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Analytical results of differential scanning calorimetry DSC and X-ray diffraction XRD indicated that after compression molding,the melt temperature of PLLA crystals decreased while the degree of crystallinity increased.

差示扫描量热DSC分析和X-射线衍射XRD分析表明PLLA模压成棒后,PLLA的结晶熔点下降,微晶尺寸变小,而结晶度增大。

He thermal shrinking mechanism of high shrinking PP fiber and change of the super molecular structure in the shrinking process was studied by means of wide angle X ray diffraction and micropolariscope.

运用X-光衍射仪、偏光显微镜及其复合测试技术,对高收缩聚丙烯纤维热处理前后超分子结构变化和纤维热收缩机理进行了研究,结果表明:高收缩聚丙烯纤维必须具有大量高取向非晶区,少量结晶区,结晶度低,晶粒尺寸小,近晶型晶胞。

The effective energy barrier for non-isothermal crystallization was estimated as a function of the relative degree of crystallinity using the isoconversional analysis of calorimetric data.

能源的有效屏障非等温结晶估计作为一个功能的相对结晶度使用isoconversional分析热数据。

Results showed that the structure and property of needle coke could be improved by magnetic field and ultrasonic capitation, such as degree of order, degree of graphitization and crystallinity. Comparatively speaking, the effect of magnetic field was greater.

结果表明:超声空化和磁场诱导均能有效提高针状焦的有序度、石墨化度与结晶度,相比较而言,磁场的影响更大。

The relationship between crystallinity and crystal size of illite or chlorite can reflect the behavior and mechanism of deformed rock.

伊利石和绿泥石平均结晶大小与其结晶度之间的关系可以反映岩石变形的机制和行为。

XRD is applied to characterize the crystal form of the products and analyze the effect of crystallinity on solubility.

用X射线衍射仪对产物结晶形态进行表征,分析了结晶度对水溶性的影响。

The crystallinity of the starch and its derivatives have a direct effect on the applications of its products.

淀粉及淀粉衍生物结晶性质及结晶度大小直接影响着淀粉产品的应用性能。

Both the structure and dimension of PP crystalline and the crystallinity change of PP phase were measured by carrying out Wide Angle X-ray Diffraction.

应用X射线衍射测定并计算了共混物中PP相的结晶结构、晶体尺寸和结晶度的变化。

Themain contents of this dissertation are as follows:(1) The quality analytiedal results of chitosan are as follows: water for 15.205%;degree of deacetylation 92.671%; the weight average relative molecular weight ofchitosan 195900; the viscosity average relative molecular weight of chitosan 194100;and the decomposing temperature 298℃. The infrared ray IR spectra of chitosanshows that the feature-absorbing band of chitosan amido was 1601cm~(-1), that ofβ-indican bond was 986cm~(-1). The results of the X-ray diffraction of chitosan indicatesthat its degree of deacetylation and degree of crystal are both big.

本文的主要内容如下:(1)对壳聚糖的质量进行分析,其水份为15.205%,脱乙酰度为92.671%,重均分子量为195900,黏均分子量为194100,分解温度为298℃,壳聚糖的红外光谱表明,壳聚糖—NH_2的特征吸收峰为1601cm~(-1),β-糖苷键的特征吸收峰为986cm~(-1),壳聚糖的X-衍射图表明壳聚糖原料的脱乙酰度和结晶度均较大。

Results of DSC determinations show that an adequate content of atactic polystyrene is favourable of the crystallization of isotactic polystyrene,but the addition of more aPS linearly decreases the crystallinity of iPS because of the dilution effect.

DSC测定表明,产物中的无规物有利于等规聚苯乙烯结晶,但对结晶的熔点有降低作用。向产物加入更多的aPS则由于稀释效应而使iPS的结晶度线性下降。

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