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Morphology, composition and structure of the obtained chromate film were studied by measurement of polarized electric resistance and neutral salt spray test, with result that corrosion resistance of the chromate film was greatly improved with the addition of titanium which attributes to the formation of titanium dioxide and titanyl sulfate in chromate films and their corrosion products.

利用SEM、XPS等方法研究了所得钝化膜的形貌、组成及结构,并通过极化电阻的测量和中性盐雾试验研究了钝化膜的耐蚀性。

The nitrides with high specific surface area from oxide precursor can be prepared through temperature-programmed reduction via topotactic reaction in ammonia or nitrogen under strict reduction conditions.

在基本不破坏氧化物前驱体晶体结构和严格的氮化条件下,氧化物前驱体通过程序升温氮化经由&局部规整反应&可以制备出高表面积的过渡金属氮化物。

Mono dodecyl phosphate is synthesized using trichloro phosphate and di dodecyl phosphate is synthesized using phosphorous pentoxide. The structures are confirmed by IR and contents are analyzed by GC and HPLC. Mixed esters with different mass ratios of mono and di esters are prepared.

分别以三氯氧磷为磷酸化剂,合成并提纯了正十二烷基磷酸单酯,以五氧化二磷为磷酸化剂,合成并提纯正十二烷基磷酸双酯,其结构通过质谱得到了确证,产品组成采用气相色谱和高效液相色谱得到了确定。

First, the geometry optimization for 1-phenyldibenzophosphole and triphenylphosphine were carried out using quantum chemical AM1 method.

用量子化学AM1方法优化了1-苯基二苯并膦和三苯基膦的几何构型,比较了两种化合物的电子结构和空间结构,发现PDBP作为羰基合成铑膦催化剂的配体要优于三苯基膦;系统研究了PDBP的合成方法,其最佳合成条件为:在无水无氧的条件下,采用二乙胺锂与溴化四苯基膦摩尔比为3,反应温度为22 ℃,反应5 h,反应后酸化, pH值为1~2,产物收率可达到85%~88%。

The microheterogeneity and tryptic fragments of glycoprotein recombinant human erythropoietin were analyzed by high performance capillary electrophoresis.

用高效毛细管电泳测定了重组人促红细胞生成素的微多相性、肽图,同时采用毛细管电泳质谱联用技术鉴定了部分非糖基化胰酶消解片段和O-126糖基化肽的结构。

Moreover, we can find two kinds of evidences in the structure of the Min dialect: the voiced and unvoiced characters of the initial and the aspirated and unaspirated characters shown after the devoicing of the initial have corresponding relationships both with the divisions of tones and with the different pronunciations in colloquial layer and literal layer. Section Two: today's pronunciation of the MC initials Fei and Zhi groups.

这还可以找到方言内部结构的两种证据:一是闽北方言的声母清浊、清化后送气不送气与声调分化存在着明显的对应;二是声母清浊和清化后送气不送气与文白异读也存在着明显的一致性。

The fatty oil from the seeds of M. cochinchinensis was extracted with petroleum ether, and the saponification was carried out with potassium hydroxide. The unsaponifiable matter was isolated and purified by silica gel column chromatography, and the structures of their constituents were elucidated by means of IR, MS, 1H-NMR, and authentic chemicals.

石油醚提取脂肪油,氢氧化钾进行皂化反应,对不皂化部分进行硅胶柱色谱的分离和纯化,用IR,MS,1H-NMR等波谱技术和对照品对照等方法进行化合物的结构鉴定。

The characteristics of C4D detector are simple in structure, easy in mini AT uriz AT ion and integr AT ion, and free of electrodes contamin AT ion, so it have the important value of applic AT ion in mini AT urized total analysis systems.

该检测器的原理清楚,结构简单,易于微型化、集成化,不污染检测电极,在微型全分析系统中具有十分重要的应用价值。

For a reference GFR core design, the criticality and burnup characteristics for the single assembly model and full core model were calculated through the coupling of MCNP and ORIGEN, and the differences in the calculation precision and calculation time were compared between the fine structure model and homogenized assembly model, respectively.

本工作以一气冷快堆的设计方案为研究对象,针对单组件模型和全堆芯模型,采用MCNP耦合ORIGEN的方法,计算了有关临界、燃耗过程的几个重要物理特性,比较了采用精细化结构和组件均匀化方法在计算精度、计算时间等的差别,说明了采用组件均匀化方法进行气冷快堆全堆燃耗计算的必要性和可行性。

For a reference GFR core design,the criticality and burnup characteristics for the single assembly model and full core model were calculated through the coupling of MCNP and ORIGEN,and the differences in the calculation precision and calculation time were compared between the fine structure model and homogenized assembly model,respective...

本工作以一气冷快堆的设计方案为研究对象,针对单组件模型和全堆芯模型,采用MCNP耦合ORIGEN的方法,计算了有关临界、燃耗过程的几个重要物理特性,比较了采用精细化结构和组件均匀化方法在计算精度、计算时间等的差别,说明了采用组件均匀化方法进行气冷快堆全堆燃耗计算的必要性和可行性。

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It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发,分析对称连杆曲线上鲍尔点的产生条件,提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品,年生产总值3000万美元,产品价廉物美、选料上乘、质量保证,深受国内外客户的青睐

The eˉtiology of hemospermia is complicate,but almost of hemospermia are benign.

血精的原因很,以良性病变为主。