结晶化

Block-copolyimide film from pPDA/ODA-PMDA was studied by TEM, SEM, PLM, ultra-deep three-dimensional microscope, TMA, and WAXD, which showed that the extensile strength and modulus of b-PI film were higher than that of irregular copolyimide film. It was also revealed that there was a large amount of crystallite formed in b-PI film, which was mainly attributed to its chain structure: rigid pPDA-PMDA chains were easy to form crystal nucleus because of phase separation, based on which semi-rigid PMDA-ODA molecular chains began to crystallize.

以pPDA／ODA-PMDA型嵌段共聚酰亚胺薄膜为对象，借助TEM、SEM、PLM、超景深三维显微镜、TMA、WAXD等手段，研究结果表明：b-PI薄膜的拉伸强度、弹性模量均高于无规共聚酰亚胺薄膜；b-PI薄膜中形成了大量的微晶，这是由于刚棒状的pPDA-PMDA分子链段因相分离容易形成晶核，然后半刚性的PMDA-ODA分子链段以PMDA-pPDA为晶核进行晶体生长造成的，而且ODA-PMDA分子链的结晶和酰亚胺化反应基本上是同步进行的。

It is shown that the porous particles are less energyconsuming to fluidize and, with their contents varying from 5%～25% in the riser, the minimum fluidization velocities based on gas stream are from 0.87×10-3 m/s to 2.2×10-3 m/s, while the critical transport velocities are from 1.0×10-2 m/s to 1.6×10-2 m/s for the operation with no liquid circulation or from 5.2×10-3 m/s to 7.1×10-3 m/s for the condition with liquid circulation.

例如，流化床电极、造粒、砂滤、结晶、浮选、聚合、煤气化、费-托合成[1]等。废水处理中三相流化床的应用得益于生物工程中的生物膜法和化工操作中的流态化技术的成功结合，主要优点为宏观混合程度高，固相内扩散阻力低，液体和固体外部传质阻力小，微生物浓度高。

The better reaction conditions are as follows: Reaction temperature is 40°C, Reaction time is 5 hour; the ratio of L - phenylalanine to acetic acid and N - formyl - L- aspartyl anhydrideis 1:10.2:1.1, Its yield is 95.4%.

在查阅文献的基础上，得到较优的α-L-天冬氨酰L-苯丙氨酸甲脂盐酸盐的合成方案，在甲醇一水体系中，N-甲酰-α-L-天冬氨酰-L-苯丙氨酸在浓盐酸的作用下60℃水解90分钟，后冷却到15℃加入浓盐酸在20～30℃保温反应96小时，进行甲脂化，形成甲脂盐酸盐，结晶析出。

Microencapsulation technology is a new and high technology in the food industry. The microencapsulation nutrition fortifier of serial food is the crystallization of this new and high technology. It takes various nutrient in a microencapsulation .The products take the form of uniformity powder. That make the material in the bag relatively isolated with the external effectively.

微胶囊技术是食品工业中的一项高新技术，微胶囊化系列食品营养强化剂就是这项高新技术的结晶，它是将各种营养素包封在一个非常微小、封闭的微胶囊中，产品呈均匀的粉末状，使囊内材料有效地与外界相对隔绝。

Hydrastine(97.7%) was obtained with extracted rate 65%by extracting the Goldenseal with mixed Solvent;Berberine hydrochloride (99.9%) was obtained by adding hydrochloride acid to alcohol (alcohol∶H 2O=1∶1) solution of the extract and Hydrastine (99.5%) was gained by CLC method with the yield 1%.

原药材用混合溶剂直接提取分离，可得到含北美黄连碱 97.7%的结晶体，提取率达 6 5%；提取物经醇水溶解、酸化，可直接获得小檗碱盐酸盐结晶，纯度达到 99.9%；用柱色谱法，可得到 99.5%的北美黄连碱，收率约 1

Preparation of a high-strength α-hemihydrate gypsum based on complex pastern material is studied by using a complex active agent of industrial waste to improve the crystal properties of hemihydrate gypsum and to eliminate impurities' effect on the properties of products of phosphorous gypsum ,such as phosphorous and fluorine.

以磷石膏为基体原料制备高强α-半水石膏基复合材料，利用工业废渣中的激发剂来改进半水石膏的结晶性质，以消除磷石膏中磷、氟等杂质对磷石膏制品性能影响，同时激发剂使具有潜在活性的矿渣得以活化，制备的低温陶瓷化磷石膏基复合材料制品兼具陶瓷和石膏性能；SEM图片表明，制备的复合材料水化后晶体结构粗大、致密

The henze 2 speer method is used to prepare the 52 substituted hydantoin ramification.

反应6 h后，加入盐酸酸化，继续加热 8 h ，冷却后过滤得到的固体用酒精和水的混合溶液重结晶，得到无色晶状目的产物。

The results indicate that the flow stress of the alloy increases with increasing strain rate and decreasing deformation temperature. The flow stress increases with increasing strain until the stress reaches the peak value, then the flow stress remains constant, which indicates that dynamic recrystallization happens during deformation. The flow behaviors are described by the hyperbolic sine constitutive equation, and the activation energy calculated is 337.75 kJ/mol. The as-forged microstructure consists of refined α2/γ and γ grains, and the grains are much homogeneous than before. The B2 phase distributes uniformly at the grain boundary of α2/γ and γ grains. The B2 phase decreases with increasing deformation temperature.

结果表明：流变应力随着应变速率提高和变形温度降低而增大；在变形过程中，流变应力随着变形量增大而增大，当流变应力达到峰值后趋于平稳，表明合金在变形过程中发生了动态再结晶；热变形过程的流变应力可采用双曲正弦本构关系来描述，平均激活能为337.75 kJ/mol；从合金的组织演化过程中可以看出，合金中不均匀的原始组织得到明显均匀化，变形后的组织是由α2/γ层片晶团和γ晶粒组成的双态组织，在α2/γ层片晶团和γ晶粒的晶界交界处发现分布均匀的B2相，并且随着变形温度升高B2相数量逐渐减少。

Using the method of linear response theory in lattice dynamics on the basis of Tyson's model, the response displacements of atoms on cleavage plane at the incipience of brittle fracture was derived and an expression for evaluating brittle fracture surface energy of metals was found.

本文在Tyson模型的基础上，应用点阵动力学线性响应的理论方法，导出了脆断发生时解理面上原子的响应位移，并进而给出金属脆断表面能的计算公式。这种处理方式既保持了解理断裂面是结晶的表现，避免了局域"熔化"和"沸腾"模拟脆断的简单模型中出现的非晶化问题，也对解理面上原子临界位移做了合理估计，避免了人为规定临界位移的随意性，同时，从理论上得出的脆断时产生的声发射信号与实际探测到的量级相近。

This paper consists of studies of synthesis, structure, physico-chemical and catalytic properties of nickel substituted mica montmorillonite .

在本文的第一部分，我们通过改变不同的配料条件和晶化条件，考察了这些因素对NiSMM结晶的影响。

Fancy gold-plated dangling earrings with facetted White Opal crystals.

花式镀金悬垂耳环与facetted白欧泊水晶。

This essay chooses the study aim from biology teachers in middle school in Shi Jiazhuang which tells us that most of the middle school biology teachers in Shi Jiazhuang have the"burnout", lower successfulness, individualize.

本文选取石家庄市初中生物教师作为研究对象，运用问卷调查的方法对石家庄市初中生物教师职业倦怠的现状进行调查，调查结果发现，石家庄市初中生物教师这一群体普遍存在职业倦怠，情感枯竭程度偏高，成就感偏低，去个性化程度最为严重。