuran, carbaryl and methiocarb） in 68 vegetable and 32 soil samples under four different cultivation systems （traditional kailyard, open field vegetable base, green house and paddy） were collected from a certain city in South Jiangsu.

本研究采用高效液相色谱-柱后衍生-荧光检测法分析了苏南某市4种不同种植方式下（传统菜地、露天蔬菜基地、大棚蔬菜基地和水稻田）68个蔬菜样品和32个土壤样品中10种N-甲基氨基甲酸酯类农药（涕灭威、涕灭威砜、涕灭威亚砜、杀线威、灭多威、残杀威、克百威、3-羟基克百威、甲萘威和灭虫威）的残留量，结果表明在蔬菜中检出的氨基甲酸酯农药残留水平多处于0.2～23μgkg^-1，土壤中为0.1～10μgkg^-1；土壤中3-羟基克百威和灭虫威全部检出，其最高检测浓度分别为10μgkg^-1和1.64μgkg^-1，其他农药仅有少数检出。

The blue crosslinking polymeric dyes were synthesized with use of leucoquinizarin and polyvinylamine prepared from the Hofmann degradation of polyacrylamide. The maximum wave length was 597nm. The effects of temperature, the concentration of amino group, the pH value and the mole ratio of leucoquinizarin to amino group on the yield of red crosslinking polymeric dye were discussed.

以具有不同聚合度和不同胺化度的聚乙烯胺为骨架，以1，4—二羟基蒽醌隐色体为原料合成了蓝色可交联高分子染料，该染料的最大吸收波长为597nm，研究了反应温度、氨基浓度、pH值以及1，4—二羟基蒽醌隐色体与聚乙烯胺中氨基的摩尔比对反应的影响。

These compounds were identified as follows:chrysophanol (FP-1),physcion(FP-2),eriosematin(FP-3),scoparone(FP-4),lupeol(FP-5),betulinic acid(FP-6),3\',4\'-Dihydroxy-trans-cinamic acid octacosyl ester(FP-7),β-sitosterol (FP-8),flemiphilippinone A(FP-9),monopalmitin(FP-10),emodin(FP-11),islandicin (FP-12),salicylic acid(FP-13),p-methoxyphenylpropionic acid(FP-14),trideca-1, 3-diene(FP-15),lupinifolin(FP-16),flemichin D(FP-17),flemiphilippinin A(FP-18), auriculasin(FP-19),erythrinin B(FP-20),6-C-prenylluteolin(FP-21), 8-(1,1-dimethylallyl) genistein(FP-22),flemiphilippinin E(FP-23),flemiphilippinin F (FP-24),5,7,3\',4\'-tetrahydroxy-6,8-diprenylisoflavone(FP-25),flemiphilippinin D (FP-26),dorsmaninsⅠ(FP-27),osajin(FP-28),6,8-diprenyleriodictyol(FP-29), lupinalbin A(FP-30),genistein(FP-31),3\'-O-methylorobol(FP-32),orobol(FP-33), 5,7,2\',3\',4\'-pentahrdroxyflavone(FP-34),the mixture of biochanin A and prunetin (FP-35 and 36),genistin(FP-37),sophororicoside(FP-38),3\'-O-methylorobol-7-glucoside(FP-39),the mixture of sissotrin and prunetin 4\'-O-β-D-glucoside(FP-40 and 41),adenosine(FP-42) and luteoloside(FP-43,mixture).

这些化合物分别为大黄酚(FP-1)、大黄素甲醚(FP-2)、eriosematin(FP-3)、滨蒿内酯(FP-4)、羽扇豆醇(FP-5)、白桦酸(FP-6)、咖啡酸二十八烷酯(FP-7)、β-谷甾醇(FP-8)、蔓性千斤拔酮A(FP-9)、单棕榈酸甘油酯(FP-10)、大黄素(FP-11)、islandicin(FP-12)、水杨酸(FP-13)、对甲氧基苯丙酸(FP-14)、十三烷-1，4-二烯烃(FP-15)、lupinifolin(FP-16)、千斤拔素D(FP-17)、蔓性千斤拔素A(FP-18)、auriculasin(FP-19)、erythrinin B(FP-20)、6-C-异戊烯基木犀草素(FP-21)、8-(1，1-二甲烯丙基)-染料木黄酮(FP-22)、蔓性千斤拔素E(FP-23)、蔓性千斤拔素F(FP-24)、5，7，3′，4′-四羟基-6，8-双异戊烯基异黄酮(FP-25)、蔓性千斤拔素D(FP-26)、dorsmaninsⅠ(FP-27)、osajin(FP-28)、6，8-双异戊烯基圣草素(FP-29)、lupinalbin A(FP-30)、染料木黄酮(FP-31)、3\'-O-甲基香豌豆苷元(FP-32)、奥洛醇(FP-33)、5，7，2′，3′，4′-五羟基黄酮(FP-34)、鹰嘴豆素甲和樱黄素的混合物(FP-35和FP-36)、染料木苷(FP-37)、槐属苷(FP-38)、7-葡萄糖基-3\'-O-甲基香豌豆苷(FP-39)、印度黄檀苷和樱黄素4′-O-β-D-葡萄糖苷的混合物(FP-40和FP-41)、腺嘌呤核苷(FP-42)和木犀草苷(FP-43，混合物)。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。