结晶

The drying and crystallizing of polyesterpellets in fluidized bed were trends of development for PET solid state polycondensation .

聚酯切片的含水量和结晶度明显影响后续的固相缩聚过程，采用特殊流化床进行干燥和结晶处理是发展方向。

Through a variety of resin filter, adsorption and elution conditions for the optimization, as well as decolorization, crystallization methods of research, this article eventually determine the strong acid cation resin HZ-001 which is at pH 3, 3BV / h, having the largest adsorption to the tryptophan; the fermentation broth were centrifuged to remove sediment,then treated with activated carbon to be decolored and then treated with strong acid cation resin HZ-001. After that,2mol/l amino acid were passed through the HZ-001 ion exchanging column,kept almost constants when the flow rate stayed 6 BV / h. At 60℃,it was condensed into the saturated state and then added Ethanol until its percentage reaching 30%. At 4 ℃ under 100rpm placed in the shaker 20h, the collection of L-tryptophan was dried up in vacuo.

本文通过对种树脂的筛选、吸附和洗脱条件的优化，以及对脱色、结晶方法的研究与摸索，最终确定强酸型阳离子树脂HZ-001在pH=3，3倍床体积流速，温度室温，对色氨酸有最大的吸附作用；将发酵液离心去沉淀并用活性炭脱色后通过HZ-001强酸型阳离子交换树脂柱，再用2mol/L的氨水6倍床体积流速在室温下进行洗脱，收集洗脱液，60℃浓缩为过饱和状态后加入30%无水乙醇，4℃下100rpm摇起晶20h，过滤搜集结晶并真空干燥得白色粉片状L-色氨酸晶体。

In this work, an attempt was made to use ultrafiltration to replace conventional resin decoloring unit operation.

在实验中使用了切割分子量为4960.5u的超滤膜，实验结果表明超滤是取代树脂脱色的有效手段，可以充分纯化土霉素结晶液并改善结晶，脱色过程收率由树脂法的95.3%提高到98.6%。

Result: The anticancer active component includes: taxol 9.45%、cephalomanine: 9.63%、10- deacetylbaccatinⅢ: 22.64%、total flavonoids: 19.15%. 3. The preparation of Seiadopitysin control Methods: Take dry Ginkgo leaves and extracted three times by sonication with 95% EtOH, solutions were concentrated under vacuum, after defatting by petroleum benzin, the sample was extracted with EtOAc and the solutions were concentrated under vacuum.

金松双黄酮对照品的制备方法：取干燥银杏叶以95％乙醇超声提取3次，提取液合并，减压浓缩，石油醚脱脂后，用乙酸乙酯萃取，萃取液减压浓缩，经硅胶柱(6cm×80cm)层析，石油醚-乙酸乙酯(9∶1～5∶5)梯度洗脱，产物用甲醇多次冲淋，再以二甲基甲酰氨溶解，反复重结晶，得黄色粉末结晶。

Lithologies are mostly sand and carbonate rocks, caps are mud rock, shale and magmatite. Entrap types are anticline, fault block rebuilt by breaking and the screened entrap diapered rock mass. The composition is CO_2, N_2, CH_4, C_2H_6 and He etc. It is magma air source body and its geologic fashions are intrusion and buried volcanic conduit. The relations between gas reservoirs and gas source bodies have three types: magma intrusion-breaking-communicated gas reservoir, magma intrusion-contacted CO_2 reservoir and buried volcanic conduit-contacted gas reservoir. The CO_2 migration in magma intrusion is consisted of fusing and crystallizing phases;it in volcanic conduit is consisted of near-surface effusion and crystallizing phases.The buoyancy of CO_2 in water far more than migration resistance in breaking or chink, CO_2 is easy float upward, the floating can results in differentiation of different density gases and concentration of sealed gas. The gas in sand reservoir firstly migrate into the higher porosity and coefficient of permeability sand, and along with the pressure going up it migrate into the lower. In magma intrusion-breaking-reservoir migration, CO_2 firstly migrate into watered breaking, began gravity differentiation and concentrate, the gas pressure time and again go up, CO_2 migrate into reservoir and concentrate under expansibility as the pressure reach upward a given extend. The CO_2 in reservoir experience four breaking modes: chemistry deposition, dissolution, diffusion and mechanic breaking, the pressure balance can be broken by faulting and the CO_2 will further migrate and form new reservoir.

济阳坳陷已发现的八里泊、阳25、平方王、平南、高青、花17 CO_2气藏主要储集层位有奥陶系、中生界、沙四段、沙三段、沙一段、馆陶组和明化镇组，储集层岩性以砂岩和碳酸盐岩为主，盖层以泥质岩、页岩和岩浆岩为主。；圈闭类型主要为受断裂改造的背斜、断块及刺穿岩体遮挡圈闭。；气体成分主要有CO_2、N_2、CH_4、C_2H_6、He等。；主要气源体为岩浆气源体，气源体的主要地质形式为侵入体和埋藏的火山通道。；气藏和气源体的空间关系有岩浆侵入体一断裂一气藏沟通型、岩浆侵入体-CO_2气储集层接触型和埋藏火山通道-气储集层接触型三种类型。；岩浆侵入体CO_2气运移分为熔融运移阶段和结晶运移阶段，火山通道中CO_2气运移分成近地表喷发阶段和结晶运移阶段。；断裂中，CO_2在水中的浮力远大于运移阻力，CO_2气容易上浮，CO_2在断裂中的易浮性导致不同密度气体的分异和走向上封闭的断裂气体相对富集。；气体在砂岩储集层运移聚集具有选择性，会优先进入孔隙度和渗透率较高的砂岩，随着压力增加，才会进入孔隙度和渗透率较低的砂岩；在岩浆气源体-断裂-储集层空间输导格架下，CO_2气在膨胀力的驱动下，首先进入含水的断裂并重力分异而聚集，气体压力会不断增高，当压力增至一定程度，CO_2气会向高孔隙度、渗透率的储集层运移并聚集。；在岩浆气源体-储集层接触空间输导格架下，CO_2气受膨胀力的驱动直接向储集层运移并聚集。；成藏的CO_2气会经历化学沉淀、溶解、扩散和机械破坏四种破坏方式，会受断裂切割而打破压力平衡，沿断裂进一步运移和聚集成藏。

According to temperature, pressure, and chemical evolution of mineral crystallization in the magma chamber, it is held that the magma of intrusive rocks ascended rather fast and was emplaced at the relatively shallow place.

据岩浆房中矿物结晶时的温度和压力条件、矿物的结晶特征及演化趋势，推测岩浆上升速度较快，侵位较浅。

The results showed that the crystallization ratio and time of mold fluxes had great difference at the different temperature.

结果表明：不同的实验温度条件下，连铸保护渣的结晶化率和结晶时间相差很大。

Under the experimental condition, the crystallization ratio of mold fluxes were 100%, and the crystallization time were 262 s and 99 s at 1000 ℃ and 1200 ℃ respectively.

在实验条件下，实验温度为1000，1200℃时，连铸保护渣的结晶化率均达到100%，但结晶时间随着实验温度的上升而减少，分别为

As a consequence, lower gabbros of the oceanic crust could have a larger crystal grain size on average than that of the upper gabbros as seen from the filed observations at the Oman ophiolite.

并试图用这个结果来解释在Oman蛇绿岩套辉长岩层野外实际观测得到的结论：海洋岩石圈底部的辉长岩的结晶颗粒大小的平均值要比浅部辉长岩结晶颗粒大小的平均值高出一个数量级。

As a consequence, lower gabbros of the oceanic crust could have a larger crystal grain size on average than that of the upper gabbros as seen from the filed observations at the Oman ophiolite.Key words Computational Geodynamics Laboratory;Department of Geophysics;Peking University;Beijing 100871;China

并试图用这个结果来解释在Oman蛇绿岩套辉长岩层野外实际观测得到的结论：海洋岩石圈底部的辉长岩的结晶颗粒大小的平均值要比浅部辉长岩结晶颗粒大小的平均值高出一个数量级。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了