结果为

The glyoxal and glyoxalic acid contents in the solution of oxidation of acetaldehyde to glyoxal by nitric acid were determined by this method, the repeatabilities of analysis results were excellent and the relative error compared to chemical analysis of glyoxal was 1.77%.

用HPLC测定乙醛硝酸氧化法制乙二醛反应液中乙二醛和乙醛酸的含量，结果的重复性好；对乙二醛的测定结果与应用化学分析法测定结果的平均相对误差为1.77%；对反应液中乙二醛、乙醛酸含量的测定有着较高的加标回收率，分别为99.6%～103.3%和98.1%～102.4%。

The aim of this study was to develop a novel amphiphilic functional block poly(ε-caprolactone) bearing ketone groups MPEG-b-P(OPD-co-CL. 2-oxepane-1, 5-dione was copolymerized with ε-caprolatone in which methoxy poly (MPEG, Mn=5 000) and stannous octoate were used as initiator and catalyst, respectively. The syntheses were conducted by bulk and solution polymerization. 1H NMR results showed that peak position and splitting of the polymers synthesized through solution polymerization were consistent with theoretical data, demonstrating the products were designed block copolymers. While in the bulk polymerization, polymer peak position was changed due to their high reaction temperature, suggesting their structural variation.

将带有羰基官能团的4-羰基己内酯和ε-己内酯分别在甲氧基聚乙二醇(MPEG，Mn=5 000)为引发剂，异辛酸亚锡为催化剂溶液和本体体系中开环聚合，合成了两亲性侧基带有羰基官能团的聚己内酯嵌段共聚物MPEG-b-P(OPD-co-CL.1H NMR结果表明采用溶液聚合法合成的聚合物各峰的峰位置和分裂情况与理论一致，证明了产物是实验所设计的嵌段共聚物，而采用本体聚合法合成的聚合物由于温度的影响，聚合物各峰的峰位置发生了变化，说明其结构发生了变化；差示扫描量热法分析结果表明随着OPD单体含量的增加，聚合物的熔点，玻璃化转变温度和熔融焓增加；热失重测试结果表明OPD单体的引入增加了聚合物的热敏感性。

The 352 valid samples were analyzed by SPSS. The results showed there was no distinct corresponding relationship between the product attributes and reaction time. The different key attributes from questionnaire importance rating and the shortest reaction time standards were used to regressively analyze the results of customers' overall rating (such as overall satisfaction,objective quality, recommend intention).The results indicated that the coefficiency of regression of the special attributes chosen from reaction time to overall rating was distinct, while the coefficiency of the special attributes chosen from importance rating to overall rating was not. The main conclusions are: 1. Regarded attributes can be obtained by the reaction time of brand performance rating.

本实验的有效样本为352个，通过SPSS软件进行分析统计，数据统计结果显示，在品牌表现评价反应时与其重要性问卷评定结果的相关系数的检验中，并未发现品牌表现评价反应时与品牌属性重要性评定结果之间的显著相关；将由问卷重要性评价最高标准所得到的关键属性与通过品牌表现评价反应时最短的标准所选取的关键属性的品牌表现分别对消费者的总体评价结果（如&总体满意度&、&主观质量&、&推荐意向&）进行回归分析，发现通过品牌表现评价反应时方法选取的特殊关键属性（与问卷重要性评定法选取不一致的关键属性）的品牌表现对总体评价结果的回归系数显著，而重要性评定问卷法选取的特殊关键属性（与品牌表现评价反应时法选取的不一致的关键属性）的品牌表现对总体评价结果回归系数不显著。

Under the optimum conditions of n: n=40, mass percentage of ZrO2 18%, temperature 400℃, m m=0.02 and reaction time 0.5 h, the conversion was 91.2% and the yield of liquid products was 83.6%. Compared with the results obtained by thermal pyrolysis and catalytic pyrolysis on HZSM-5, ZrO2/Ti-MCM-41 was of better catalytic activity and higher yield of liquid products, and was especially suitable for the pyrolysis of sterically hindered polymers such as PP.

结果表明，n：n=40，ZrO2负载质量分数为18%的ZrO2/Ti-MCM-41，在反应温度400℃，m(ZrO2/Ti-MCM-41)：m=0.02，反应时间30min的条件下，PP的转化率可达91.2%，液体产物的收率为83.6%，该结果优于热裂解及传统的HZSM-5小孔分子筛催化剂的催化裂解结果。

The transition from the systemic inflammatory response syndrome to seere sepsis and septic shock inoles a myriad of pathogenic changes, including circulatory abnormalities that result in global tissue hypoxia.1,2 These pathogenic changes hae been the therapeutic target of preious outcome studies.12 Although this transition occurs oer time, both out of the hospital and in the hospital, in outcome studies interentions hae usually been initiated after admission to the intensie care unit.12 In studies of goal-directed hemodynamic optimization, in particular, there was no benefit in terms of outcome with respect to normal and supranormal hemodynamic end points, as well as those guided by mixed enous oxygen saturation.9,13 In contrast, een though we enrolled patients with lower central enous oxygen saturation and lower central enous pressure than those studied by Gattinoni et al.9 and with a higher lactate concentration than those studied by Hayes et al.,13 we found significant benefits with respect to outcome when goal-directed therapy was applied at an earlier stage of disease.

从全身炎症反应综合征转为严重脓毒症和脓毒性休克牵涉大量发病的变化，包括导致全身性缺氧的循环紊乱。这些发病的变化成为先前结果研究的治疗学目标。尽管这些转变随着时间的流失而逐渐出现，既可以在院外，也可在院内，在结果研究中，干预措施往往在进入ICU之后才启动。特别的，在那些目标导向血流动力学最优化研究中，依照结果，那些以正常或超正常血流动力学为终点的措施未能显示出益处，以混合静脉血氧饱和度为导向的研究同样如此。

EDS and Surface-profile results indicate that the stoichiometries of all the samples approach 2:3 and the thicknesses are over 500nm. XRD results indicate that the major diffraction peaks of the film match those of Bi2Te3.The film growth exhibits preferred orientation at (015) phase and many Bi, impurity peaks are observed. Hall and Seebeck coefficient measurement reveals that all the samples are n-type with the carrier density of 10^23cm^-3 and conductivity of 10^-5Sm^-1 which confirm the samples have nice thermoelectrically properties.

能谱分析和台阶仪测量结果显示本文所制备的薄膜Bi：Te原子比接近2：3，厚度都大于500nm；XRD测量结果显示薄膜的主要衍射峰与Bi2Te3标准衍射峰相同，在（015）晶面上择优选向明显，有少量的Bi、杂质峰存在；霍尔系数测试及Seebeck系数测量结果显示，薄膜都为n型半导体薄膜，载流子浓度量级为10^23cm^-3，电导率量级10^-5Sm^-1，具有良好的电学性能。

To verificate the correctness and reliability of the simulation system, a typical processing of 3 rollers stretch reducing of tube is simulated by simulation system of 3D Thermo-mechanical Couple rigid-plastic FEM.

为验证作者开发的&钢管张力减径三维热力耦合刚塑性有限元虚拟仿真集成系统&的正确性和可靠性，对典型的三辊张力减径过程进行了模拟，并将模拟结果与产品实测结果进行对比，结果证明了采用有限元模拟技术能够为钢管张力减径工艺制度制定和轧辊孔型优化提供依据。

Characteristics of Ten-Roll Tube Straightener;2. Ultimate strength of short steel tube-confided concrete;3. To verificate the correctness and reliability of the simulation system, a typical processing of 3 rollers stretch reducing of tube is simulated by simulation system of 3D Thermo-mechanical Couple rigid-plastic FEM.

为验证作者开发的&钢管张力减径三维热力耦合刚塑性有限元虚拟仿真集成系统&的正确性和可靠性，对典型的三辊张力减径过程进行了模拟，并将模拟结果与产品实测结果进行对比，结果证明了采用有限元模拟技术能够为钢管张力减径工艺制度制定和轧辊孔型优化提供依据。

It is pointed that the parabola method is straightforward, but the results are relatively coarse, and the catenaries method is relatively complicated, but the results are precise, which takes into account all-around factors.

结果发现：抛物线法比较简单，但计算结果比较粗略；分段悬链线法考虑因素比较全面，计算相对复杂，但结果比较精确；对于空缆线形竖向坐标值两种方法的误差为0 739%，无应力索长计算两种方法的误差仅为0 31%。

Result junior high school male, schoolgirl overweights occurence rate is respectively 10.03%, 9.55%, fat occurence rate is respectively 5.32%, 3.04%, BMI of male, schoolgirl evaluates junior high school of Fen in relief city overweight result and standard of height standard weight are uniform, evaluate fat result under law of height standard weight.

结果初中男、女学生超重发生率分别为10.03%，9.55%，肥胖发生率分别为5.32%，3.04%，汾阳市初中男、女学生BMI评价超重结果和身高标准体重法一致，评价肥胖结果低于身高标准体重法。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了