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The interaction of tributyltin, the main components of antifouling paint of ships, and its degradation products of monobutyltin and dibutyltin with human serum albumin was investigated by ultraviolet, fluorescence and circle dichromism spectra. The influences of the concentration, acidity, organic solvent such as ethanol and ionic strength on the interaction of butyltin compounds and HSA molecule were examined to find that the interaction of butyltin compounds and HSA was dual.

通过紫外、荧光和CD光谱,研究了船体防污漆中主要防污成分——三丁基锡化合物及其降解产物——一丁基锡和二丁基锡与人血清白蛋白相互作用的方式与程度,考察了浓度、酸度、有机溶剂和离子强度等因素对相互作用的影响。

The polymerization reacts from the inverse emulsion . Selecting white oil as continuous medium , Span60 and TX-10 as the complex emulsifier , AM-01﹑(NH4)2S2O4 and NaHSO3 as new-type complex initiator , the copolymerization of dimethylamino ethyl acrylate methyl chloride/acrylamide was developed . The effects of the concentration of monomer﹑emulsifier and initiator﹑ temperature﹑reaction time and pH on the molecular weight﹑intrinsic viscostity﹑conversion ratio and cation degree of copolymer were studied .

以反相乳液为初始聚合体系,油酸失水山梨醇酯Span60和辛基酚聚氧乙烯醚TX-10构成复配乳化剂,白油为连续介质,AM-01、过硫酸铵和亚硫酸氢钠组成新型复合引发体系,进行丙烯酰胺/(2-甲基丙烯酰氧乙基)三甲基氯化铵的反相准微乳液共聚合,研究了单体浓度、乳化剂、反应温度、反应时间、pH等因素对聚合产品分子量、特性粘数、转化率及阳离子度的影响。

The concentrations of Mg^2+, dNTPs, Taq DNA olymerase, primers which affect the SRAP-PCR reactions were optimized in order to establish the SRAP molecular marker system in Diospyros spp.

为了建立柿属植物SRAP技术体系,对影响SRAP-PCR的Mg^2+、dNTPs、Taq聚合酶、引物浓度等因素进行了优化。

In this article, we have been investigated that synthesizing and properties of shape memory polyurethane. The shape memory polyurethane was synthesized from PCL diol, MDI(4, 4'-diphenylmethane diisocyanate) and BDO (1,4-butanediol) in this experiment. We analyzed that the effect of differential mole ratio of monomers to synthesized SMPU. Besides, the various concentrations of Nano-silver were mixed with SMPU. Mechanical properties and shape memory behavior of SMPU nanocomposite films were investigated.

本研究目的为藉由改变4,4'-二苯甲基二异氰酸盐(4,4'-diphenylmethane diisocyanate, MDI)/聚己内酯二元醇(polycaprolactone diol, PCL diol)/1,4-丁二醇(1,4-butanediol, BDO)等不同莫耳比制备形状记忆型聚氨基甲酸酯(Shape Memory Polyurethane, SMPU);并探讨改变不同单体莫耳比及添加不同浓度奈米银溶液对其物性及形状记忆性的影响。

The dominative factors of PAC dose include temperature, pH, SS and turbidity.

混凝剂投加量的主要控制因素有原水水温、pH值、SS浓度和浊度等。

The antifungal activities of these materials were investigated and build foundation to develop low poison plant antifungal products. In experiment, polyphenols were extracted by reflux ectraction method which applyed petroleum ether to degrease and methyl alcohol solvent. Phenolic hydroxyl were examined and inspected by colour-developing reaction and the content of total polyphenols was determined by UV-spectrophotometry. Screening test were performed to the antifungal activities of polyphenol extraction by the tube dilution method to the selected ten pathogenic fungus such as Dothiorella gregaria, Rhizoctonia solani, Phyllosticta pirina, and the minimal inhibitory concentration were measured. The column chromatography and thin layer chromatography were applyed to separate and analyse cortex extracts of Dracaena cochinchinensi Lour.

实验部分采用以石油醚脱脂,甲醇为溶剂的回流提取法来提取植物多酚,用显色反应检识酚羟基;采用紫外分光光度法对多酚粗体物进行总多酚含量的测定;选取了聚生小穴壳菌、立枯丝核菌、梨叶点霉等10株常见农林业致病真菌,采用试管液基稀释法对多酚粗提取物进行了抗真菌活性筛选试验,并测定其最低抑菌浓度;采用柱层析法和薄层层析法对其中抑菌效果较好的龙血竭进行分离分析,根据其中3种化合物的光谱数据UV、IR、~(13C-NMR、1H-NMR和MS鉴定其结构。

The fluctuations of the EC abundance correlate well with that of δ〓O in GRIP ice core, indicating the existence of some short-term climate change events, such as Younger Dryas, Heinrich events and Bond's cycles.

渭南黄土剖面的元素碳浓度曲线的总体波动形式与格陵兰GRIP冰芯氧同位素记录曲线有相似性,并对短尺度的气候事件如:新仙女木事件、哈因里奇事件(H1-H6)、Bond旋回等有较好的反映。

This cognition is coincident with the resu1ts of organic carbon, pollen and phyto1ith. The f1uctuations of the EC abundance correlate we1l with that of 5 ls0 in GRIP ice core, indicating the existence of some short--term climate change events, such as Younger Dryas, Heinrich events and Bond's cycles.

渭南黄土剖面的元素碳浓度曲线的总体波动形式与格陵兰GRIP冰芯氧同位素记录曲线有相似性,并对短尺度的气候事件如:新仙女本事件、哈团里奇事件(H1-H6)、Bond旋回等有较好的反映。

In this paper, synthetic process of PTT and cationic dyeable PTT was studied, including molar ratio, catalyst concentration, reaction time and temperature, types of antioxidants in the esterification reaction and the condensation reaction.

研究了聚对苯二甲酸丙二醇酯、阳离子染料可染PTT的合成工艺条件中各因素对酯化及缩聚反应的影响,包括单体物质的量比、催化剂浓度、反应时间和温度、抗氧剂种类等。

Polyunsaturated fatty acid of Elsholtzia rugulosa seed oil were enriched by urea inclusion method.

应用尿素包合技术对野香籽油中不饱和脂肪酸进行了富集,通过正交实验(L934)考察了尿素在乙醇中质量浓度、脂肪酸与的质量比、时间及温度等因素对不饱和脂肪酸提取率的影响。

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