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The optimum conditions for making microspheres were obtained via orthogonal experiment with adsorptive capacity as the index as follows: the mass fraction of water phase is 2%(ratio between starch and β-cyclodextrin is 1:2), 110 mL oil, 3.3 g Span60, 6.6 g Tween60, 15 mL water, 18 mL assistant surfactant, 0.07 g metaphosphoric acid trisodium salt. The microspheres were characterized by microscope and the average particle size is about 329.3 nm with productive rate of 41%.

结果表明,质量分数为2%的可溶性淀粉与β-环糊精溶液为水相(二者的质量比为1:2),油相用量为110 mL,水相用量为15 mL,乳化剂Span60用量为3.3 g,Tween60用量为6.6 g,助乳化剂用量为18 mL,三偏磷酸钠用量为0.07 g,制备得到的复合纳米微球在扫描电子显微镜下,微球大小分布均匀,所得纳米微球产率为41%,平均粒径为329.3 nm。

The starch-cyclodextrin microspheres were prepared by using starch/β-cyclodextrin as raw material, normal hexane as dispersed phase, Span60 and Tween60 as emulsifying, pentanol as assistant of emulsifying, and metaphosphoric acid trisodium salt as linking agent.

纳米微球以可溶性淀粉和β-环糊精为原料,选用正己烷为油相,Span60和Tween60为乳化剂,正戊醇为助乳化剂,三偏磷酸钠为交联剂,以对亚甲基蓝的去除率为指标进行了单因素和正交试验。

The technological methods and optimal combination ratio were studied in the present paper, involving protection of natural color, elimination of bitter taste, mixtion and stability of the beverage. By single factor trial and orthogonal test, we optimized the processing techniques: Using 100mg/kg Zinc gluconate and 0.1% Calcium hydroxide as the color protection agent, burned in 80℃for 2min. The natural green color of material can be protected effectively.

通过单因素考察及正交实验设计确定了优化后的饮料制作工艺:以100mg/kg葡萄糖酸锌和0.1%氢氧化钙为护色剂,在漂烫温度80℃,漂烫时间2min条件下,有效地保持了苦瓜原料特有的绿色;以苦瓜皂苷为功能强化因子,以1.25%海藻酸钠为包埋剂,通过锐孔-凝固浴法对苦瓜原汁和苦瓜皂苷进行包埋;使用8%木糖醇、0.3%β-环状糊精、15%苦瓜汁和10%苦瓜胶囊对饮料进行调配,很好地保持了苦瓜特有的苦香味和口感;以0.15%黄原胶、0.2%琼脂、0.05%羧甲基纤维素钠复配方式,来增加饮料的稳定性。

Firstly, a series of organic molecules which use phthalimido group as electron acceptor, N as electron donor, COO~- as eletrofugal group were synthesized based on SET-promoted photocyclization processes. These compounds were irradiated by 500 W ultraviolet under nitrogen atmosphere in room temperature. After filtration of the photochemical character of these molecules, substrate S1 and S2 were selected as appropriate model reactants. Secondly, the monosubstituted derivatives at the 6-position ofβ-cyclodextrin were synthesized as chiral template of photocyclization.

首先,以单电子转移机理为指导,设计了一系列以邻苯二甲酰亚胺基为电子受体、N为电子给体、羧基为离去基团的光环合反应底物,这些化合物在氮气保护下以500瓦紫外光室温下进行光照反应,对这一系列的分子的反应情况进行了研究与筛选,最终选择底物S1和S2作为研究光环合反应中立体控制方法的模型底物;其次,又合成了一系列6-位单取代β-环糊精,以此作为光环合反应的手性模板。

Porous carbons were prepared with tetraethyl orthosilicate as the silica template and solube starch and β-cyclodextrin as carbon precursor by sol-gel method.

以正硅酸乙酯为模板硅源,β-环状糊精和可溶性淀粉分别为碳前驱体,运用溶胶-凝胶法制备了多孔炭材料。

Aim To study the oscillographic behavior of β-cyclodextrin and its application in oscillographic determination .

目的研究β-环糊精的示波行为并将其用于客体分子的示波测定。

Aim To study the oscillographic behavior of β-cyclodextrin and its application in oscillographic determination. Methods The research is based on distance transform.

目的 研究β-环糊精的示波行为并将其用于客体分子的示波测定。

In addition, avermectin was made into the formulation of cyclodextrin inclusion, so as to increase the photostability of pesticide molecules.

另外将阿维菌素制备成合适的环糊精剂型有利于提高农药的光稳定性。

With Platycodon root as experiment material and Platycodon extract,sucrose,citric acid and β-cycloheptaamylose as experiment factors,on the base of Response Surface Methodology Analysis,researches on optimal prescription of Platycodon health protection beverage were conducted.

以桔梗为实验材料,以桔梗提取物、β-环状糊精、蔗糖和柠檬酸为实验因素,利用响应曲面法进行实验设计,对桔梗保健饮料的最佳配方进行研究,并对最佳配方进行感官评价验证,理化指标检测和微生物学检测。

Other applications of the sol-gel technology on textile were discussed in this paper as well, such as ultra-violet cutting, water repellency, weighting of silk and knitting fabrics, fixing the β-cyxlodextin on cotton for"Host-Guest"effect etc.

本论文对溶胶-凝胶技术在纺织上的其它应用进行了初步探索,如抗紫外、拒水、真丝绸和针织物的增重、β-环糊精在织物上的固着、香精的缓释等。

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