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A simple NACE method has been developed for the assay of Rutaecarpine in Evodia rutaecarpa for the first time. Optimum separation of the analytes was obtained using a nonaqueous buffer system with 40 mmol/L ammonium acetate containing 30% acetonitrile and 10% acetate acid.

考察了影响电泳分离的各因素如缓冲溶液的浓度、用于调节酸碱度的乙酸的添加比例及用于调节电渗流的乙腈的添加比例,最后优化的分离缓冲溶液的组成是40 mmol/L NH4Ac 的甲醇溶液,其中含有30%的乙腈和10%的乙酸。

A very large sample plug was introduced hydrostatically into the capillary (65 cm×50 μm i.d., effective length of 35 cm) over 80 s at a height difference of 11 cm. The working conditions for CE-FA separation are as follows: operating voltage, 10 kV; running buffer, 67 mmol/L phosphate, pH 7.4. The unbound ketoprofen concentration was directly measured from the height of the frontal peak.

一大体积样品虹吸进样至未涂层毛细管(65 cm×50 μm i.d。,有效长度35 cm),进样时间80 s,毛细管两端高度差11 cm,工作电压10 kV,运行缓冲液为67 mmol/L磷酸盐缓冲液(pH 7.4),游离酮洛芬浓度由前沿峰的高度直接测定。

The results of the CV study showed that the interaction was mainly of an electrostatic one in phosphate buffer solution at pH 4.4,whereas intercalative binding played a dominant role at pH 6.5 and 7.4 solutions.The results of the UV-Vis spectroscopic study further confirmed them.

电化学测量结果表明,在pH4.4的磷酸盐缓冲液中,AE与DNA之间以静电作用为主,而在pH6.5和7.4的磷酸盐缓冲液中,则以嵌入结合为主,紫外-可见吸收光谱也证明了这一结论。

Under isocratic elution condition including pH of the buffer solution, separation voltage and the ratio of organic solvent in the buffer solution.

首先以等位冲堤的方式,寻找最佳的实验参数,其参数包含缓冲溶液酸碱值,操作电压及有机修饰剂在缓冲溶液中的比例。

This paper investigated the effects of environmental factors, such as, pH, buffer capacity, the concentration of chloride ions and the concentration of nonaggressive anions, on the crevice corrosion potential E_(cc of Type 304 stainless steel. The E_c was ascertained by galvanodynamic polarization.

本实验主要研究pH 值、缓冲容量、氯离子浓度及其缓冲溶液中其它阴离子浓度等环境因素对304 不锈钢缝隙腐蚀电位的影响,缝隙腐蚀电位由动电位扫描确定。

Human pericardia from cadaeric donors were treated sequentially with hypotonic buffer, SDS in hypotonic buffer, and a nuclease solution.

将来自尸体供体的人类心包先后用低张缓冲液、加有SDS的低张缓冲液和核酸溶液处理。

The result shows that the structure of reformative package is simple than the old one, the cushion capability is better.

结果显示:改良后的手机内衬结构设计简单,缓冲性能较好,在节约材料的基础上增强缓冲性能。

The experiment results indicate that logarithmic growth phase,resuscitative buffer Ⅴ,electrotransfection buffer Ⅳ,23kv/cm and 200 resistance are regarded the best electrotransfection condition of Sinorhizobium meliloti.

结果表明细胞的对数生长初期、复苏缓冲液Ⅴ、电转缓冲液Ⅳ、23 kv/cm和200Ω适合作为苜蓿中华根瘤菌电转的条件。

In order to investigate the electrotransformation condition of Sinorhizobium meliloti variable curve was devised by different cell cycles time,resuscitative buffer,electrotransfection buffer,pulsed electric field and resistance.

为了研究苜蓿中华根瘤菌电转化的条件,通过对不同的细胞生长周期、复苏缓冲液、电转缓冲液、电场强度和电阻对电转率影响程度来作出变化曲线,以确定电转化的最优条件,从而提高苜蓿中华根瘤菌电转化率。

Commercial manufacturers will often use a low-molarity buffer so that the consumer can easily resuspend the conjugate in the buffer of his or her choice. Generally, high-salt buffers and surfactants should be omitted from the final storage buffer as they may cause damage by hydrolysis or displacement of the antibody.

最终储存用的缓冲液应避免使用高盐缓冲液和表面活性剂,因为它们可能水解或取代抗体。

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