缩酮

In this research, two novel compounds in which alkylenedithiomethylene Malonic acid act as the main coordination agents and the compounds containing N atom (such as pyridine, Phenanthroline Ethanediamine and 4,4'-Bipyridinyl) act as the associating coordination agents have been synthesized by the means of solution and solid-liquid diffusing reactions. 9 coordination complexes and polymers have been designed and synthesized in which the transition metals Cu and Zn acted as the centre ions. These compounds have been characterized by X-ray single crystal diffraction analysis, and some properties of them have been tested and analyzed.

本论文设计合成了两种结构新颖的含有二硫缩烯酮结构的丙二酸类化合物，以此为主要配体，以含氮化合物(吡啶、邻菲罗啉、乙二胺和4，4'-联吡啶)为辅助配体，采用常规溶液合成和固-液相扩散等方法，设计合成了9个过渡金属Cu和Zn离子配合物和配位聚合物，采用单晶X-射线衍射等技术对晶体结构表征，并对其部分性质进行了测试和分析。

A new photochromic organic compound of thiosemicarbazone, 4-( p -bromo-α-methylaminothiocarbonyl hydrazonobenzal)-2,5-dihydro-3-methyl-5-oxo-1-phenyl pyrazole, was synthesized and characterized by elemental analyses, IR, 1H NMR spectra, and X-ray single-crystal diffraction analysis.

文章合成了一个新的有机化合物1-苯基-3-甲基-4-对溴苯亚甲基-吡唑啉酮-5 缩甲基氨基硫脲(1)，并分别用元素分析、红外光谱、氢核磁共振及X-射线单晶衍射对化合物的结构进行了确证和表征。

Studies on the Synthesis, Crystal Structures and Photochemical Photochemical Properties of Pyrazolone Thiosemicarbazones

论文标题：吡唑啉酮缩氨基硫脲类化合物的合成，晶体结构及光化学性质研究

In general, juice from ripe fruits contained higher total quantities of phenolic compounds, condensed tannins, flavonoids and scopoletin, and thus exhibiting better scavenging capacity for free radical, superoxide anion radicals and H2O2 and higher ACE inhibitory activity.

一般而言，成熟的诺丽果含有较高的总酚化合物、缩合单宁、类黄酮和7-羟－6-甲氧香豆素。因此具有较佳能力以扫除自由基、超氧阴离子和过氧化氢及较强ACE抑制力。

On the basis of previous work in our laboratory, several novel thiosemicarbazones and semicarbazone compounds containing pyrazolone-ring have been synthesized.

本文在实验室原有工作的基础上，合成了以吡唑啉酮环为变色主体的缩氨基脲、氨基硫脲类有机光致变色化合物，通过对固态光致变色性质和晶体结构的研究，深入分析了它们的变色机理，并总结了光致变色性质与之间结构的关系。

Because the limonene does not have a carbonyl group, the small amount of it which remainsin the carvone fraction will not form a semicarbazone derivative.

由于柠檬烯没有羧基，留在香芹酮馏份中少量的柠檬烯将不会产生缩胺基脲的衍生物。

3,6-Bis(1 H -1,2,3,4-tetrazol-5-yl-amino)-1,2,4,5-tetrazine was synthesized by triamino- guanidinium nitrate with 2,4-pentanedione of condensation, followed by oxidation and substitution reaction. The product was characterized by elemental analysis, IR, NMR and DSC.

以三氨基胍硝酸盐、戊二酮为起始原料，经缩合、氧化、取代等反应合成了3，6-双(1 H -1，2，3，4-四唑-5-氨基)-1，2，4，5-四嗪，并通过元素分析、红外、核磁、差示扫描量热法等分析手段对其进行了表征。

In this work,the non\|aqueous carbonyl nickel slips were prepared by ball\|milling using Cyclohexanone\|butyl alcohol,Glycerol trioleate,Poly\|vinyl\|butyl and polyethylene glycol as the solvent,dispersant,binder and plasticizer,respectively.

本文以环己酮丁醇为溶剂，三油酸甘油酯为分散剂，以聚乙烯醇缩丁醛为粘结剂，聚乙烯乙二醇为增塑剂，通过球磨工艺制备了非水基羰基镍粉浆料。

Based on our early work, we will discuss the coupling the reaction of α-cyano ketenedithioacetals with Baylis-Hillman adducts.

基于以上的研究，本文着重讨论了α-氰基二硫缩烯酮与Baylis-Hillman加成产物的偶联反应。

Fter different detraining cycles on the physiological performance, the detraining cycles will be reflected different degrees of impact. We found that the strength and endurance of athletes in detraining has reduced the capillary density, oxidative fibers, slow-twitch muscle. On the other hand, AVO2-diff, oxygen enzyme decline in the number of mitochondria, the change of muscle fiber types and reduced neuromuscular control in long-term detraining. In cardio-respiratory fitness, particularly in endurance athletes among blood flow, plasma volume, and cardiac output's decline are the most conspicuous. After hormone and metabolic's short term and long-term detraining, we found that growth hormone, testosterone, cortisol, respiratory exchange rate, showed a decline in insulin sensitivity, it will directly affect the exercises performance. Further more, the exercises performance and physiological benefits could have been completely eliminated.

bstract 不同周期停止训练后，对生理表现将反映出不同程度之影响，其中发现肌力性与耐力性运动员在短期停止训练后，毛细血管密度、氧化纤维、慢缩肌呈现减少情形；反观长期停止训练后，将会使动静脉血含氧差异(arterial-venous oxygen difference， AVO2-diff)、氧化酶粒腺体数目下降与肌纤维型态之改变，而减少神经肌肉控制能力、在心肺适能方面，尤以耐力性运动员在血流量、血浆量、每跳输出量、最大心输出量下降情形最明显；而贺尔蒙与代谢在短期与长期停止训练后，发现生长贺尔蒙(growth hormone， GH)、睪固酮、可体松、呼吸交换率、胰岛素敏感性均呈现下降情形，这些情形将直接影响其运动表现之发挥，甚至使先前获得之运动表现与生理效益完全消失。

I am accused of being overreligious," she said in her quiet, frank manner,"but that does not prevent me thinking the children very cruel who obstinately commit such suicide.""

客人们在卡罗利娜·埃凯家里，举止就文雅一些，因为卡罗利娜的母亲治家很严厉。

Designed by French fashion house Herm è s, this elegant uniform was manufactured in our home, Hong Kong, and was the first without a hat.

由著名品牌 Herm è s 设计，这件高贵的制服是香港本土制造，是我们第一套不配帽子的制服。