精馏

In order to achieve a rapid and accurate selection for extractive distillation solvent, and to acquire 1,2,3-trimethylbenzene with high purity from solvent oil via extractive distillation, the UNIFAC model was used to calculate the relative volatility of 1,2,3-trimethylbenzene to indane (the mass ratio of 1,2,3-trimethylbenzene to indane is 4∶1) in five different solvents, acetophenone, di-2-octylhexyl phthalate, glycol, dimethyl sulfoxide,sulfolane at 17.47 kPa.

为了快速准确地选择萃取精馏溶剂，由190#溶剂油萃取精馏获取高纯度连三甲苯，运用UNIFAC模型，计算了质量比为4∶1的连三甲苯-茚满体系在苯乙酮、乙二醇、邻苯二甲酸二辛酯、二甲基亚砜和环丁砜5种溶剂中在17.47 kPa下的相对挥发度。

In this dissertation, a three-phase nonequilibrium model for packed column distillations is developed.

在三相共沸精馏过程建模仿真和优化计算中，由于两个液相可能同时出现，判断液相稳定性问题已成为了一个三相精馏过程计算的瓶颈问题，这也是本文的研究重点之一。

In order to solve the problems such as multiple components in products, long time of rectification, high energy consumption, low yield and purity of product occurring during the production of p - octyl phenol, the effects of reaction conditions including reaction temperature, reaction time, the molar ratio of phenol to diisobutene on the conversion and yield of the product were examined.

为解决对辛基酚生产过程中精馏时存在组分多、精馏时间长、能耗高、产品收率和纯度低等问题，用正交实验探讨反应温度、反应时间、苯酚与二异丁烯原料摩尔比3因素对原料转化率和产品对辛基酚收率的影响。

This paper introduced briefly developing trend of propylene rectification technology in gas separating unit and analyzed theoretically the middle reboiler used in propylene rectification column.

简述了气分装置丙烯精馏技术的发展趋势，对丙烯精馏塔增设中间重沸器进行了理论分析。

To solve the practical problem where the temperature field distribution is low at the lower part of furnace chamber and high at the upper part and the temperature difference is untolerable , which is reflected by the thermocouples at site, the authors take the methods of multipoint test and computer hologram simulation to research into the fields in the furnace chamber of the zinc fractionating tower at Shaoguan Smelter CNNC.

针对锌精馏炉炉膛各检测点反映出的其上部温度偏高，下部温度偏低，上下温度偏差过大的实际问题，采用现场多点温度测试，结合炉膛内流场、浓度场、释热场和温度场数值仿真的方法对韶关冶炼厂二精馏系统进行研究；利用仿真结果中的流场扣浓度场数据，统计出实测中无法得到的各次空气和煤气在南1号至南4号各喷口的流量。

The paper proposed a new method by compartmentalizing the whole start-up process into several parts based on control task. Then, the paper proposed a method by using timed Petri net to model the start-up process.

在此基础上，基于控制任务对精馏塔开车过程进行划分，并使用赋时Petri网对划分后的精馏塔开车过程建模，并进行仿真分析。

In this paper, on the base of powerful calculation and diagramming ability of MATLAB, the typical examples in distillation are analyzed and the corresponding ideas and methods of computer-aided calculation in distillation are given.

本文利用MATLAB语言强大的运算与图形表达功能，通过剖析精馏计算过程中的典型例题，给出了计算机辅助计算精馏过程的具体思路和方法。

In the present dissertation, the principles and application of the reaction rectification techology in the syntheses of benzyl chloride, chloroacetic acid, monochloroacetone were approached.

本论文采用反应精馏技术氯化苄的合成、氯乙酸的合成进行了认真的研究，并且对一氯丙酮、氯苄系列产品进行了反应精馏研究，都得到了理想的结果。

Currently the batch process of chlorination and rectification is mainly applied in the production of benzyl chloride. A few continuous processes of chlorination and still rectification have been found.

工业上氯化苄生产大多采用歇釜式氯化、间歇精馏的方式，少数采用连续釜式氯化、连续精馏的方式。

Based on these, an improving μ-synthesis is presented, with which the high-purity distillation is designed well. 2. The robust performance problem of MIMO plant is explained with the plant direction angle, which shows that the robust performance varies with different input uncertainties and the μ-synthesis should be applied correctly according to the uncertainty structure. 3. Condition number and bandwidth are the important items for robust performance design in MIMO system. The H〓 two-block problems can not deal with the robust performance design of MIMO system because of the condition number cancellation. A general μ-synthesis procedure for MIMO system with uncertainties is presented. 4. For the SISO system, the object function in robust performance is amplified by at most 〓 than that of H〓 two-block problems in value: So the robust performance of SISO system can be done with the H〓 two-block problems to avoid the complicated μ-synthesis procedure. 5. All the conclusions and methods presented in this paper are demonstrated by some typical design examples.

从而形成一种改进的μ综合方去，并对精馏塔病态对象进行了鲁棒性能设计，得到令人满意的结果；（2）利用对象的方向角解释了MIMO对象鲁棒性能设计出现问题的原因，并提出不同输入摄动形式下系统的鲁棒性能问题也并不相同，因此利用μ综合处理鲁棒性能设计时，应根据不同的摄动情况采用不同的结构进行设计：（3）条件数问题和带宽问题是MIMO系统鲁棒性能设计的两个主要问题，指出由于条件数对消的存在使得一般H〓两块问题无法处理MIMO系统的鲁棒性能设计，而μ综合方法则是处理MIMO系统鲁棒性能设计的有效方法，并给出了其处理MIMO系统鲁棒性能设计的一般性方法；（4）提出对于SISO系统H〓两块问题（S/T问题、S/KS问题）的设计指标函数与鲁棒性能设计的μ指标函数在数值上最大差〓倍，因此对于一般SISO系统的鲁棒性能设计可以简单地用一般的H〓的两块问题处理，而避免μ综合设计的复杂过程；（5）本文中提出的结论和算法都利用H〓/μ发展中的典型例子：Doyle-Stein问题，Safonov的战斗机模型，精馏塔对象等进行了设计验证。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。