结构

The benezothiazolocoumarin dyes substituted with chlorine on 5'-position also showed bathochromic shift of the maximum absorption and fluorescence emission.

这9只染料用於涤纶染色有很好的应用性能，差别不大；恶唑环结构和喹唑酮结构的染料耐光牢度明显好於噻唑环结构和咪唑环结构的染料。

The results show that the porosity of the membrane prepared by ScCO_2 induced phase separation is higher than that prepared by conventional method;the membrane structures are significantly influenced by the process parameters;compared with the conventional immersion precipitation phase inversion,ScCO_2 induced phase separation process can effectively avoid the formation of macrovoids at suitable operating conditions;during depressurization process,the great differences in the effect of depressurization time on membranes structure for various polymer materials result from that the speed of CO_2 gaseous nuclei escaping from membrane substrate can not keep the pace with the outer depressurization rate.(2) The tendency that the interaction parameters affect the binodal curve position is illustrated by changing the interaction parameters in reasonable ranges.

研究结果表明：与传统方法相比，采用ScCO_2诱导相转化法可获得更高的膜孔隙率；通过改变操作参数可对膜的结构进行调控，且操作参数对膜结构的影响与铸膜体系的自身性质也紧密相关；在适宜的操作条件下，ScCO_2诱导相转化法能有效避免采用传统的浸入沉淀相转化法制膜时易出现的大空腔结构；泄压过程中CO_2气核从聚合物膜基体中逃逸的速度能否与膜基体外部的泄压速度保持同步，是泄压时间对不同材质膜结构影响截然不同的根源所在。

The invention discloses a dielectric hole-microhole composite material and synthesizing method in the inorganic porous material, adsorbing material and catalytic material technical domain, which comprises the following steps: adopting zeolite molecular sieve as raw material; reacting with sodium bisilicate solution under 30-60 deg.c for 10-300 min; disintegrating particle part of zeolite molecular sieve into piece with microhole structure; adding cetyl trimethyl ammonium bromide as molder; adjusting pH value of mother liquid to 10-12; aging 1-8h; adding in the high-pressure autoclave to do water heat synthesizing reaction at 80-130 deg.c for 24-72h; separating solid; washing; drying; sintering under 500-600 deg.c for 5-10h; obtaining the Si-Al porous material with dielectric hole and microhole composite structure.

本发明属于无机多孔材料、吸附材料和催化材料技术领域，涉及具有介孔-微孔复合材料及其合成方法。其特征是以沸石分子筛为原料，用偏硅酸钠的水溶液在30～60℃反应10～300分钟，使沸石分子筛的颗粒部分解离形成具有微孔结构的碎片，加入模板剂十六烷基三甲基溴化铵，然后调节母液pH值为10～12，老化1～8小时，然后加入高压釜于80～130℃进行水热合成反应。反应24～72小时后，分离出固体，水洗、干燥，然后于500～600℃焙烧5～10小时，得到具有介孔和微孔复合结构的硅铝多孔材料。本发明的效果和益处是所发明的合成方法可用于合成多种沸石结构和介孔结构的复合材料，所合成的材料经过质子交换可以具有较强的酸性，在吸附和催化领域具有广泛应用前景。

Unique for features of the ZWB555 straight pattern blobbed gives improved flow measurement accuracy and lower head loss characteristics compared to "Y" pattern globes, all and plug style balancing valves.

与Y形截止阀结构、球阀结构和旋塞阀结构平衡相比，ZWB555直线形截止阀结构平衡阀的独特功能，改善了流量测量的精确度，减少了压头损失。

According to the result, we believed that the reason resulted in the low sensitivity was that the marker residue compound MQCA structure has changed after conjugated with protein and the antibody induced by the conjugation could not recognize the free MQCA in the ci-ELISA. Therefore we designed some hapten which could reserve the marker residue structural speciality mostly. After synthesis route selection and optimum, the hapten 7-Hydroxymethyl-3-methyl-quinoxaline-2-carboxylic acid was synthesized, used 4-methyl-2-nitroaniline as the start material via six steps, such as oxidation cyclization, bromize reaction, hydrolysis, Beirut reaction, reduction, hydrolysis. This work established basis for producing the high affinity antibody and developing the sensitive ELISA residue detection method.

本论文认为导致ELISA检测灵敏度较低的原因，是残留标示物和蛋白偶联后的特征结构发生改变，诱导产生的抗体不能够对游离MQCA很好的识别，因此，本论文设计了能够最大化保留MQCA结构特征的系列半抗原结构，并对其合成路线进行了筛选和优化，最终以对甲基邻硝基苯胺为起始原料，经氧化环化、溴代、水解、Beirut缩合、还原、水解六步反应制备含羟甲基结构的MQCA衍生物7-羟基甲基-3-甲基-喹噁啉-2-羧酸，为制备对游离残留标示物高亲和力的抗体，高灵敏度的ELISA残留检测方法的建立奠定基础。

Afterwards, the crash process of the thin-walled structure is simulated to find the effect of the cross section, the thickness and the pre-deformation on the crash capacity, and the axial impact deformation of the circinal tube is analyzed in the theoretical way, the axial impact deformation of the square tube and subulate tube are analyzed by simulation.

最后本文建立了原DF_(8B)机车车体正面碰撞刚性墙的仿真模型，在分析碰撞结果后，对原DF_(8B)机车车体的底架和司机室结构进行了改进；并利用薄壁圆管和锥形结构设计了吸能装置，利用凸凹相见的防爬板设计了防爬装置；对安装了吸能装置和做出结构改进的耐碰撞DF_(8B)机车以10m/s和15m/s速度正面撞击刚性墙进行仿真，结果表明碰撞时吸收装置先于车体主结构破坏，吸收碰撞能量，其吸能能力达到了国外有关标准的要求。

2The static behavior of one prestressed spatial truss string structure is analyzed systematically in this paper. The change of the structural internal forces and displacements with the rise-to-span ratio, sag ratio, prestress and the number of brace struts is studied and the influence of these parameters on the mechanical behavior is discussed compressively in detail.

2对一张弦立体桁架结构的静力性能做了系统分析，研究了结构的内力和位移在矢跨比、垂跨比、预应力和撑杆数不同参数下的变化情况，全面详细的探讨了结构的主要参数对结构静力性能的影响。

Our calculated results show that the relative stability of the isomers depends on the level of theory used: in the framework of DFT, Au10 trends to form planar structures, while the MP2 calculations show that the three-dimensional isomers are energetically more favorable. Based on the present results, Au10 may be conjecturably a critical species of gold clusters which bridges the planar structures and three-dimensional ones.

计算结果表明Au10团簇异构体的相对稳定性明显依赖所使用的理论方法和泛函，密度泛函结果显示Au10倾向于采用平面结构，且不同的泛函给出异构体的相对稳定性次序也不相同，而MP2计算则显示三维空间结构的Au10团簇更稳定， Au10可能是金团簇从二维结构到三维结构演化的一个临界点。

This paper discusses the characteristics of the portal frame building constructer and studies optimization method to design them.The systematic analysis of the portal frames steel structural characteristics is done in section 2. And in section 3 and section 4, the structural optimization design is introduced based on the principles of finite element analysis and the technology of Object Oriented Programming in the software ANSYS.

本文系统地分析研究了门式刚架钢结构的特点，在此阶段，以有限元为基础，借助大型有限元ANSYS面向对象程序设计技术进行优化设计，研究基于功能强大的ANSYS作结构优化设计的问题：提出有效的设计变量、优化目标函数(以降低结构重量、充分发挥材料性能为目标)，编写APDL优化程序控制文件，在ANSYS程序上实现门式刚架结构优化设计。

This thesis classifies the traditional market structure into three kinds on the basis of contestable market theory .

在可竞争理论的基础上，将传统的市场结构进行了调整分类，将其分为行政性垄断的市场结构，竞争性的市场结构和过度竞争的市场结构。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。