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The invention provides an anhydrous hydrogen fluoride production process; reaction raw materials fluorite powder and sulfate are mixed by an external mixer and enter into a converter with jacket; hot air with the temperature of 350 DEG C to 600 DEG C is fed in the jacket; the fluorite powder and the sulfate have chemical reaction and produce hydrogen fluoride; the produced hydrogen fluoride enters into a scrubber from a furnace header to be washed; the washed hydrogen fluoride enters into an intermediate tank from a condenser, and then receives distillation and degasification to prepare the finished product anhydrous hydrogen fluoride; solid residue is emitted from a furnace tail.

本发明提供一种无水氟化氢生产工艺,反应原料萤石粉及硫酸经外混器混合后进入带有夹套的转炉,向夹套内通入350~600℃的热风,萤石粉和硫酸在发生化学反应生成氟化氢,生成的氟化氢气体由炉头进入洗涤塔进行洗涤,洗涤后的氟化氢由冷凝器进入中间槽,然后经过精馏、脱气制得成品无水氟化氢;固体残渣由炉尾排出。

Meanwhile, experiment with the ternary mixture of methanol, butyl methyl ether and 1-chlorobytane showed that the system was not ternary azeotrope and can be separated by combination of extractive and rectification using water as extractive solvent.

针对甲醇、甲基正丁醚和正氯丁烷三元混合物,研究了该物系的性质,得到该物系不是三元共沸物的结论,并用水作萃取剂,通过实验验证了利用萃取和精馏耦合的方法分离该物系的可行性。

In chapter 3, in view of the control problems of the distillation columns in the butadiene plant, the advanced control strategy based on soft-sensing technology is designed, and the implementing method based on OPC technology is proposed. Firstly, the control system is reconstructed.

第3 章针对某石化企业丁二烯装置的精馏工段中组分浓度的控制难题,设计了基于软测量技术的先进控制方案,提出了基于OPC 技术的先进控制实现方法。

A scheme for compactification of ammonia water absorption refrigerators, especially for the reduction of the height of the generating rectification column is proposed, which includes using spiral sheet heat exchangers as the generator and the partial condenser of the refrigerator instead of the tube shell ones.

提出了一种氨水吸收式制冷机紧凑化的方案,特别是采用螺旋板式换热器作为发生器和分凝器以降低发生精馏器高度的新设计,给出了采用上述改进方案所研制的乙醇蒸馏装置的实验结果。

This paper introduces industrial application of the new compound slant-hole tray with multiple downcomer in the refinery gas separation unit, The result shows that the methods for design of the new tray is reliable, and the new tray can be used widely among the fractionating tower, absorbing tower, desorber in petrochemical, chemical, pharmaceutical industries and so on.

介绍了新型多溢流复合斜孔塔板在炼厂气体分馏装置上的工业化应用,结果表明其设计方法是可靠的,可以广泛应用于石化、化工、医药等许多行业的精馏塔、吸收塔和解吸塔上,特别适用于液相负荷很大的体系。

N-methylacetamide was used as entrainer in separating acetic acid from water with extractive distillation ,and the interaction mechanism in this process was studied by using the density functional theory.

文献[1-4]认为萃取精馏分离乙酸水溶液过程中萃取剂与乙酸之间的氢键作用改变了溶液中乙酸和水的活度系数关系,从而改变了两者之间的相对挥发度,使得水和乙酸的分离变得相对容易。

With regard to the practical problems of estimating product quality on-line in hydrocracking fractionator, the soft-sensing engineering implementation strategy, which combines several soft sensors by weights for product quality estimating, is proposed to improve robustness of on-line estimation.

运用此控制策略对Shell公司重油常压塔和Wood-Berry精馏塔进行了仿真研究,通过与直接针对实际对象的基于RNNARX模型的多变量约束预测控制策略的仿真结果相比较,显示了PLS-MPC控制策略的有效性。

The mixture produced fromβ-pinene mainly containing geraniol and nerol,whose difference in boiling-point is only 2 C. They were separated by using the omethod of vacuum batch distillation and flash distillation with additives.

以β-蒎烯路线生产的香叶醇和橙花醇混合醇产品为原料,采用减压间歇精馏和闪蒸方法,通过添加络合剂提高产品的质量,实现了沸点差仅为 2℃的橙花醇和香叶醇的分离。

In this paper, a closed*.loop gain shaping algorithm for MIMO system is presented. It is applied to a high purity distillation column, good control effect and robust stability are obtained.

给出了MIMO系统的闭环增益成形算法,将之应用于精馏塔的控制中,取得了良好的控制效果和鲁棒稳定性。

In this paper, a closed*.loop gain shaping algorithm for MIMO system is presented. It is applied to a high purity distillation column, good control effect and robust stability are obtained.

摘 要:给出了MIMO系统的闭环增益成形算法,将之应用于精馏塔的控制中,取得了良好的控制效果和鲁棒稳定性。

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