结构体

The study of crystal structure indicates that the complexes belongs to tetragonal,14(1)/a, a=b=27.047(5) A, c=14.103(3) A, a=b=y =90,V=10317(4)A3, Z=16, Dc=1.071g/cm3, F(000)=3408, R,=0.1395, R2=0.1766 and every unit of the tetranuclear complexes is four-coordinated to tridentate ligand and nitrogen atom in pyrazolone from other ligand. The complexes is slightly deformed square-planar geometry.

晶体结构研究表明，该配合物为四方晶系，空间群I4(1)/a，a=b=27.047(5)，c=14.103(3)，α=β=γ=90°，V=10317(4)，Z=16，Dc=1.071g/cm~3，F(000)=3408，R_1=0.1395，ωR_2=0.1766，其结构单元是由一个三齿配体中的ONO和另一个配体吡唑啉酮环二位上的N配位后形成略微畸变的平面四边形构型，其中Cu的配位数为4。

Rhombohedral ITO solid solution was metastable in air and it would be transformed to cubic ITO solid solution by heat-treatment.

刚玉型结构ITO固溶体在空气中处于亚稳态，并且在加热的条件下可以转变为萤石型结构ITO固溶体。

The transformation from rhombohedral ITO solid solution to cubic ITO solid solution started at 578℃ and ended below 800℃, and it exhibited a weakly endothermic behavior.

刚玉型结构ITO固溶体向萤石型结构ITO固溶体的转变起始于578℃，在800℃以前转变终止并且表现为一种弱吸热行为。

EAA formed a rodlike extension structure in PP matrix, and much more continuous structure are formed, which resulted in a rapid decreasing of the volume resistivity with the increasing of EAA resin content.

EAA相在PP基体中呈棒状伸长结构，且随着EAA树脂含量的增大，在PP基体中形成更多更为连续的棒状伸长结构，使体积电阻率迅速下降。

1H-imidazolyl)-1H-imidazolium chloride-4-aminobenzoic acid, 2,2-bi-1H-imidazolium bis(3,4,5-trihydroxy benzoate) tetrahydrate and bis2-(2-1H-imidazolyl-1H-imidazolium 3-carboxy-4-hydroxybenzene-sulfonate monohydrate have been synthesized and characterized by X-ray diffraction methods.

在化合物中，晶体结构中的基本单元是一个通过氢键模式R_2~2(9)和R_2~1(7)构成的氢键三聚体PABA…H_3biim~+…Cl~-，这个三聚体基本单元又通过N-H…Cl氢键相互作用形成了一维带状结构。

In this paper, material properties of the segment of the porous metal-bonded diamond grinding wheel were researched by finite element simulation. Segments were manufactured according to the design result and their elastic modulus was measured. The key points are as follows: The influence of the porosity on the elastic modulus was analyzed through a finite element method. In the FEM model, the design variable only includes the porosity, and the tetrakaidecahedron model is applied as the microstructure model of porous metal matrix. The corresponding porosity was decided in order to meet the requirement of the elastic modulus.

本文利用有限元软件对多孔金属结合剂金刚石砂轮节块的材料性能进行了数值模拟计算，依设计结果制备了节块试样，并测试了节块的弹性模量，主要内容有： 1、充分借鉴多孔材料结构设计和分析的方法，以十四面体模型为多孔金属胎体的微观结构模型，以孔隙率为设计变量，通过有限元分析，计算出满足一定弹性模量要求的多孔金属胎体的孔隙率范围。

But the electrochemical results show that complexes exhibitcompletely irreversible redox behaviour which is different from thatfound in diiron proteins. 1.3 To obtain the diiron species which are stable to elec-trochemical reduction, a series of new tetranuclear cage ironspecies containing two 〓 cores, with using hexadentatepolybenzimidazole ligands, were synthesized and characterized by vari-ous spectroscopic methods. Their physical properties have been investi-gated. The crystal structures of 〓〓tetrakis (benzimidazol-2-ylmethyl)-1, 4-diaminobutane and 〓,〓-tetrakis ( N-ethylbenzimidazol-2-ylmethyl )-1, 4-diaminobutane were determined. They contain two 〓 cores which arelinked to each other by -〓-chain in the ligands.

1.3为了获得电化学还原稳定双核氧桥联Fe化合物，使用六齿配体合成了一系列含有两个〓单元四核笼状化合物，并用各种谱学手段表征了它们，还研究了它们的物理化学性质确定了〓L=N，N，N'，N'-四(苯骈咪唑基-1，4-丁二胺和〓，〓四-1，4-丁二胺化合物的晶体结构，它们含有两个〓单元，其中两个〓单元是通过配体的〓链桥联成四核笼状结构。

Equiaxed and bigger grains are produced after C.P.Ti is deformed under the high temperature. Besides, many tiny subgrains were found in some of the metallurgical structure. The dislocation reaction caused by the deformation under the high strain rate generates ductile cellular metastructures, while the equiaxed cellular metastructures are generated under the low strain rate. The metallurgical structure of TC4 alloy including lath-shaped hexagonal martensite and trimetric martensite only exists in the higher temperature. The homogeneous, tiny and reticular grain shown after extreme high temperature deformation.

在高应变速率下变形引起的位错反应形成拉长的胞状亚结构，而低应变速率下变形则形成等轴的胞状亚结构；TC4合金在特高温变形条件下其金相组织呈网篮状，显微组织几乎全部为均匀细小的晶粒，同时出现了板条状六方马氏体；在温度尤其高的情况下还形成了斜方马氏体，变形引起的位错反应形成六方位错网络，在1200℃以下的变形易产生孪晶。

Lastly, in accordance with the actual situations of the prototype structure of mosque pagoda, based on the similar relation of model experiments, a model structure of mosque pagoda with a similar coefficient of 1/10 is designed and fabricated. Earthquake simulating shaking table tests are performed on the model structure of pagoda in the cases the AB type passive control system with SMA dampers is erected or unerected. The leading earthquake responses like the relative drift at the top of the main tower and the small tower, interstory drift ratio, acceleration, and cracking process of the pagodas body etc. are studied. The operational behaviors involving the deformation capacity and energy dissipation capacity is tested for passive control system with SMA dampers under the earthquake excitation, and the corresponding control mechanism and regularity is also analyzed. Furthermore, the performance changes and protection effectiveness is comprehensively evaluated while the model structure of pagoda is seismically protected or not.

最后，根据光塔原型结构的实际情况，以模型试验的相似关系为基础，设计并制作了一个相似系数S，为1/10的光塔模型结构，并先后进行了未安装和安装A、B型SMA阻尼器被动控制系统光塔模型结构的地震模拟振动台试验，研究了模型结构在3种不同工况下，主塔顶部和小塔顶部的相对位移、层间位移角和加速度以及塔体开裂等光塔结构的主要地震反应，测试了SMA阻尼器被动控制系统在地震激励下的变形能力和消能能力等工作性能，分析了相应的控制机理和控制规律，并从总体上评价了光塔模型结构抗震保护前后的性能变化和保护效果。

In short, this study has systematically researched the mechanical properties of rockmass structural plane by employing new theories and methods, and has made creativeachievements in controlling rock mass structural plane and raising the stability ofunderground stopes and tunnels. It is of great referential value for the design,construction and production of rock mass works, and so is it for enterprises in raisingeconomic benefits and ensuring production safety.

总之，本文采用新理论、新方法，系统地研究了岩体结构面的力学特征，对控制岩体结构面的方法、手段和措施及提高地下采场、巷道的稳定性等方面的研究取得了创造性成果，本文对解决岩体工程的设计、施工和生产中存在的问题，提高企业经济效益和确保生产安全等都具有十分重大的意义。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失