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Accurate measurement crystallize water quantity of CuSO4 crystal with iodometric methods ...

硫酸铜晶体所含结晶水的测定,常用加热失重、微波加热等方法。

Thermochemical study shows the loss of lattice H2O at 60°C and then the coordinate H2O.

热重分析表明,晶体约在60°C开始失去结晶水,紧接着开始失去配位水。

LiBOB was synthesized by an improved solid-state method. H2C2O42H2O was dehydrated to get anhydrous H2C2O4, and H2C2O42H2O was mortared with LiOHH2O. The mixture of H2C2O4 and LiOHH2O was preheated at 60 ℃ for 2 h before adding H3BO3 in several times to be mortared. In vacuum dryer, the mixture of the three starting materials was preheated in two steps: at 70 ℃ for 6 h and then at 100 ℃ for 3 h.

用改进的固相法合成一种新型电解质锂盐-双乙二酸硼酸锂:首先将脱去结晶水的H2C2O4与LiOHH2O研磨混匀,在60 ℃预热2 h后分批加入H3BO3,然后,于真空条件下在70 ℃和100 ℃分别保温6 h和3 h,得到LiBOB粗产品。

LiBOB was synthesized by an improved solid-state method. H2C2O4·2H2O was dehydrated to get anhydrous H2C2O4, and H2C2O4·2H2O was mortared with LiOH·H2O. The mixture of H2C2O4 and LiOH·H2O was preheated at 60 ℃ for 2 h before adding H3BO3 in several times to be mortared. In vacuum dryer, the mixture of the three starting materials was preheated in two steps: at 70 ℃ for 6 h and then at 100 ℃ for 3 h.

摘 要:用改进的固相法合成一种新型电解质锂盐——双乙二酸硼酸锂:首先将脱去结晶水的H2C2O4与LiOH·H2O研磨混匀,在60 ℃预热2 h后分批加入H3BO3,然后,于真空条件下在70 ℃和100 ℃分别保温6 h和3 h,得到LiBOB粗产品。

Outside the hotel is a tropical island with crystal waters, white sand and the soothing sun.

旅馆外面是热带岛屿与结晶水,白色的沙滩和宁静的太阳。

In the third chapter, eight new complexes of 4, 6-dimethylpyrimidine 2-thioacetic acid with rare earth metals has been synthesized and characterized by means of elemental analysis, molar conductivity, IR,〓 NMR and TG-DTA. The general formula of the complexes is Ln〓(n=4 or 5). In the complexes, the deprotonated ligand coordinated to the rare earth metal ions in chelate bidentate mode. 4 or 5 molecular of crystal water existed in the complexes.

第三章合成了八种4,6-二甲基嘧啶-2-硫代乙酸的稀土配合物,通过元素分析、摩尔电导、红外光谱、核磁共振氢谱和热重-差热对配合物进行了表征,研究结果表明,配合物的组成为Ln〓n=4或5),在配合物中配体羧基脱去质子后采用螯合双齿的方式与稀土离子形成配位键,同时,配合物中含有4或5个结晶水

In process of zinc norfloxacine by two-step, the reaction between sodium hydrate and zinc sulphate can be avoided to improve the quality of products. Thermogravimetry shows there is the crystal water of 3 molecules in the zinc norfloxacine. Complexometry can be used to assay zinc norfloxacine.

结论采用两步法合成氟哌酸锌可以避免NaOH与ZnSO4的反应,使产品质量得以提高;通过热重量分析,表明氟哌酸锌分子中含有3分子的结晶水;络合滴定法可作为氟哌酸锌的检测方法。

It is easy to absorb the moisture, and can be soluble by absorbing the water in the air. The water-free Zinc Chlorideis easily soluble in water. It is soluble in ethanol ,acetone and

易吸潮,能自空气中吸收水分而溶化,氯化锌水合物有1、2、3、4个结晶水,无水氯化锌极易溶于水中,能溶于乙醇、丙酮和丙三醇中,具有腐蚀性,并具有使纤维素润胀的性质,有毒性,灼热时,有浓厚白烟生成。

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