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Using trimeric surfactant C_(14-2-14-2-14) as templating agent, the low cost and facile inorganic species sodium aluminate and sodium silicate as inorganic precursors, highly ordered 2D hexagonal aluminosilicate MCM-41 with high Al content were successfully synthesized.

利用廉价易得的硅酸钠和偏铝酸钠作为无机前驱体,以低聚季铵盐表面活性剂C_(14-2-14-2-14)为模板剂合成了高铝含量,高有序性的二维六方结构介孔硅铝酸盐材料,并对材料的结构、表面性质、形貌以及酸性进行了研究。

We report a previously uncharacterized alpha-helical module, the BEN domain, in diverse animal proteins such as BANP/SMAR1, NAC1 and the Drosophila mod(mdg4) isoform C, in the chordopoxvirus virosomal protein E5R and in several proteins of polydnaviruses.

我们在多种动物蛋白质,如BANP/SMAR1,NAC1和果蝇mod(mdg4)异构体C,及脊椎动物痘病毒亚科蛋白质E5R和一些多去氧核糖核酸病毒科中,报道了一个以前没有描述的α螺旋结构模块----BEN结构域。

Mn(H_3biim)_2_2Cl_2 and Cd(H_3biim)_2_2Cl_2 have been synthesized from H_2biim, their structures were determined by X-ray crystallography. The two complexes have similar structures and both are neutral compounds. One N atom in H_2biim is protonated, forming a H3biim+ cation. The later is an unidentate ligand, the central metal, Cd or Mn is six coordinated and adopts a distorted octahedral environment.

合成了联咪唑锰配合物Mn(H_3biim)_2_2Cl_2和联咪唑镉配合物Cd(H_3biim)_2_2Cl_2,晶体结构表明这两个配合物结构相似,均为中性化合物,联咪唑的一个氮原子被质子化,形成一价阳离子(H_3biim~+),它采取单齿配位,中心Mn原子是六配位,其配位环境为畸变的八面体。

Part Ⅰ: Brain structural abnormalities in patients with a first episode of major depression — An Optimized Voxel-based morphonmetry MRI study OBJECTIVE: We examined the structural difference in regional gray matter density between unmedicated patients with a first episode of major depression and healthy comparison participants in order to find the base of pathophysiologic mechanism in MD.

第一部分首发重性抑郁症患者脑结构磁共振异常的研究—基于体素的优化形态测量学分析方法目的:探讨首发、未服药重性抑郁症患者全脑灰质密度的异常变化,以揭示抑郁症患者病理生理机制的脑结构基础。

The second part was to test the appearance, ingredient analysis, surface potential, thermal conduction properties, and magnetism of the nano composite fluid prepared from the parameters. The experiment found that unoxidized particles, Ag, Cu, Fe, and Ni appeared round. If combined with oxygen in water as oxides, the nano particles would grow toward certain directions. In copper/iron nano composite fluid, FeO appeared cubic, Cu2O appeared coniferous. In silver/iron nano composite fluid, FeO was polygonal. In dielectric potential detection, the nano composite fluid was likely to aggregate and deposit, except for silver/iron set. In other sets, the pH of silver/cobalt nano composite fluid was 7, surface potential was 21.21mV; the pH for silver/nickel nano composite fluid was 6.5, surface potential was 21.04mV; the pH for copper/iron nano composite fluid was 7, surface potential was -30mV. The fluid particles of the three sets could all maintain suspension of 2 weeks or more. For thermal conduction, the silver/nickel, nano composite fluid showed the best thermal conduction. Under temperature of 30℃ fluid weight conduction of 0.4%, the thermal conduction increase was 26%. For magnetic detection, except for silver/iron nano composite fluid, the nano particles of other three sets were paramagnetic, and all four sets were soft magnetic nano composite materials.

第二部分。将由较佳制备参数所产出的奈米复合流体,进行形貌外观、成分分析、表面电位及热传导性质实验与磁性检测;在奈米颗粒的形貌部分,经实验发现Ag、Cu、Fe、Ni等未氧化的颗粒皆呈现近似圆形,而若与水中的氧结合形成氧化物,奈米颗粒则会朝特定方向成长,在铜/铁奈米复合流体中FeO为四方体结构、Cu2O的颗粒是针叶状,在银/铁奈米复合流体中FeO则为多边形结构;而介面电位检测方面,结果显示经本制程所产出的奈米复合流体除银/铁奈米复合流体这一组较容易聚集沉淀外,其他三组中银/钴奈米复合流体的pH值为7,表面电位为21.21mV,银/镍奈米复合流体的pH值6.5表面电位为21.04mV而铜/铁奈米复合流体的pH值为7时表面电位约在-30mV,且此三组流体颗粒皆能维持悬浮性2周以上,悬浮性较佳;热传导实验部分,四组奈米复合流体中以银/镍奈米复合流体在增进热传上效果最佳,在温度30℃及流体重量浓度0.4﹪条件下热传导系数增进达26﹪;磁检测方面,除了银/铁奈米复合流体外,其他三组奈米颗粒皆属顺磁性,且这四组奈米复合材料都是属软磁性。

ResultsThere was no expression of Caspase-3 in group A. The expression of Caspase-3 in group C was decreased compared with that in group B(P<0.01. In groups B and C, expansion and vacuolization of mitochondria, swollen neurons and apoptotic bodies appeared, which suggested that WBH could induce neuron injury, and the neuron injury in group C was more severe than that in group B.

结果A组大鼠海马区神经元无Caspase-3表达,B、C两组大鼠海马区神经元有Caspase-3表达,B组较C组Caspase-3表达平均灰度值减小。B、C两组大鼠海马神经元超微结构发生改变、细胞器水肿,部分线粒体空化,内质网稀疏,突触前膜、后膜结构不完整,可见自噬体结构;B组大鼠的神经元超微结构损害较C组轻。

Better numerical prediction of the distributions of shear forces and bend moment within the pile group has also been obtained with the consideration of many stochastic parameters such as the soil properties of sea warf, seismic properties, etc. And then we analyze the dynamic nonlinear seismic pile-soil interaction in sea warf as an example to apply the software of ANSYS to the assessment of the dynamic interaction of soil-structure in the harsh situation of random earthquake. And then we denoted that the soil-pile interaction is too difficult to be expressed in equations because the non-linear interaction between soil and pile.

5桩基由于其本身的优点得以在海洋码头结构中大量的运用,但是海洋码头结构在海洋环境下受多方面的影响,土与桩体的相互作用关系很难清楚的表达,由于影响因素的多样性及复杂性,以及它们与桩基性状之间的非线性和非确定关系,使得关于桩基性状的各种理论解答还不能采用简便的表达式以反映其复杂多变的机理,尤其是难于反映施工及环境因素对桩基性状的影响,而且如何发挥桩基的技术经济效益和如何合理的确定桩的极限承载力,也是一个技术难度很大的问题。

Mesoporous zincum sulfide is synthesized by gentle wet chemosynthesis method, with DDA as templates and Zinc acetate and TAA as precursors. The effect to the synthesis of the ratio of reactive components, the volume of pH, reactive time and reactive temperature has been dicussed systematically, and structures of the as-synthesized samples have been characterized by X-ray diffraction, N2 adsorption-desorption, scanning electron microscopy, Fourier transform-infrared spectra, UV-vis diffuse reflectance spectroscopy, transmission electron microscopy.

以十二胺为模板,醋酸锌及硫代乙酰胺为前驱体,温和湿化学法合成了硫化锌无序介孔结构,系统研究了反应物配比、pH值、反应温度、反应时间对材料合成的影响,运用X射线衍射、N2吸附-脱附、扫描电镜、红外光谱、紫外-可见吸收光谱、透射电镜等分析手段对介孔材料的结构进行了详细的表征。

We observed the changes of the proprioceptors in the partly injuried ACL and the xenogeneic graft/artificial graft being used to reconstructing the injuried ACL with gold chlorid staining method and laser copolymerization electron micrography method to observe the morphological changes of the neuromechanism in the ligament tissue,with RT-PCR method to evaluate the proportion and the regeneration of the nerve component and with HRP retrograde tracking technology and electrophysiologic study to judge the functional changes of the neuromechanism in the ligament tissue,respectively.

本研究分别制作兔ACL部分损伤动物模型、异种肌腱移植物重建损伤ACL动物模型和LARS人工韧带重建损伤ACL动物模型,分别于术后不同时间点对损伤ACL/移植物进行氯化金染色光学显微镜检查和PGP9.5免疫荧光染色后激光共聚焦电子显微镜检查观察韧带内神经结构形态学变化,用RT-PCR法检测韧带中GAP-43和PGP 9.5的mRNA表达情况以评价损伤ACL/移植物内神经成分比例及神经再生情况,通过HRP逆行追踪技术和电生理检查(包括体感诱发电位和腘绳肌肌电图)评价损伤ACL/移植物内神经结构的功能情况。

In this paper, the stable Au complexes are classified according to the coordination atoms and their characteristic structure. The recent development of the researches on the antitumor activity of Au complexes including the structure-activity relationship, biological targets and the mechanisms of action are reviewed. The structure of the coordination ligand and the leaving group have great impact on the in vitro cytotoxicity of the Au complex. Many physical and biological methods are introduced to study the interaction between the Au complexes and the suspected bio-target, such as DNA, protein, mitochondrion, thio-containing biomolecules, etc. The interaction modes (intercalating, electrostatic interaction, covalent bonding, etc.) are focused to illustrate the reason for the antitumor activity of Au complexes.

本文按配位原子的不同总结了稳定三价金配合物的结构特征,按其生物活性的构效关系、生物靶点和作用机制综述了三价金配合物抗肿瘤活性研究的最新成果:配体的结构特点以及离去基团对三价金配合物的体外细胞毒性影响较大;介绍了用于检测三价金配合物与可能的生物靶分子之间的相互作用的多种物理和生物学方法,重点关注了相互作用的模式,如嵌入/静电吸引/共价结合等,并解释了三价金配合物抗肿瘤活性的原因。

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Others availed themselves of the throngs which attended the sacred festivals to indulge in immoderate enjoyment and tumultuous revelry.

其他人利用自己的throngs出席神圣的节日,以沉迷于immoderate享受和动荡不定的狂欢。

I'll go into the matter.

我会调查这事的。

At distance, Bulwer's Petrel appears to be uniform black.

在远距离之下,穴鸟呈现一致的黑色。