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In this paper the applications of mesitylene in dyestuff, medication and chemical industry etc. were summarized. From the literatures, we generalized the merit and defect of all kinds of methods and presented that the method of extraction rectification is effective and worth of research.

本文概述了均三甲苯在染料、医药、化工等令贞域中的应用;针对合成分离均三甲苯中存在的问题,查阅了大量的国内外文献,总结并分析了各种合成分离方法的优缺点,提出萃取精馏方法是生产均三甲苯的一种有效方法。

The experiment gains reaction parameters of methylal from formaldehyde and methanol,it also found a mathematical model for continuous production process.

通过实验取得了甲醛和甲醇合成甲缩醛的反应参数;建立了其连续生产工艺的数学模型,利用ASPEN PLUS软件对甲醛和甲醇缩合生成甲缩醛进行了模拟,结果表明反应精馏连续生产甲缩醛的工艺是可行的,转化率高达99%,并得到含甲缩醛99%的产物,同时确定了进料板和反应区。

The experiment results indicate that: the increases of catalyst concentration, feed mole ratio of methanol to formaldehyde and the decrease of total feed flow can increase the yield of methylal; the concentration of methylal in distillate also increases with the increase of catalyst concentration; that the effects of reflux ratio on the yield and concentration of methylal in distillate are different from conventional distillation process, an optimal value of reflux ratio exists between 1 and 2 for this process.

实验结果表明:回流比对甲缩醛收率和塔顶甲缩醛纯度的影响不同于一般的精馏过程,存在一个最优回流比,本过程最佳回流比在1-2之间;提高催化剂浓度,甲缩醛收率和塔顶甲缩醛纯度均增加;提高进料醇醛摩尔比也会提高甲缩醛收率;进料总流量对甲缩醛的收率的影响十分明显,进料总流量减少可以使甲缩醛的收率得到明显提高。

Secondary variables selecting method based on PCA is researched, and then secondary variables selecting method based on Partial Least-Squares Regression is proposed.

并且研究了基于主元分析的辅助变量选择方法,提出了基于偏最小二乘回归的辅助变量的选择方法,采用两种方法分别对常压精馏塔航空煤油干点的辅助变量进行了选择比较。

Deethanizer right choice is the sieve column, so we Tower Drive, plate spacing, sieve number of openings rate Hydrodynamics sieve has done a serious basis, and make a distillation of the stripper and the load performance of the plan, determine the operating point and the operating line.

对脱乙烷塔选择的是筛板塔,因此我们对塔径、塔板间距、筛孔数、开孔率、筛板的流体力学都做了认真的计算,并且做出了精馏段和提馏段的负荷性能图,确定了操作点和操作线。

The reduced quasi-block tridiagonal matrix simultaneous correction algorithm based on LU decomposition is developed for interlinked distillation columns, which can successfully solve non-tridiagonal matrix caused by connecting stream or recycle stream of the column system.

提出了处理内联精馏塔系统的基于LU分解的压缩型拟块三对角矩阵方程组同时校正算法,解决了由于塔之间存在联接物流或回流而形成的非三对角矩阵方程的求解问题。

Through computer simulation of azeotropy rectification dehydration tower with benzene as entrainer, the optimal technical parameters were obtained as follows:①the output quantity of top tower was 69 kg/h, return benzene phasor as 58 kg/h and reflux ratio as 3, alcohol concentration in charge the higher the better, however, its maximum value influenced by water content at azeotropy point;②sensitivity analysis results indicated that the sensitivity of output quantity of top tower was the highest, alcohol concentration in charge the second and return benzene phasor and reflux ratio the lowest.

对以苯作为夹带剂的共沸精馏脱水塔进行了计算机模拟,得到了最佳工艺参数:①塔顶采出量为69 kg/h,返回苯相量为58 kg/h,回流比为3,进料乙醇浓度越高越好,但其最大值受共沸点水含量的影响。②敏感性分析的结果为塔顶采出量的灵敏度最大,进料乙醇浓度次之,而返回苯相量和回流比较小。

Especially for structured packed columns, which are boomingly used, due to the poor self-distributivity resulted from the lower pressure drop of the structured packing, and the more sensitivity to gas distribution, the influence of gas distribution for structured packed columns is more severe.

特别是目前逐渐被广泛应用的规整填料塔,由于其阻力小,对气体得自分布性能较差,同时有对气体的分布较为敏感,所以气体分布状况会对整个精馏塔的分离效率有较大的影响。

The distillation column with a single photochlorination reactor was built in this paper, which is used in the laboratory study. In light initiation, the semi-continuous operation was applied to study the influence of the chlorine flow, the reflux and the height of the packing on photochlorination of acetic acid. Crude MCA with a purity of 90% or more was attained and the feasibility of this technology was proved.

本文建立了适合实验室研究的背包式光氯化反应精馏耦合装置,采用半连续操作的方法,在光引发条件下,考察了氯气流量、回流量和填料高度对乙酸光氯化反应的影响,得到了含量达90%以上的氯乙酸粗品,证实了工艺的可行性。

Directed against disadvantages existing in the conventional process and an improved process on the basis of test, a continuous recovery process of triethyl amine in producing glyphosate was proposed, realizing continuous neutralization and rectification of mother liquor, and was applied successfully in recovery of triethyl amines in producing 5 000 t/a of glyphosate for Fujian Sannong Group Co.

针对早期的三乙胺回收工艺和在小试基础上改进的回收工艺的缺点,提出了一种三乙胺连续回收工艺,实现了母液连续中和分层及精馏,并将此工艺成功地应用于福建三农集团公司5 000 t/a草甘膦生产过程的三乙胺回收中。关键词:草甘膦;三乙胺;重力层析器

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

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