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Crystallization behavior of isotactic polypropylene were studied and observed by polarizing microscope,and also compared to that of PP/MMT composites.

采用偏光显微镜对全同立构聚丙烯等温结晶行为进行系统的研究,并与聚丙烯/蒙脱土复合材料的结晶行为进行比较。

Molecular Formula and Molecular Weight : C27H32O14; 580.53Melting Point and solubility: When crystallized from water ,it contains 6 to 8 mol H2O, mp 83℃. After drying at 110℃ to constant weight, it contains 2 mol H2O, mp 171℃. Sol in methanol,alcohol, acetone, warm acetic acid,dil alkali and hot water.

熔点及溶解度:纯品柚皮甙中结晶水的含量及其熔点因结晶和干燥方法而异,以水作溶剂结晶所得柚皮甙分子中含6~8个结晶水,熔点83℃;而在110℃下干燥至恒重后得到的柚皮苷分子含有2个结晶水,其熔点升至171℃。

Synthetic nitro-musks are used in the most wide area recently and industrial crystallization is the most important process to separate solid mixtures such as perfumes. In order to develop new crystallization process to separate synthetic nitro- musks, the phase equilibrium of musk ketone, musk xylene and 1,3-dimethyl-2, 4- dinitro-5-tert- butyl benzene were studied.

合成硝基麝香是用量最大的合成麝香而工业结晶是分离香料等固体产品的重要方法,为了开发麝香体系结晶分离新工艺,本文首先研究了酮麝香、二甲苯麝香和1,3-二甲基-2,4-二硝基-5-叔丁基苯的相平衡关系。

It was found that the inorphology ofsulfates is related to the orientation of tetrahedral [SO4]2- in the crystal, i.e., the faces, the edges and faees of the tetrahedra normal to, are expected to grow slowly and observed in final form; in contrast, the faces, the vextices of the tetrahedra pointing to, usually grow fast, and will disappear.

晶体的结晶形貌与[SO4]2-四面体在晶体中的结晶方位密切相关,四面体的面和棱的法线( L 2)所对向的晶面,生长速率慢,顽强显露,均属晶体的板面;四面体的顶角所指向的晶面,生长速率快,显露面积小,经常消失。

The injection moulding shrinkages of HDPE/LLDPE blend and its blend filled with CaCO3 were studied.

研究了高密度聚乙烯/线性低密度聚乙烯共混物及其碳酸钙(CaCO3)填充体系的注射成型收缩率,分别用示差扫描量热仪和AR2000高级流变仪分析测定了共混物的结晶度和熔体黏度,并探讨了不同配比下共混物结晶度和熔体黏度与成型收缩率的关系。

The injection moulding shrinkages of HDPE/LLDPE blend and its blend filled with CaCO3 were studied. The effects of the crystallization and melt viscosity of the blends with different mass ratio on the shrinkage were analyzed by means of DSC and advanced AR2000 rheometer.

研究了高密度聚乙烯/线性低密度聚乙烯共混物及其碳酸钙(CaCO3)填充体系的注射成型收缩率,分别用示差扫描量热仪和AR2000高级流变仪分析测定了共混物的结晶度和熔体黏度,并探讨了不同配比下共混物结晶度和熔体黏度与成型收缩率的关系。

Spinel is a compound of magnesia and alumina(Al2O3) and is thus a magnesium aluminate(MgAl2O4), found as accessories in igneous rocks, in metamorphosed aluminous schists, in contact metamorphosed limestones and sometimes in high temperature iore veins.

尖晶石主要成分是氧化镁和氧化铝,结晶习性是等轴晶系漂亮的正八面体。镁被铁置换就是铁尖晶石,被锌置换就是锌尖晶石,铁完全置换镁形成磁铁矿,铬置换铁尖晶石形成铬铁矿,这些类质同相的等轴晶系都是八面体结晶的尖晶石族矿物。

Coenzyme Q10 is obtained through saponification, extraction with petroleum benzine, chromatography with silica gel and crystallization with ethanol.

采用醇碱皂化法,经石油醚萃取、硅胶柱层析,无水乙醇结晶、重结晶得到辅酶Q10。

We have successfully synthesized two high-performance polys, 6F-PEEK and m-TPEEK.

但无定形区的老化并不能从根本上影响较高结晶度的PEEK的结晶行为,无定形区的总量没有明显变化。

In this bath, maleic acid was an inhibitor, when its concentration was kept at 20 mg/L, the deposition rate could reduce to 6.17μm/h, the content of nickel decreased to 1.74% and the resistivity was 7.51μΩ·cm; Potassium ferrocyanide inhibited deposition of copper, when its content was 0.5 ppm, the deposition rate decrease to 3.38μm/h, the content of nickel was 2.03%, the resistivity can reduced to 5.41μΩ·cm, the copper deposits also had higher (111) plane orientation. Thiourea was also an inhibitor in this system, when its concentration was kept at 0.8 ppm, the deposition rate was 4.72μm/h, the content of nickel in the film was 1.20%, the resistivity can reduced to 5.46μΩ·cm, at the same time, the deposition at (111) plane orientation become more favorable.

结果表明,马来酸在该体系中是抑制剂,当其浓度为20 mg/L时,镀速降为6.17μm/h,镀层镍含量降为1.74%,表面电阻率降为7.51μΩ·cm,铜层颗粒细小均匀,更有利于在(111)面上的结晶;亚铁氰化钾的加进可以明显降低镀,当其浓度为0.5 ppm时,镀速为3.38μm/h,镀层镍含量降为2.03%,表面电阻率降为5.41μΩ·cm,铜层颗粒细小均匀,(111)晶面衍射峰增强;硫脲在体系中也显示为抑制剂,当其浓度为0.8 ppm时,镀速降到4.72μm/h,镀层镍含量为1.20%,表面电阻率降为5.46μΩ·cm,形成的铜颗粒很小,同时(111)晶面衍射峰增强,有利于铜在(111)面上结晶

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