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The main object of this research is to investigate synthesis of Cu23Cl Cu and CuO nanoparticles through electrospinning and heat-treated method The research is mainly focused on preparative parameter and the change of heat-treated temperature to form the nanoparticles inlaid in silicon fibers the shape and color change are dicussed First of all to prepare the Polyvinyl butyral and silica dioxide complex nanofiber by electrospinning and then to investigate different heat-treated temperature and reactive time to being an influence on the products The results detected by SEM XRD TEM EDS FTIR combined sol-gel process and electrospinning can prepare Polyvinyl butyral and silica complex nanofiber The experimental result is found when heat-treated temperature is 100~4750C it can produce Cu23Cl nanoparticles; Above 4750C~ 4900C it can produce Cu nanoparticles; Above 450~7000C it can produce CuO nanoparticles And the viscosity is lain between 20~40cp and the sol-gel process time is 3hr it can produce the thinner fibers The average diameter of the fibers are 107 88±21 01nm;Due to the nanoparticles inlaid in the silica fibers the thinner fibers can be inlaid the smaller nanoparticles so this is the result that the experiment is expected To calcine the complex fibers is to produce surface silica fibers contain Cu23Cl Cu and CuO nanoparticles due to surface plasma resonance it make the color of the fibers become yellowish green from light white green turn into the red nuclear finally As the experimental result to utilize sol-gel process combine electrospinning can produce porous silica fibers contain Cu23Cl Cu and CuO nanoparticles

本研究旨在探讨「利用放电纺丝和热处理法来合成Cu23Cl、Cu和CuO奈米粒」之研究,实验著重在制备参数与热处理温度变化对所形成的奈米粒镶嵌在二氧化矽纤维中的形态与颜色变化探讨。首先,利用放电纺丝法制备出聚乙烯醇缩丁醛及二氧化矽之奈米纤维,比较不同的热处理温度与反应时间的改变对产物生成产生影响,进而研究不同热处理温度和时间对生成奈米粒的影响。产物经由SEM、XRD、TEM、EDS和FTIR等仪器分析结果显示,结合溶胶-凝胶法(sol-gel process)和放电纺丝法可产生聚乙烯醇缩丁醛及二氧化矽复合奈米纤维。实验结果发现,若热处理温度在100~4750C下可得到Cu23Cl奈米粒,475~4900C 可得Cu奈米粒,450~7000C以上可得 CuO奈米粒。而黏度介於20~40cp间和溶胶-凝胶时间为3hr时,可产生直径比较细的纤维,纤维直径为107 88±21 01nm;且由於奈米金属颗粒镶嵌在二氧化矽纤维中,直径比较细的纤维,可以得到比较小的奈米金属颗粒,这与实验预期相符。而锻烧此复合物产生多孔的二氧化矽纤维并包含Cu23Cl、Cu和CuO奈米微粒时,由於表面电浆子共震关系,而使纤维颜色由淡白黄绿色变成黄绿色,再变红褐色。由实验结果得知,利用溶胶-凝胶法(sol-gel process)结合放电纺丝法和不同热处理温度,可产生Cu23Cl、Cu和CuO奈米粒镶嵌在二氧化矽纤维。

Result: Rhesus BMSC can be got in mass by density gradient centrifugation.; Rhesus BMSC can adhere to PLGA fiber quickly after plant and its growth , division ,proliferration is good; Some cells arrange like rosary on PLGA fiber surface, some cells still form the catenate or flaky cell bridge joined among PLGA fiber.

结果:采用密度梯度离心的方法可得到大量增殖能力强的猕猴骨髓基质干细胞;接种后的骨髓基质干细胞很快粘附于PLGA纤维上,生长、分裂、增殖良好,在PLGA纤维表面形成串珠样排列,部分细胞还形成连接在PLGA纤维间的链状或片状细胞桥。

Among these results, we suggested that the monomer structure play a important role between E-O performances and morphology. Monomer STD02 shows fastest response time, and monomer M3 exhibits slowest one. As a result for roughness, it's the same with response time. From SEM photograph, the beadlike morphology was obtained from monomers without spacers. On the other hand, the filberlike morphology was obtained from monomers with spacers. It's suggested that the more harder structure will lead to the former, and the more softer structure will lead to the latter.

发现 STD02 反应时间最快,而 M3 则是最慢,而粗糙度大小也是与反应时间相符合,最大的是 STD02 而最小的是 M3,在 SEM 下结果显示,各单体所呈现的型态皆为颗粒状且排列均匀,因无含烷链段关系导致形成的型态为颗粒状,论文里有提到另一种单体含烷链段其所形成的型态为纤维状,以结构上来看,越是刚硬之单体所形成的型态都较易为水滴或是米粒状,而结构上越是柔软,所形成的型态都较易为稻穗或是纤维状。

Results: Arthroscopic examination showed that there were synovitis, debris and fibrillation in the joints of ADD with reduction; synovitis, synovial hyperplasia, debris, fibrillation, chondromalacia,fibrocartilage rupture and adhision in the joints of ADD without reduction.

结果:可复性关节盘前移位的病例出现滑膜炎,关节腔内有絮状物,关节结节表面有纤维形成。不可复性关节结节表面纤维形成,关节软骨软化,软骨剥脱,同时伴有纤维粘连。

The amphiphiles, 4-8, can not form reverse bilayers in organic solvent, which result in that the molecular interactions unable to meet the need for hydrophile-lypophile balance, so that they crystallize and exhibit no gelling abilities. The mono-chained L-alanine derivatives, 1-3, can self-assemble into bilayer aggregates, through intermolecular hydrogen bonding and homochiral effect in a number of organic liquids, which are juxtaposed and interlocked by van der Waals interaction, and finally gelate the organic liquids.

单链酰基化L-丙胺酸两亲物1-3在一些低极性的有机溶剂可以通过分子间氢键相互作用及同手性聚集作用形成有序的反双分子膜结构,这些有序反双分子膜结构单元依靠vander Waals力相互作用可以平行排列且相互之间进行连结形成长纤维状的聚集体,纤维状聚集体在有机介质中可以进一步相互连结形成三维网状结构,进而胶凝有机溶剂。

The psammoma body mineralization in meningioma is a common type of mineralizationThe analysis of the mineral composition may provide some support information in finding the reason of happening and developing of the diseaseThis paper focuses on the concentric layered structure mineralization in meningiomas, using mineralogical methods, such as HRSEM, ESEM, EDAX, EPMA, HRTEM, XRD and FTIR to systematically investigate the mineral composition, structure and shape of the minerals in psammoma bodies in meningiomasWe have devised a method for preparing the silicon wafer sheet which was used for the ESEM insitu observations and analysisIn this study, we first got the ESEM and HRTEM images of the initial mineralization phase of meningiomasThese images showed that in the early stage of psammoma body mineralization in meningiomas, many mineralized balls composed of octocaphosphate were precipitated on the collagen fibersThese balls continued to grow and aggregate, and were gradually hydrolyzed to become the dahlliteThe continued development of mineralization resulted in the mineralized collagen fibersThe study revealed that the concentric layered structure of the psammoma bodies in meningiomas is formed by the spiral arrangement of the mineralized collagen fibers on which the mineralized grains precipitated.

砂粒体矿化是脑膜瘤中常见的矿化类型,对其形成机理和矿物成分的分析可能会对肿瘤发生、发展的研究提供辅助信息。该研究选取人脑膜瘤中的砂粒体矿化作为研究对象,采用偏光显微镜、环境扫描电镜及能谱、X射线衍射仪、高分辨透射电镜和电子探针对样品的形貌、结构和成分进行测试分析,并以此为依据探讨脑膜瘤中砂粒体的形成机理。研究结果表明矿化的初期为沉淀在胶原纤维上的矿化小球,成分为磷酸八钙;矿化小球不断生长聚集,并逐步水解为碳羟磷灰石晶体,矿化的不断发展致使胶原纤维也发生矿化。砂粒体的同心层状构造是由螺旋状排列的矿化胶原纤维及沉淀在其上的矿化颗粒组成的集合体,而不是多数研究中所述:砂粒体是以坏死细胞残骸为中心由内至外的同心层沉淀。

The method according to claim 6, for manufacturing a blade wherein a part external to the shell comprises a blade rooting part having at least one attachment bar, in which an end portion for linkage to a hub of said rotor is fitted with a laminate attachment, also comprising thermoplastic composite, and extending said at least one spar bar housed in the shell, the method further comprising the step of producing the elementary piece comprising the at least one spar by producing each attachment bar and the spar bar in the form of a strip of continuous and unidirectional reinforcing fibres which are agglomerated by said thermoplastic matrix, obtained by pultrusion at a melting temperature of the matrix, of several plies of continuous and unidirectional fibres which are agglomerated by said matrix, and, if said rooting part comprises at least two attachment bars, each one of which respectively extends one spar bar, in superimposing parts of corresponding strips forming the spar part housed in the shell, with interposition of at least one ply of continuous and unidirectional fibres which are agglomerated by said matrix between the adjacent superimposed strip parts, and fitting a removable tool, in the shape of a wedge, between parts held spaced from each other of two neighbouring strips, to form two attachment bars of the rooting part, then arranging the strips in a mould, and inserting each linkage end portion of a pultruded strip between two laminate elements of the attachment, to superimpose all the laminate elements of the attachment, closing the mould and compacting its contents under pressure and at a melting temperature of said thermoplastic matrix, and solidifying the matrix by cooling to rigidify the spar thus obtained with the laminate attachment solidly attached to its rooting part.

该方法根据索赔六,制造业刀片其中的一部分,罐壳外部包括一个叶片生根的一部分,拥有至少一个实习酒吧,在其中一结束部分为联系枢纽的说,转子是带有附件的层压板,也包括热塑性复合材料,并延长说,至少有一石酒吧住在蚬壳公司,进一步组成的方法步骤,生产初级一块组成的至少有一个SPAR公司生产每个附件的酒吧和酒吧在SPAR公司的形式,带不断加强和单向纤维是由烧结说,热塑性矩阵,得到的拉挤在熔化温度矩阵,数层的连续和单向纤维是由烧结说,矩阵,如果说,生根部分组成,至少有两个实习酒吧,每个人都分别延长一石酒吧,在叠加部分,相应的带形成的SPAR公司的一部分,居住在蚬壳公司,与干预的至少有一单层连续和单向纤维是由烧结说,矩阵之间的毗邻叠加条形零件,及装修一个可移动的工具,在形状,离间,部分之间举行的间隔从对方的两个邻国带,形成两个附件酒吧的生根部分,然后安排带在一个模具,并插入每个联系年底部分一拉挤带之间的二板的要素扣押,叠加所有层压板的要素扣押,关闭模具和压缩其内容的压力下和在熔化温度说,热塑性矩阵,并巩固矩阵冷却 rigidify该SPAR公司,从而获得与层压板的附着牢固重视其生根的一部分。

Then introduced a new theory on forming super high-intensity wood-based panel with wood fiber reconsolidated micron technology, at the same time analysed its advantages, discussed the practicability of developing the new panel-MLFB.

回顾了纤维形成方法及纤维板发展历程,分析了传统纤维板形成理论的缺陷,介绍了微米长纤维高强度低密度人造板的形成理论,分析并阐述了该板种的优势,论述了开发研制这一新板种的可行性。

The method includes the steps of gripping the peripheral edge of the fabric in a stretching assembly, activating the stretching assembly to stretch the fabric in a location adjacent to the mold assembly, clamping the stretched fabric against a face of the mold assembly, releasing the peripheral edge of the fabric from the stretching assembly, moving the stretching assembly from the path of the mold assembly, closing the mold assembly on the fabric with the peripheral edge of the fabric terminating in the mold cavity and injecting molten material into the mold cavity to form the frame directly on the peripheral edge of the fabric.

方法包括的步骤为在拉伸装置中夹紧纤维织物的外围边缘、在邻接浇模装置的位置启动拉伸装置来拉伸纤维织物、贴着浇模装置的面夹住已拉伸的纤维织物、从拉伸装置释放纤维织物的外围边缘、从浇模装置的轨迹移动拉伸装置、在纤维织物上闭合浇模装置并使同纤维织物的外围边缘终止在浇模空腔中和将熔化的材料注射到浇模空腔中以在纤维织物的外边缘直接形成框架。

The wear debris of three semi-metallic friction materials reinforced by low carbon steel fiber, brass fiber and pure copper fiber respectively, and grey cast iron couple woren at different temperatures were studied by XRD and EDAX. Wear properties were analyzed together with the surface images got by scanning electron microscope.

摘 要:采用X射线衍射和X射线能谱分析对分别使用低炭钢纤维、黄铜纤维和紫铜纤维增强的3种半金属摩擦材料与灰铸铁在不同温度下滑动摩擦形成的磨屑进行分析,并结合扫描电子显微镜观察摩擦材料表面形貌,分析材料的磨损特性,并对黄铜纤维和紫铜纤维增强的摩擦材料磨屑成分进行对比分析。

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随着死亡的吉他手Schuldiner接受主唱的职务,乐队在现实中树立了重要的影响。

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关闭眼睛,深呼吸,一切不再是梦想,犹如。。。。。。