结构射

To obtain precise result, itis necessary, in the aspect of hardware, to set up one stable optics system with highSNR, only if so, can we do the measurement with the steady NIR. To do so, we designthe optics system using AOTF, and take some measures to increase the light energyand the system SNR, which includes the three layers structure of the light chamber,the equipments to cover the useless light, polarizing to reduce the influence of 0 gradelight and focalize the light with lens. Apart from the hardware aspect, according to theexperiments, we can see that the different temperatures between at setting up themodels and at predicting the results will affect the prediction results in a way, and theaffection extent will be increased along with the increase of the temperaturedifference. Moreover, the light energy that can be detected will be different with thecontact pressure, and the match of the refractive indexes between the tissue and thesurroundings will enhance the light transmission depth, which will take moreinformation of the tissue. So, during the measurement, we should ensure the sametemperature between measuring and predicting, the same contact pressure at everymeasurement and the match of the indexes between the tissue and the surroundings aspossible as we can.

要提高测量精度，从硬件方面就必须有一个稳定的、信噪比较高的分光光路系统，以此得到稳定的近红外光来进行无创检测，针对这个目的，我们设计了 AOTF 分光光路系统，并在系统中采用一定的措施如三层灯室结构、遮光筒以减小杂散光、起偏和检偏来减小 0 级光影响、透镜汇聚等等来提高出射光的能量和系统的信噪比；从其他影响因素方面，通过实验，我们得到不同的建模温度对于预测结果有一定的影响，且影响随着温度的差值越大而越大，另外散反射光谱的能量也随着接触压力的不同而不同，组织的折射率与环境匹配将加大光的入射深度，从而能携带更多的组织信息，所以在测量时我们尽可能保证同一温度、保证同一接触压力以及利用物理或者化学的方法使组织与环境折射率匹配等。

In the meanwhile, we summarized the inspective methods and principles of the DLC: N films such as Raman spectrum, X-ray photoelectron spectrum, infrared absorption spectrum, atomic force microscope, scanning electron microscope.

第三章介绍了射频磁控溅射方法制备薄膜的步骤及设备操作的步骤，并制备了DLC薄膜及DLC：N薄膜，对其成分和结构进行了对比。

By means of measurements of mechanical and electrical properties, metallographical and transmission electron microscope observation, X-ray diffraction and selected diffraction analysis, scanning electron microscope and energy spectrum, the phase transformation process of Cu-15Ni-8Sn alloy and the relation between its microstructure and properties were studied.

本文利用力学与电学性能测试，金相与透射电镜观祭，X-射线衍射与选区电子衍射分析，扫描电镜和能谱分析等方法对Cu-15Ni-8Sn合金的相变过程以及合金的组织结构与性能之间的关系进行了研究。

Finally, the cytotoxic and antibacterial activities of the oxamido-bridged binuclear complexes were studied in vitro.. This dissertation consists of three sections as follows:1. The crystal structure of a oxamide dinitrate,(1) [H_4dmaeoxd](NO_3)_2 H_2dmaeoxd = N,N\'-bis[2-ethyloxamide, has been obtained. The diversity of complexes with different structures is carried out by successful synthetic strategy of controlling species of metal ions, counter anions, pH values and solvents in the course of synthesis. Four dinuclear complexes bridged by trans-dmaeoxd2-: [Cu_2_2](ClO_4)_2 (2), [Cu_2_2](ClO_4)_2 (3),、[Cu_2(Me_2phen)_2](ClO_4)_2 (4), [Cu_2_2(H_2O)_2] (5); Four dinuclear complexes bridged by cis-dmaeoxd2-: [NiNi_2](ClO_4)_2 (6), [CuNi_2](ClO_4)_2·2CH_3OH (7), [CuZn_2]-(ClO_4)_2·2H_2O (8), [Cu(H_2O)Ni_2](ClO_4)_2.0.5CH_3OH (9); three 1-D polynuclear complexes: [Cu_2]_n·nH_2O (10), [Cu_2(H_2O)_2-]_n·4nH_2O (11), [Cu_2(H_2O)]_n(NO_3)_n·2nH_2O (12); one 2-D polynuclear complex,[Cu_6_3(μ_3-OH)_2(H_2O)_2]_n(ClO_4)_(4n).2nH_2O (13); the others: [VO(H_2O)]·2H_2O (14), [Zn_2_4](ClO_4)_2·H_2O (15), [Cu_2]·2DCM (16) have been synthesized and characterized by X-ray single crystal diffraction, elemental analysis, IR spectra.

本论文主要包括以下三部分：一、合成得到了一个草酰胺配体硝酸盐的单晶结构，[H_4dmaeoxd](NO_3)_2 (1)；通过调控金属离子的种类、端基配体、抗衡阴离子、溶剂、pH值等条件定向合成了四个反式草酰胺桥联双核铜配合物：[Cu_2_2](ClO_4)_2 (2)、[Cu_2_2](ClO_4)_2 (3)、、[Cu_2(Me_2phen)_2](ClO_4)_2 (4)、[Cu_2_2(H_2O)_2] (5)；四个顺式草酰胺桥联同/异双核配合物：[NiNi_2](ClO_4)_2 (6)、[CuNi_2](ClO_4)_2·2CH_3OH (7)、[CuZn_2]-(ClO_4)_2·2H_2O (8)、[Cu(H_2O)Ni_2](ClO_4)_2.0.5CH_3OH (9)；三个一维聚合物： [Cu_2]_n·nH_2O (10)、[Cu_2(H_2O)_2-]_n·4nH_2O (11)、[Cu_2(H_2O)]_n(NO_3)_n·2nH_2O (12)；一个二维聚合物： [Cu_6_3(μ_3-OH)_2(H_2O)_2]_n(ClO_4)_(4n)。2nH_2O (13)；单核钒配合物[VO(H_2O)]·2H_2O (14)、草酸根桥联双核锌配合物[Zn_2_4](ClO_4)_2·H_2O (15)、美洛西康铜配合物[Cu_2]·2DCM (16)，利用元素分析、摩尔电导、红外光谱、电子光谱和单晶X-射线衍射对上述所得化合物进行了结构表征，探讨了结构影响因素，并研究了其超分子结构。

In this research, two novel compounds in which alkylenedithiomethylene Malonic acid act as the main coordination agents and the compounds containing N atom (such as pyridine, Phenanthroline Ethanediamine and 4,4'-Bipyridinyl) act as the associating coordination agents have been synthesized by the means of solution and solid-liquid diffusing reactions. 9 coordination complexes and polymers have been designed and synthesized in which the transition metals Cu and Zn acted as the centre ions. These compounds have been characterized by X-ray single crystal diffraction analysis, and some properties of them have been tested and analyzed.

本论文设计合成了两种结构新颖的含有二硫缩烯酮结构的丙二酸类化合物，以此为主要配体，以含氮化合物(吡啶、邻菲罗啉、乙二胺和4，4'-联吡啶)为辅助配体，采用常规溶液合成和固-液相扩散等方法，设计合成了9个过渡金属Cu和Zn离子配合物和配位聚合物，采用单晶X-射线衍射等技术对晶体结构表征，并对其部分性质进行了测试和分析。

The invention uses the normal glass as the basal board , the studded target made of the indium metal mixing into molybdenum or tungstenic, and applies the responsive direct current magnetron sputtering technique under the condition of the basal board temperature equals room temperature, and also, under the appropriate state for the sputtering pressure, the oxygen partial pressure, the sputtering current, and the sputtering voltage to achieve the non-crystal structure In2O3:M film.

本发明以普通玻璃为基板，利用铟金属掺钼或钨的镶嵌靶，在基板温度为室温的条件下采用反应直流磁控溅射技术，在适当的溅射压强、氧分压、溅射电流和溅射电压的条件下制备获得具有非晶结构的In2O3：M薄膜。

Conrolled pore sizes proper the pore size distribution of the microporous materials were uniformally achieved by the process of vacuum filtration and calcination. SEM images revealed that ZrO2 porous ceramics with ordered and uniform micropores have been obtained ...

用X-射线衍射和扫描电子显微镜观察了ZrO2多孔陶瓷的相组成和显微结构，结果表明其具有孔径分布均匀的结构特点且ZrO2四方相结构没有改变。

The separation angle about beam and beam is depended on the vice structure angle:the design of splitting Li P prism is better about the need of beam vertical out;the design of splitting Grand · Thompson prism is better about the need of big splitting angle .

出射的 光与光的分离角与副结构角有关；对于光垂直出射的需要，选用分束李普奇棱镜设计为好；对于大分束角的需要，选用分束格兰·汤普逊棱镜设计为好。

Rare earth metal seed Tb was employed for the growth of GaN nanorods. GaN nanorods were synthesized successfully through ammoniating Ga2O3/Tb films sputtered on Si(111) substrates. X-ray diffraction results indicated that the nanorods were hexagonal GaN.

使用稀土元素Tb作催化剂，通过氨化溅射在Si(111)衬底上的Ga2O3/Tb薄膜，成功制备出GaN纳米棒。X射线衍射测试显示，GaN纳米棒具有六方结构。

The analysis results of FTIR , SEM, X-ray Diffraction and TG-DSC proved that,the existence of graft copolymerization between cassava starch and acrylamide was occured;the structures of cassava were destroyed during the copolymerizing; the structures of the copolymer were largely amorphous; within the range of 700℃,the thermal degradation process of the St-g-PAM was divided into three-steps, which was more complex than that of cassava.

FTIR、SEM、X射线衍射、TG-DSC分析结果表明木薯淀粉与丙烯酰胺已发生接枝共聚反应；木薯淀粉在接枝共聚反应中，结构被破坏，接枝共聚物的结构基本上为无定型结构；在700℃温度范围内，木薯淀粉丙烯酰胺接枝共聚物的热降解为三步降解历程，比木薯淀粉复杂。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。