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We investigated constituent of triterpenoid saponins ofAlbizzia, two new compounds together with two known compounds were isolated from Albizzia julibrissin Durazz. by using column chromatography (macroreticular resin, silica gel, Sephadex gel, reverse phase silica gel),preparative HPLC methods et al.On the basis of spectroscopic analysis, including IR,ESI-MS,~1H-NMR,~(13)C-NMR,HMBC,HMQC,~1H-~1HCOSY and chemical methods, the structure of two new compounds were identified as 3 - O -[β-D-xylopyranosyl(1→2)-β-D-fucopyranosyl (1→6)-β- D -2- deoxy - 2 - acetoamidoglucopyranosyl] -21-O-[(6S)-2- trans- 2,6-dimethyl - 6 - O-β- D - quinovopyranosyl -2,7- octadienoyl] - acacic acid- 28 - O-β-D-glucopyranosyl(1→3)[α-L-arabinofuranosyl(1→4)]-α-L-rhamnopyranosyl(1→2)-β-D-glucopyranoside acacic acid 3- O -β- D- glucopyranosy(1→3)-β- D- fucopyranosl(1→6) [β-D- xylopyranosyl (1→2)]-β-D-glucopyranoside ;two known compounds were acacic acid lactone 3- O -β-D- xylopyranosyl-(1→2)-β-D-fucopyranosl (1→6)- 2-deoxy -2 -acetoamido -β-D- glucopyranoside ; acacic acid lactone 3- O-β-D-xylopyranosyl(1→2)-α-L- arabinopyranosl (1→6)- 2- deoxy - 2- acetoamido -β-D-glucopyranoside . The study lays chemical foundation and chemical reference substance for enhancing quality standard of Albizzia julibrissin Durazz.

本研究论文在综述国内外对合欢属Albizzia三萜皂苷化学成分和药理作用研究进展的基础上,利用传统植化分离手段和现代分离技术,包括大孔树脂、硅胶、葡聚糖凝胶、反相硅胶等柱色谱,制备高效液相色谱法等技术从中药合欢皮中分离得到了4个化合物,其中,2个新化合物和2个己知化合物,并进一步通过现代分析技术IR,ESI-MS,~1H-NMR,~(13C-NMR,HMBC,HMQC,~1H-~1HCOSY等和化学方法鉴定了2个新化合物的结构分别是:3-O-[β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖基]-21-O-[(6S)-2-反式-2,6-二甲基-6-O-β-D-吡喃鸡纳糖基-2,7-辛二烯酸基]-金合欢酸-28-O-α-L-呋喃阿拉伯糖基(1→4)[β-D-吡喃葡萄糖基(1→3)]-α-L-吡喃鼠李糖基(1→2)-β-D-吡喃葡萄糖苷,金合欢酸3-O-β-D-吡喃葡萄糖基(1→3)-β-D-吡喃夫糖基(1→6)[β-D-吡喃木糖基(1→2)]-β-D-吡喃葡萄糖苷;2个已知化合物结构分别是:金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷,金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-α-L-吡喃阿拉伯糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷。

The Research on the Photosynthetic Characteristics of Different Sand Pear Cultivars;2. Four sand pear s,including Jinshui No.

测定了翠冠、金水2号、丰水、金水1号4个不同熟期砂梨品种果实的生长、主要糖酸含量的变化。

To improve the brix to acid ratio in VECO will not decrease its effects on soberness.

而且提高金葛露糖酸比值不会影响其解酒效果。

Currently has a class of calcium agents, such as amino acid calcium, Stachyose calcium, vitamin C calcium are among the elements of calcium, they can be absorbed by the body take the initiative and do not need the help of vitamin D, but it does not take elements of calcium Children do not need vitamin D, because the absorption of dietary calcium of vitamin D is still needed help.

目前有一类钙制剂,如氨基酸钙、苏糖酸钙、维生素C钙等都属于分子钙,它们可以被人体主动吸收,并不需要维生素D的帮助,但并不是说服用分子钙的孩子就不需要维生素D,因为食物中钙的吸收仍然需要维生素D的帮助。

Methods To study the influence of microwave heating to the determination of sodium gluceptate and stannous chloride for injection,and compare with water bath heating method.

考察微波加热对注射用亚锡葡庚糖酸钠含量测定的影响,并与水浴加热进行比较。

300Mg Calcium L-threonate containing 40mg 〓Ca was given to the subjects shortly after intravenous injection of 4mg 〓Ca chloride solution. Urine samples were collected for 48 hours, and purified by precipitation of ammonium oxalate.

研究中,14名受试者在空腹状态下口服〓Ca标记的L-苏糖酸钙咀嚼片(含300mg元素钙,其中〓Ca 40mg),同时静脉注射含有4mg 〓Ca的氯化钙溶液,分段收集给药前和给药后48小时内的全部尿样。

All the chelators are labeled with technetium-99m and further tested for the biological activity in mice.

采用葡庚糖酸钙交换法对 4个配体进行了99Tcm 标记,研究了配合物在小鼠体内的生物分布特征。

Temperature, light, water, which mainly influence on the components of sugar and acid in peach fruit.

糖酸组分及其含量对果实内在品质有着重要的影响,是决定果实风味的重要指标。

You can listen to the wind,whether it blows with majestic voice through a forest or sings a many-voiced chorus around the corners of your apartment building,and in the listeni

海藻——海藻含有丰富的蛋白质、纤维素、维生素和矿物质。而海苔更是含有丰富的可溶性纤维藻糖酸,可以保护人体

Of 12 tomato lines, the analysis on the 4 fruit nourishment quality traits (the contents of vitamin C, total soluble solids and dry matter and ratio of sugar-acid ) was carried out to study the four kinds of disparities, which included the interspecific one, the one between two varieties in the same species , the one between the lines bred by different means in the same variety ,and the one between the different fruit-shaped lines in the same variety .The analytic method of orthogonal comparison of single degree of freedom was applied. The results showed that the line of Lycopersicum pimpinellifolium was better than the average of the lines of L.esculentum in the 4 traits at significant level of 1%, the average of the lines of var.cerasiforme was better than the average of the lines of var.vulgare in the 4 traits at significant level of 5% or 1%,and the two space mutation line(YH02-2 or YH02-6) was better than the average of the other lines of the same variation in the 4 trait, respectively, at significant level of 1%. Of the lines of var.cerasiforme , the lines with pear fruit were lower than the average of the lines with round-shaped or plum-shaped fruits in the 2traits(the contents of vitamin C and total soluble solids), at significant level of 1%,the lines with plum-shaped fruits were higher than the average of the lines with round-shaped fruits, at significant level of 1%,and the lines with yellow-colored fruits(YH02-11) was lower than the average of the lines with red-colored fruits(YH02-1and YH02-7) in the trait of the contents of vitamin C.

对12个品系进行种间、种内变种间、变种内不同选育方式间、变种内不同果实形状间在果实营养品质(果实维生素C含量、可溶性固形物含量、干物质含量和糖酸比)上的差异进行分析,采用统计学上单一自由度正交比较分析法与植物学分类相结合的方法进行分析,结果表明:醋栗番茄种品系YH02-12在4个营养品质性状上,极显著高于普通番茄种品系;樱桃番茄变种品系在4个营养品质性状上的平均水平极显著或显著高于普通番茄变种品系的平均水平;2个空间诱变品系YH02-2、YH02-6在4个营养品质性状上均极显著高于同变种的其他品系的平均水平;樱桃番茄变种品系中,梨形果品系YH02-5、YH02-8的果实维生素C、可溶性固形物含量均极显著地低于樱桃番茄变种中圆形或李形品系的平均水平,李形果品系YH02-9在4个营养品质性状上均极显著地高于圆形果品系的平均水平,黄色圆形果品系YH02-11的果实维生素C偏低于红色圆形果品系YH02-1和YH02-7。

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