精馏的

Main contributions and achievements are as follows:A general non-equilibrium rigorous model for RDP is developed in this thesis. Based on the pseudo-homogenous assumption, two main factors reaction and separation are de-coupled, and an RDP model with the same format as that for a traditional distillation process is established. To solve the model with a large number of algebraic equations, modified M-K equations with tri-diagonal matrix form are developed based on the improved Separation Efficiency Functions, which greatly increases the iteration efficiency. This thesis also develops a general reactive distillation dynamic model. Through splitting of the differential variables based on SEFS, large-scaled differential algebraic equations can be solved with the improved Gear's algorithm which makes the dynamic model suitable for the on-line application. A simulation platform for the control loop design and evaluation of RDP by introducing control system equations into the dynamic model is also developed.A lactic acid purification pilot-scale RDP is investigated.

论文对热点问题——反应精馏过程的建模与优化控制相关技术进行了深入的研究，取得了一系列成果：1、建立了反应精馏过程机理模型，基于拟均相假设，将反应和分离过程进行解耦，推导出反应精馏过程的非平衡级稳态模型和动态模型，通过引入推广的分离效率函数，对模型变量进行了合理划分，显著提高了模型求解效率；将动态模型和控制系统方程结合，建立了反应精馏过程控制系统研究的辅助工具。2、全面分析了乳酸提纯反应精馏新工艺试验装置，利用本文建立的过程机理模型，对该试验装置进行了稳态和动态性能分析及水力学核算；设计和分析了单边质量控制方案，比较了间接和直接物料平衡控制两种方案的控制性能。

In the experiment, compared to atmosphere distillation, low-pressure distillation is proved to be able to save more nourishment, remain more yeast for the fermentation with cornstalk and finally give more energy saving.

与常压精馏相比较，低压低温精馏能够减少醪糟中营养物质的损失，更多地保存了酶活力和发酵菌体的活性，为醪糟进行下一步的秸秆固态发酵饲料生产提供保证；而且有利于进行浓醪精馏，实现大幅度的节能。

The binary and ternary experimental equilibrium data of the composites of mesitylene,1-methyl-2-ethylbenzene and 1,2,4-trimethylbenzene and the infinite activity coefficients γ~∞ are measured in the solvent of DBP .

以邻苯二甲酸二丁酯为萃取精馏溶剂，测定了邻甲乙苯—均三甲苯—偏三甲苯体系的二元及三元汽液平衡数据；编程关联了W ilson模型参数；采用物料平衡三对角矩阵法对萃取精馏过程进行了模拟，得出了萃取精馏塔的最佳操作条件，为萃取精馏法生产均三甲苯提供了基础数据。

Continuous distillation processes including three-tower,four-tower and five-tower for separation of methyl cyanoacetate were proposed to replace the conventional batch distillation process.

针对氰乙酸甲酯传统的间歇精馏分离过程，提出了连续精馏分离氰乙酸甲酯的三塔、四塔和五塔工艺流程，并对3种分离流程进行工艺分析，确定了连续精馏五塔分离工艺。

Fit , the fractions in different temperature ranges were ingathered by rectifying wash oil azeotropic distillation were done with the different fractions and ethanediol respectively .

首先精馏洗油，切取不同温度段的馏分，然后分别与共沸剂乙二醇进行共沸精馏试验；在共沸精馏中，通过改变馏分与共沸剂的质量比和回流比，考察了不同条件对喹啉纯度的影响。

The presumption that new technology about distillation column with a single reactor can be used in photochlorination of acetic acid is first proposed in this paper. The fact that reaction distillation has obvious advantages in the number of theoretically perfect trays and energy consumption was obtained by theoretical analysis between the coupling of reaction and distillation and the independent operation, which lays a theoretical foundation on the application of the distillation column with a single reactor in photochlorination of acetic acid.

本文首次提出了将背包式反应精馏耦合技术应用于乙酸氯化反应的设想，通过对反应精馏耦合和反应精馏独立操作两种情况进行理论分析，发现反应精馏耦合在理论板数、能耗方面均具有明显优势，因而为背包式反应精馏应用于乙酸光氯化反应奠定了理论基础。

On the basis of summarizing separation method of acetic acid-water system, we studied the azeotropic distillation process of acetic acid-water system, selecting butyl acetate, isobutyl acetate and isopropyl acetate as entrainers. The influence of packing height, ratio of water to entrainer and acetic acid initial concentration to separation effect of azeotropic distillation was studied in detail. Simulation calculations of general distillation and azeotropic distillation were carried out. The influence of reflux ratio, theoretical plate, feed position, feed temperature and feed concentration to distillation process were discussed. Preferred process operation parameter, which had guiding meaning to practical production of distillation process were obtained. Basic data for the process amplifying design of azeotropic distillation tower were provided. Invest and operation energy consumption of two distillation methods were compared. The elementary technical design of azeotropic distillation tower was carried out on the basis of result of simulation calculation. The type of major auxiliary equipments and inner parts of packed tower were selected.The research results are as follows:(1) Butyl acetate, isobutyl acetate and isopropyl acetate could be selected as entrainer, and separation effect was near.

本文在综述醋酸-水体系分离方法的基础上，以醋酸丁酯、醋酸异丁酯、醋酸异丙酯为挟带剂，对醋酸水溶液进行共沸精馏过程研究，详细研究了填料高度、水与挟带剂的配比、醋酸初始浓度等对共沸精馏分离效果的影响；对醋酸-水体系进行普通精馏和共沸精馏过程模拟计算，讨论了回流比、理论板、进料位置、进料温度和浓度对精馏过程的影响，获得了对醋酸-水体系精馏过程实际生产具有指导意义的较佳的工艺操作参数、共沸精馏塔的工艺设计放大的基础数据，并对两种精馏方法的投资、操作能耗进行了比较；同时在共沸精馏模拟计算的基础上进行了共沸精馏塔的初步工艺设计计算，并对填料塔的主要辅助设备及塔内件进行了初步选型。

The results show that the three-effect concurrent distillation is the best separation technology in response to the objective function of the ratio of multi-effect distillation expenditures to mono-column expenditures.

并以多效精馏与单塔精馏总费用的相对值最低为目标函数，确定分离甲醇－水体系的最佳方案为三效顺流精馏工艺。

Application of vacuum rectification technology, molecular distillation technology, and high pressure rectification technology in oils and fats industry were reviewed.

综述了精馏技术在油脂工业中的应用进展，主要介绍了减压精馏技术、分子蒸馏技术以及高压精馏技术在现代油脂工业中的应用，并对精馏技术在今后油脂工业的应用前景及发展方向进行了阐述。

By soluting each level respectively, which makecomplex of construcing heat pump distillation process to be a better solution. By analyzing the thermodynamic properties of conventional distillation and heatpump distillation, mathematical model and computational method is established. Byoptimizing method of designing various structures, the most costeffective isdetermined.

通过分析常规和热泵精馏系统的热力学特性，建立了热泵精馏流程数学模型及优化设计方法，针对不同的热泵精馏流程结构采用不同的优化设计方法以获得最大的经济效益；为验证热泵精馏流程的可行性提供有利依据，建立了用于确定热泵精馏热集成方案的经济评价标准；将策略与优化设计算法相结合应用于热泵精馏流程，以实现构建较优热泵精馏流程。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了