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In the condition of various treatment of phosphorus adding levels 0.06%,0.12%,0.18%,0.24%,biological value of dicalcium phosphorus were as follows,respectively:100,109,112,115 when body weight gain was employed as response criterion;100,102,94,89 when ratio of phosphorus retention employed;100,116,130,139 when bone ash content (the average of tibia ash and toe ash) employed and 100,114,132,133 when serum phosphorus level employed.

结果表明:在日粮磷添加水平分别为0.06%,0.12%,0.18%,0.24%的试验处理下,肉雏鸡磷酸氢钙生物学效价以体增重为指标时分别为100,109,112,115;以磷存留率为指标时分别为100,102,94,89;以骨灰分含量(胫骨灰分和趾骨灰分含量的平均值)为指标时分别为100,116,130,139;以血清磷浓度为指标时分别为100,114,132,133。

Results show that 4-oxo-β-ionone is the major product with yield of 53.5% under the conditions as follows: reaction temperature 45℃, reaction time 24 h, the molar ratio of n: n(NaClO3): n 20: 100: 3, and pH value of solution in 1-3; on the other hand, 5,6-epoxy-β-ionone is major product with yield of 25.4% when reaction temperature is 40℃, reaction time is 24 h, the molar ratio of n: n(NaClO3): n is 20: 120: 5, and pH values of solution is 3. The excessive β-ionone can be recovered by vacuum distillation for reusing again. 4-oxo-β-ionone and 5,6-epoxy-3-ionone were purified by recrystallization and silica gel column chromatograph respectively with the purity over 98%.

研究结果表明:氯酸钠氧化β-紫罗兰酮的反应主要生成4-氧代-β-紫罗兰酮和5,6-环氧-β-紫罗兰酮,经重结晶和硅胶柱层析分离,纯度高于98%;4-氧代-β-紫罗兰酮的有利合成条件是反应温度为45℃,反应时间为24h,溶液的pH值为1~3,反应物配比n:n(NaClO3):n为20:100:3,最佳收率为53.5%;5,6-环氧-β-紫罗兰酮有利的合成条件是反应温度为40℃,反应时间为24h,溶液的pH值为3,反应物配比n:n(NaClO3):n为20:120:5,其收率为25.4%;未反应的β-紫罗兰酮经减压蒸馏回收后可重复使用。

After dealing with the CT image of pedicle screw with interpolation numberical method, for pedicle screw of gradeⅠ,CT had a positive predictive value of 52.7%, a negative predictive value of 94%.,a sensitivity of 67% and a specificity of 94%; for pedicle screw of gradeⅡ, CT had a positive predictive value of 75%, a negative predictive value of 100%.,a sensitivity of 100% and a specificity of 94%.

结果:采用"低窗位、高窗宽"原则处理CT影像后,CT对于Ⅰ度椎弓根螺钉的敏感度为33%、特异度为87%、阳性预测值为32%、阴性预测值为88%。CT 对于Ⅱ度椎弓根螺钉的敏感度为100%、特异度为88%、阳性预测值为60%、阴性预测值为100%。Kapper值为0.603。

Results Of 61 cases, 4 cases (7%) in center 3 mm zone of cornea had mean thickness:(0.439±0.071) mm and polar distance:(3.108±0.904) nun; 8 cases (13%) in 3~5 mm zone had T:(0.328±0.088) mm and p:(3.108±0.904) mm; 28 cases (46%) in 5~7 mm zone had T:(0.320±0.093) mm and p:(3.233±0.381) mm; 21 cases (34%) in 7~9 mm zone had T:(0.340±0.128) mm and p:(3.756±0.539) mm; 61 cases (100%) in 0~9 mm zone had T:(0.336±0.112) mm and p:(3.108±0.904) mm.

结果 61例角膜最薄点平均厚度为(0.336±0.112)mm且平均极距为(3.108±0.904)mm;其中最薄点分布,角膜中央3mm区4例(7%)T为(0.439±0.071)mm且p为(3.108±0.904)mm;角膜3~5mm区8例(13%)T为(0.328±0.088)mm且p为(3.108±0.904)mm;角膜5~7mm区28例(46%)T为(0.320±0.093)mm且p为(3.233±0.381)mm;角膜7~9mm区21例(34%)T为(0.340±0.128)mm且p为(3.756±0.539)mm。

The results of POPGENE analyze indicated that it was moderate level of the genetic diversity of Dipelta, mean PPB (percentage of polymorphic bands) h and I of 4 species of Dipelta as below: D.wenxianensis.(PPB=62.02%,h=0.1850,I=0.2826); D.yunnanensis (PPB=40.31%, h=0.1238, I=0.1874); D. floribunda (PPB=36.82%, h=0.1395,I=0.2045); D. elegans (PPB=15.51%, h=0.0583,I=0.0861). Genetic diversity in D.elegans is the lowest. It is possibly caused by the endemic distribution and local ecotope.

POPGENE分析结果表明,文县双盾木的多态位点百分率平均为62.02%,Nei&s基因多样性指数平均为0.1850,Shannon&s信息指数平均为0.2826;云南双盾木的PPB平均为40.31%;h值平均为0.1238;I值平均为0.1874;双盾木两个居群的PPB平均为36.82%;h值平均为0.1395;I值平均为0.2045;优美双盾木两个居群的PPB平均为15.51%,h值平均为0.0583;I值平均为0.0861;因此,我们认为双盾木属4个种的遗传多样性适中;而优美双盾木由于分布上的地理限制,居群的生境比较孤立,其遗传多样性较低。

The mainly conclusions in our research are as flowing: tungsten trioxide powders with 100 nm primary particle are obtained by spray drying,calcination and wet milling process, and an average size of quadric particle composed of agglomerated particles is 0.64 μm; tungtsen powders with 39 nm grain size and 60 -100 nm primary particle are produced directly from previous tungsten trioxide using one step reduction in hydrogen at 700℃, and an average size of quadric particle of tungsten powder is 2.91 μm; tungsten trioxide and copper tungstate compound powders with 100 nm - 200 nm primary particle are produced using ammonia metatungsten and copper nitrate as raw materials by spray drying,calcination and wet milling process;the compound powders are transformed completely into tungsten and copper compound powders by reduction in hydrogen at 700℃,in which tungsten grain size is 59 nm and copper grain size is 51 nm; primary particle size of compound powders is 80 - 120 nm,and an average size of agglomerated quadric particle is 1.86 μm; tungsten nitride powders with 35 nm grain size are prepared from tungsten trioxide powders by nitrogen treatment thoroughly in pure ammonia at 650℃, and an average size of agglomerated quadric particle is 0.64 μm in normal temperature.

研究结果表明:采用喷雾干燥—焙烧—球磨工艺可以制备出粒度约为100nm的WO_3粉体,它们在团聚后形成的二次颗粒平均粒度为0.64μm;采用一步直接氢还原方法可在700℃下从上述WO_3粉体制备出晶粒尺寸为39nm的、一次颗粒粒度为60-100nm的W粉体,其二次颗粒的平均粒度为2.91μm;以偏钨酸铵、硝酸铜为原料,采用喷雾干燥—焙烧—球磨工艺可制备出一次粒度为100-200nm的WO_3和CuWO_4混合粉体;采用氢还原工艺可在700℃下将这种粉体完全转变为W、Cu复合粉体,其中W的平均晶粒粒尺寸为59nm,Cu的平均晶粒尺寸为51nm;复合粉体的一次颗粒尺寸为80-120nm,在常温下团聚后形成的二次平均粒度为1.86μm;采用纯氨氮化工艺可以在650℃下由WO_3粉体制得WN,其晶粒尺度为35nm,在常温下团聚后的二次平均粒度为6.4μm。

The results were as follows the airdried density ( moisture content of wood is 12%), the basic density and the ovendry density were 0.583 g·cm-3, 0.462 g·cm-3 and 0.507 g·cm-3 respectively, the airdried density was at the medium level in domestic wood species;the shrinkage coefficient of radial, tangential and volumetric were 0.099%, 0.183% and 0.296% respectively, the maximum swelling were 4.106%, 7.958% and 12.627% respectively;the ratio of tangential shrinkages to radial shrinkages was 1.5-1.9;the toughness was 52.12 kJ·m-2;the hardness of cross, radial and tangential section were 41.53 MPa, 31.41 MPa and 35.51 MPa respectively;the compressive strength parallel to grain was 44.50 MPa ;the modulus of elasticity in static bending and the bending strength were 12.63GPa and 127.31 MPa respectively;the shearing strength parallel to grain of radial and tangential were 8.76 MPa and 10.54 MPa respectively;the cleavage strength to grain of radial and tangential were 124.3 N·mm-1 and 138.6 N·mm-1 respectively.

结果表明大叶栎木材的气干密度(含水率为12%)、基本密度和全干密度分别为0.583 g·cm-3、0.462 g·cm-3和0.507 g·cm-3,气干密度属于国产木材的中等级水平;径向、弦向和体积干缩系数分别为0.099%、0.183%、0.296%,湿胀率依次为4.106%、7.958%和12.627%,差异干缩为1.5-1.9,其尺寸稳定性较好;冲击韧性为52.12 kJ·m-2,端面、径面和弦面硬度分别为41.53 MPa、31.41 MPa和35.51 MPa,顺纹抗压强度为44.50 MPa,抗弯弹性模量和抗弯强度分别为12.63 GPa和127.31 MPa,径面和弦面顺纹抗剪强度分别为8.76 MPa和10.54 MPa,抗劈强度依次为124.3 N·mm-1和138.6 N·mm-1。

The results were as follows: the air-dried density(moisture content of wood is 12%),the basic density and the oven-dry density were 0.583 g·cm-3,0.462 g·cm-3 and 0.507 g·cm-3 respectively,the air-dried density was at the medium level in domestic wood species;the shrinkage coefficient of radial,tangential and volumetric were 0.099%,0.183% and 0.296% respectively,the maximum s...

结果表明:大叶栎木材的气干密度(含水率为12%)、基本密度和全干密度分别为0.583 g.cm-3、0.462 g.cm-3和0.507 g.cm-3,气干密度属于国产木材的中等级水平;径向、弦向和体积干缩系数分别为0.099%、0.183%、0.296%,湿胀率依次为4.106%、7.958%和12.627%,差异干缩为1.5-1.9,其尺寸稳定性较好;冲击韧性为52.12 kJ.m-2,端面、径面和弦面硬度分别为41.53 MPa、31.41 MPa和35.51 MPa,顺纹抗压强度为44.50 MPa,抗弯弹性模量和抗弯强度分别为12.63 GPa和127.31 MPa,径面和弦面顺纹抗剪强度分别为8.76 MPa和10.54MPa,抗劈强度依次为124.3 N.mm-1和138.6 N.mm-1。

In this bath, maleic acid was an inhibitor, when its concentration was kept at 20 mg/L, the deposition rate could reduce to 6.17μm/h, the content of nickel decreased to 1.74% and the resistivity was 7.51μΩ·cm; Potassium ferrocyanide inhibited deposition of copper, when its content was 0.5 ppm, the deposition rate decrease to 3.38μm/h, the content of nickel was 2.03%, the resistivity can reduced to 5.41μΩ·cm, the copper deposits also had higher (111) plane orientation. Thiourea was also an inhibitor in this system, when its concentration was kept at 0.8 ppm, the deposition rate was 4.72μm/h, the content of nickel in the film was 1.20%, the resistivity can reduced to 5.46μΩ·cm, at the same time, the deposition at (111) plane orientation become more favorable.

结果表明,马来酸在该体系中是抑制剂,当其浓度为20 mg/L时,镀速降为6.17μm/h,镀层镍含量降为1.74%,表面电阻率降为7.51μΩ·cm,铜层颗粒细小均匀,更有利于在(111)面上的结晶;亚铁氰化钾的加进可以明显降低镀,当其浓度为0.5 ppm时,镀速为3.38μm/h,镀层镍含量降为2.03%,表面电阻率降为5.41μΩ·cm,铜层颗粒细小均匀,(111)晶面衍射峰增强;硫脲在体系中也显示为抑制剂,当其浓度为0.8 ppm时,镀速降到4.72μm/h,镀层镍含量为1.20%,表面电阻率降为5.46μΩ·cm,形成的铜颗粒很小,同时(111)晶面衍射峰增强,有利于铜在(111)面上结晶。

Whereas the sensitivities after 48 h were similar for all media tested (77% for MRSA_ID and ORSA; 73% for C_MRSA and ORSA after enrichment ), the specificities of MRSA_ID (98% after 24 h and 94% after 48 h) and C_MRSA (98% after 24 h and 90% after 48 h) were superior to the specificities of ORSAs (92% after 24 h and 83% after 48 h) and TSB-ORSA (86% after 24 h and 81% after 48 h).

结果所有的培养基在经过48h后得出的敏感性均接近(MRSA_ID 和 ORSA的敏感性为77%; C_MRSA和的敏感性为73%),而特异性则是以MRSA_ID (24 h为98%,48 h 为94%)和 C_MRSA (24 h为98%,48 h为90%)为优,优于ORSAs (24 h 为92%,48 h为83%)和 TSB-ORSA (24 h为86%,48 h为81%)。

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