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The structure and morphology of CNTs which have been purified and not yet, were characterized by TEM, SEM, XRD, Raman, TG-DTA, BET, IR. The results indicated that when the stokehole reaction temperature was 1170℃,the decompose temperature of Ferrocene was 150℃,he volatilize temperature of Benzene was 50 ℃, hydric flow rate was 270ml/min, the concentration of thiophene was 1% and the reaction time was 20 minutes, the CNTs with single-walled and multi-walled were prepared. The diameters of the single-walled CNTs are in the range of 0.08~1.15nm, and that of the multi-walled CNTs are in the range of 40~120nm.

结果表明:炉膛反应温度1170℃、二茂铁的分解温度150℃、苯的挥发温度50℃、氢气的流量270ml/min、吩体积分数1.00/100ml苯、反应时间20min时,可以得到碳纳米,既有单壁又有多壁,单壁的内径分布在0.881.15nm之间,多壁的直径分布在40120nm之间;纯化后的碳纳米比表面积增加,壁光滑,而且产生了大量的含氧官能团,有利于在水溶液中的分散。

Feed the gross pipe from front plant, cog down the upper roller to given size to rotating bring the pipe into rolling zone for reducing diameter and wall form rolling; after rolling from head to tail, turn 90Deg with the gross pipe, top bar and core head by tilter for next rolling travel that inverse roll to head to bring the pipe back to front plant; then, turn again for next periodical to-an-fro rolling till design size request.

将毛自轧机前台喂入,将上轧辊压下至设定的尺寸,毛在轧辊的旋转带动下曳入轧制区域,进行减径和减壁变形轧制;毛从头部轧制到尾部后,将毛、顶杆及芯头在翻转装置的作用下翻转90°,进行下一个轧制行程,反向轧制到头部,毛回到轧机前台;再将毛、顶杆及芯头在翻转装置的作用下翻转90°,进行下一个轧制周期往复轧制,轧制到毛成达到设计尺寸要求。

This paper traces the history of America's drug regulatory regime change from the perspective of institutional change. It argues that this centurial history can be divided into three regimes: ex-post regulatory regime, ex-ante regulatory regime and process regulatory regime.

本文从制度变迁史的角度,对美国联邦政府药品规体制的百年变迁历史进行了梳理,并结合风险规本身的特征,将其划分为事后型规、事前型规和全过程规三个阶段,力图展现出现代风险社会中规型国家起源和发展的基本轨迹,反映出国家对商业社会、工业社会和信息社会三种不同社会形态下社会风险的规模式。

Theurinary IL-6 level positively correlated with density of glomerular matrix membrane, global sclerosis, fiber or fibrocellular crescents and interstitial fibrosis (p. 05). According to the degree of density of glomerular matrix membrane and interstitial fibrosis, urinary Col-IV level had better correlation than urinary TGF-betal and IL-6 levels.In IgAN, Col-IV showed increased expression in diseased renal tissue whereas the site of expression of TGF-betal was mainly localized within the cytoplasm of tubular epithelial cells. Interstial expressionwas also present but glomerular TGF-betal expression was found only in patients with heavy mesangial proliferation. There was a significant correlation between glomerular positivity for Col-IV and severity of histological damage. There was also a significant correlation between positivity for TGF-betal and Col-IV in the tubular epithelial and interstitial lesions. In contrast, there was no ralationship between glomerular positivity for TGF-betal and severity of histological damage.The urinary TGF-betal level paralleled tubular TGF-betal expression.

结果 ①IgAN患者尿TGF-β1、IL-6、Col-Ⅳ水平较健康人明显增高(P<0.01),该变化与血中的浓度无关(P>0.05);②尿TGF-β1水平与小间质TGF-β1阳性表达呈正相关(P=0.000),而与小球TGF-β1阳性表达无关(P>0.05),尿Col-Ⅳ水平与小球和小间质Col-Ⅳ阳性表达均呈良好的相关性(P<0.01),还与小间质TGF-β1阳性表达呈正相关(P<0.05):③小球Col-Ⅳ阳性表达与肾组织慢性病变密切相关(P<0.05),小间质Col-Ⅳ和TGF-β1阳性表达均与肾小间质病变呈良好的相关性(P<0.01),而小球TGF-β1阳性表达与肾组织损伤无关(P>0.05);④尿TGF-β1、Col-Ⅳ水平与肾小球基质基底膜面密度、小间质病变呈正相关(P<0.01),与小球内细胞数呈负相关(P<0.05),该结果与其在组织中的表达一致;尿IL-6水平浙江大学硕士学位论文尿TGF一B一、IL一6和Col一IV在IgA肾病中的应用价值与基质基底膜面密度、球性硬化、纤维或细胞纤维新月体所占肾小球百分数及小间质病变均有显著的相关性(F.05);在轻度肾病理损伤时,尿'l'G卜pl、I卜6、Col一IV水平即升高,而尿Col一W在反映细胞外基质积聚和间质纤维化程度上比尿TGF一pl和IL一6有更好的相关性。

A group: to measure the length of root canal by Root ZX, prepare the root canal and test the trial point for a best position of the major Gutta Percha Point in root canal obturation with lateral compaction, then take X-ray photos.

随机选择需行根治疗术的单根恒前牙、双尖牙 2 30颗,分为A、B两组,A组采用RootZX 根测量仪测量根长度,根预备后,根充填时加试尖步骤,调试出最适主尖后侧压充填根,摄牙片

The main products with the brand "LUTONG" include the PE pressure pipeline system (PE gas, water supply pipes and pipe fittings), PE tele communication pipeline system (PE silicon-core pipe, PE corrugated pipe, PE porose pipe, PE optical fiber pipe with silicon-core), PE electric cable pipeline system and PE water discharge pipeline system (PE large diameter corrugated pipe).

沧州明珠塑料股份有限公司是由河北东塑集团股份有限公司和钜鸿有限公司共同出资设立的中外合资股份制企业。2007年1月24日&沧州明珠&(股票代码:002108)在深圳证券交易所挂牌上市,公司现注册资本6875万元,占地1000余亩,主导产品为&陆通&牌塑料压力道系统(PE燃气、给水材、件)、通讯道系统(HDPE硅芯、波纹、梅花、格栅、子、硅芯光纤微)、排水道系统。

CNTs were first pre-treated using acid solution (HNO3) to obtain CNTs functionalized with carboxylic groups. Subsequently, the stearyl alcohol was grafted onto CNT with the assistance of dehydrating agent, N,N'-dicyclohexyl-carbodiimide. Excellent dispersion in organic solvents such as acetone, THF, and chloroform was found for the modified CNTs (CNT-C18). In addition, the PBS/CNTs nanocomposites were then prepared through simple melt-blending. Mechanical properties, thermal behavior, conductivity of resultant polymer/CNT composites were investigated. The results show that excellent dispersion of nanotubes in the PBS matrices was achieved.

为了增加多壁奈米碳在复合材料中的分散性,将碳表面进行化学修饰,首先将多壁奈米碳浸入HNO3溶液中,进行酸化,使碳表面带有羧酸的官能基,然后再加入十八烷醇,在温和的条件下,藉由N,N'-二环己基碳二亚胺(N,N'-dicyclohexyl- carbodiimide,DCC)脱水剂脱水,使碳和十八烷醇之间产生酯基的化学键结,改质后的碳可以分散在acetone、THF、chloroform…等有机溶剂中,结果显示成功的利用DCC脱水剂完成碳的改质。

Methods insert the stomach tube nasal cavity, with the help of intubating ferceps, take the stomach tube out of mouth cavity from the posterior wall of dysphagia, insert trachea catheter (cid 7.0~7.5) to esophagus, under the help of trachea catheter, insert the stomach tube to esophagus then take the trachea catheter out of the esophagus and vertical, cutting off, in the course of into esophagus.

经鼻腔插入胃,用插钳将胃从咽后壁前取出口腔外,用id 7.0~7.5的气插入食,在气诱导下将胃经气插入食,然后将胃向食内送进,同时将气退出,将胃置入相当合适的深度后,固定胃

The old technology and equipment in the curve of columnar ,plane and cambered coiled pipes for circular pipe-coiled pipes and half pipe-coiled pipes were very complicated.

原有的圆和半中的柱面螺旋盘、平面盘和曲面盘的结构繁杂、弯制质量差以及弯制工艺工装造价昂贵。

Results: in contrast with model group, SSM can (1) increase the survival rate of ARF in rats, cut down Scr and BUN at 24hr, improve renal function, slightly surpass Vp in its therapeutic effect;(2) mitigate the extent of renal pathologicchanges, decrease the numbers of renal tubule necroses and casts;(3) protect renal ultrastructure such as microvilli, mitochondria, endoplasmic reticulum of TEC, podocytic process of glomerulus epithelial cell,endothelial cell etc, better than Vp;(4) enhance SOD activity, lower MDA contents in renal cortex;(5) enhance NO contents in serum, reduce ET levels in plasma;(6) evidently cut down TNF- a contents in serum, superior to Vp;(7) antagonize calcium overload in TEC;(8) alleviate renal pathological changes in ARF metaphase (at 3d), advance regeneration and recovery of TEC, restore renal structure in ARF convalescence (at 5d), and better than Vp;(9) increase the expression of TEC PCNA and prepro EGFmRNA in ARF metaphase.

结果:与模型组相比,SSM能(1)提高ARF大鼠的存活率,降低24hr时Scr及BUN,改善肾功能,其疗效略优于维拉帕米;(2)减轻ARF肾脏病变程度,减少24hr肾小坏死数及腔内型数;(3)对肾脏的超微结构如肾小上皮细胞微绒毛、线粒体、内质网、肾小球上皮细胞足突、内皮细胞等形态结构均有一定的保护作用,其疗效略优于维拉帕米;(4)提高肾皮质SOD活性,降低MDA含量;(5)提高血清NO水平,同时降低血浆ET含量;(6)显著降低血清TNF-α的水平,疗效明显优于维拉帕米;(7)拮抗小上皮细胞[Ca~(2+)]_i的升高;(8)使ARF中期(第3d时)肾组织病变较同期其它两组明显减轻,并使肾小细胞再生修复提前,至ARF恢复期(第5d时)肾组织结构恢复重建良好;作用明显优于维拉帕米;(9)促进ARF中期肾小上皮细胞PCNA的表达及EGF前体mRNA的合成,从而增加EGF的合成释放,而维拉帕米无此作用。

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