粒剂

The conclusions were as follows: theνO-H andνC=O IR absorption maxima shifted towards higher wave numbers after imprinting 17β-estradiol on TFMAA-co-TRIM copolymer with the red shift of theνO-H groups being apparent after precipitation polymerization for 16h while that forνC=O groups being observed after polymerization for 24h. A strong interaction between TFMAA and 17β-estradiol was confirmed by the high selectivity for 17β-estradiol, as indicted by the values of the separation factor of isomers of 17β-estradiol/17α-estradiol (2.28) and the imprinted factor (3.01). Particle diameter of TFMAA-co-TRIM polymer was between 300 nm and 1.5μm, which suited well for solid phase sorbent throughout at low column pressure. The recognition of imprinting TFMAA-co-TRIM polymer for sterol molecules was driven by enthalpy eluted with acetronitile, and low temperature was in favor of the separation of sterol structure analogues on imprinting column. TFMAA-co-TRIM polymer possessed of determinate anti-heat stability, with melting point beginning at 255.84℃, Tp=257.40℃, control TFMAA-co-TRIM polymer and imprinting TFMAA-co-TRIM polymer were respectively decompounded at 267.79℃and 343.11℃, and solid micro-extraction noddle prepared by the special polymerization also showed definite recognition for 17β-estradiol by GC/MS detecting at 270℃. By selection of various washing and elution solvents, elution reagents of close polymerization system were of more advantage in template molecules retention and recognition on molecularly imprinted solid phase extraction column. At a certain extent, progesterone, 17α-estradiol, 17β-estradiol and 4-androstene-3, 17-dione could be intercepted on the MISPE column. Especially, MISPE had high selectivity for progesterone, and imprinting TFMAA-co-TRIM polymer could achieve adsorption balance within 50 min by absorption kinetics test for 17β-estradiol. However, MISPE column showed better selectivity and enrichment property for 17β-estradiol than C18 and CSPE columns according to the data from HPLC and GC/MS analyses. Recovery of 17β-estradiol on MISPE column was up to 85.5% while when prime extracting solution of milk powder was sampled, the recovery of CSPE and C18 columns were 43.7% and 30.7%, respectively.

通过研究阐明：紫外聚合产物TFMAA-co-TRIM中的νO-H振动吸收峰在聚合16h后红移，νC=O振动吸收峰在聚合24h后红移；TFMAA-co-TRIM对雌二醇异构体的印迹因子达到了3.01，α为2.28，优于其它功能单体参与得到的聚合物识别特性；TFMAA-co-TRIM聚合物粒径介于300 nm至1.5μm之间，作为色谱固定相具有良好的通量和低的柱压；在乙腈流动相中，TFMAA-co-TRIM分子印迹固定相的分离过程主要被焓驱动，低温有利于分子印迹固定相分离甾醇结构类似物；TFMAA-co-TRIM分子印迹聚合物在255.84℃时开始熔融，Tp=257.40℃，聚合物CP的降解温度在267.79℃，MIP降解温度在343.11℃，制备的固相微萃取头初步经GC/MS 270℃的耐热性测定；不同的洗提溶剂筛选证明了选择接近聚合溶剂的洗脱体系更有利于MISPE发挥识别效应；分子印迹固相萃取柱对孕酮、17α-雌二醇、17β-雌二醇和雄烯二酮都具有不同程度的保留特性，可作为此类化合物的吸附材料，特别对孕酮强保留的富集特性，可作为孕酮的选择性识别吸附剂，其分子印迹聚合物对17β-雌二醇的吸附动力学测定显示在50 min内基本达到吸附平衡，具有作为传感器核心敏感材料的潜力；对比萃取奶粉中17β-雌二醇性能，MISPE柱比非分子印迹固相萃取柱和C18柱具有更高的保留，回收率依次为85.5%，43.7%和30.7%。

Preparation of the prescription of gu yan was divided into drug granule and capsule by the primary study of preparation. Nux vomica was made into capsule according to 0.33g per granulation and the other was made into drug granule according to 15g per bag.

制剂研究初步确定"骨炎方"的制剂分为颗粒剂与胶囊剂两部分，将"骨炎方"中马钱子制成胶囊、余药按一定工艺制成颗粒剂，颗粒剂15克/袋，胶囊0.33克/粒。

The importance of studying shrinking of polystyrene pattern for evaporative pattern casting is pointed out in this paper.After studying effects of technological factorsexpandable polystyrene(EPSbead diameter,pre-expansion time,age time of pre-expansion bead,molding steam pressure,storage time and temperature of pattern on shrinking of pattern,it is shown that the stress relaxation of pattern and the escape of pentane and water in pattern are main cause of pattern shrinking.

指出了对消失模铸造用聚苯乙烯模样收缩展开研究的必要性，研究了可发性聚苯乙烯珠粒粒径、预发泡时间、预发泡珠粒熟化时间、成形蒸汽压力及模样的放置时间、贮存温度对模样收缩的影响，认为模样中发泡剂和水分的挥发以及应力的释放是引起模样收缩的主要原因，最后提出了在实际生产中为减少模样收缩应采取的措施。

The grinding characteristics of coal tar pitch were analyzed by contrast of particle size distribution under different effects of grinding agents, and the grinding process parameters for CTPWS preparation have been determined.

通过煤沥青在不同助磨剂条件下的粒级分布率比较，分析了煤沥青的研磨特性，确定了煤沥青水浆制备的磨矿工艺参数。

The result shows that when the emulsifying agent layer not perfectly covering the primary particles' surface or the primary particles' surface being covered with overmuch powder grain, it will lead to the higher plastisol viscosity.

结果表明初级粒子表面的乳化剂层包覆不严或表层粉粒太多，均会导致增塑糊粘度偏高；次级粒子聚结松散，结构脆弱，有较低的糊粘度和触变性；次级粒子聚结紧密，有熔结现象，增塑糊粘度偏高。

The results show that spherical BaHfO3Ce nano-powders are synthesized only at 900 ℃ for 2 h and the average diameter is about 15 nm with ammonia as precipitant.

结果表明：以氨水做沉淀剂在900 ℃煅烧2 h合成的BaHfO3Ce粉体形貌近似球形，平均粒径约15 nm。

Discussed PVP and precipitant to reach the influence that distributing to diameter of small globose appearance, bead.

探索了PVP及沉淀剂对微球形貌、粒径及分布的影响。

This paper studies the relationship of infrared extinction effect of pyrotechnic agent with material granularities on the base of infrared extinction mechanism of smoke.

本文在深入理解烟幕微粒红外消光机理的基础上，研究了粒径因素与发烟剂遮蔽红外辐射性能的关系。

Human bladder cancer cell line T24 was used, two different NF-kB inhibitors, pyrrolidine dithiocarbamate and dominant negative IkBα were used.

在人膀胱癌细胞系T24中，使用两个核转录因子kB抑制剂即显性失活IkBα质粒和二硫氨甲酸脂吡咯烷。

The aim of this study was to determine the relationship between NAFLD and low concentration of mitochondrial inhibitor, rotenone.

本次实验目的主要在了解低剂量粒线体抑制剂对於非酒精性脂肪肝疾病形成之影响。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。