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It was shown that the improvement of electric properties in 1%Eu-PZT can be attributed to Eu donor doping, which decreases the concentration of defects such as oxygen vacancies and holes, while the degradation in fatigue and leakage current properties shown in the films with more than 1mol% Eu dopant results from the apparently dominant acceptor doping, which increases the concentration of oxygen vacancies and holes.

结果表明,1mol%Eu施主掺杂,可以减少氧空位以及空穴等缺陷浓度,因此1%Eu-PZT薄膜的极化疲劳和漏电流特性得到明显改善;高于1mol%Eu的受主掺杂作用使薄膜中氧空位以及空穴等缺陷浓度增加,导致PZT薄膜电学性能恶化。

The effect of initial pH, temperature and N263 concentratio n on extraction of fucoidan was investigated. It has shown that temperature and initial pH of the solutions have no great influences on the extraction of fucoid an, and when N263 concentration is low, an increase in the concentration incre ases the extraction of fucoidan.

对影响萃取褐藻糖胶的水溶液初始pH、温度及N263浓度等因素研究结果表明,N263浓度是影响褐藻糖胶萃取的主要因素,而初始pH、温度等的影响不大。

The water activities and osmotic coefficients have been determined at 25 ℃, over the range of concentrations from diluted up to saturated with respect to the solute of NaCl for the synthetic salt lake brine Li Na K Mg Cl SO 4 H 2O systems by isopiestic method using an improved apparatus.

根据我国青海一里坪和东台吉乃尔盐湖晶间卤水Li Na K Mg Cl SO4 H2 O体系的组成制备了两种合成卤水储备溶液,采用等压法和改进的实验装置在 2 5℃下,从稀释到溶液中溶质NaCl达到饱和的浓度范围,对合成卤水溶液进行了等压测定,确定了它们的水活度aH2 O,和渗透系数φ;比较了两种卤水的热力学性质及其变化的规律,揭示了其天然卤水浓度差异的物理化学成因。

The effects of grafting conditions such as temperature,reaction time ,Mohr's salt concentration,and total concentration of monomer on grafting yield were studied.

讨论了辐照剂量、储藏时间、反应温度、Mohr's盐浓度及单体浓度等因素对接枝率的影响(所有的实验,辐照及接枝聚合等都是在有氧的条件下进行的)。

We designed a novel system of Alginate/(NaCS+CaCl2) for preparation of intra-hollow Ca-alginate capsule and studied the effects of operation conditions gelation time,dropping velocity and(concentrations of CaCl2,NaCS or sodium alginate) on the diameter,membrane thickness and compression intensity of ...

重点探讨了反应时间、滴加速度、海藻酸钠溶液浓度、NaCS和CaCl2溶液浓度等参数对制得胶囊的直径、膜厚和机械强度等性质的影响。并确定了中空海藻酸钙胶囊的制备条件:1%的海藻酸钠溶液,10%的CaCl2溶液,2%的NaCS溶液,180滴/min的滴加速度和10 min的凝胶反应时间。

Methods We adopted four methods that single cpidural block anesthesia or narcotics analgesies were injected into subarachnoid space and epidural space or single narcotics was injected into subarachnoid space (group C fentanly 25μg;group D fentanly 20μg) to study analgesia birth for 130 nullipara women. The analgesia efficacy, side effect, birth time md mode,postpartum haemorrhage and the condition of the fetus and the newborn were compared.

采用单纯硬膜外腔阻滞、蛛网膜下腔-硬膜外腔联合给予低浓度麻醉药及镇痛药、单纯蛛网膜下腔给予低浓度镇痛药(C组芬太尼25μg,D组芬太尼20μg)等四种不同的方法对130例初产妇进行分娩镇痛,比较几组的镇痛效果、不良反应及对产程、分娩方式、产后出血、胎儿及新生儿等的影响,并与40例正常未干预组产妇比较。

The Zetasizer Nano ZS is made in Marvern in England. It is the newest Zetasizer Nano ZS with the newest technology. Malvern Zetasizer Nano ZS90 is for the measurement of size, zeta potential of dispersed particles and the molecular weight of random coiled polymers. If it connect with the Autotitrator, it can measure zeta potential as a function of pH, conductivity or concentration of an additive, provides much greater insight into the processes involved in stabilizing or flocculating disperse systems.

英国马尔文公司生产的Zetasizer Nano ZS型纳米粒度仪是目前世界上技术最先进的纳米粒度仪之一,该仪器可以测定纳米材料的粒度分布、ZETA电位值,并可以进行蛋白质的熔点测定,及蛋白质等大分子和聚合物材料的分子量测试,如果与自动滴定仪相连接后,可自动测定粒度或Zeta电位随pH值、盐浓度或添加剂浓度等的变化趋势。

In the paper, some factors influencing the effect of reduction including the anodic material, the cathodal material, the area ratio of cathode to anode and the kind of electrolyte have been investigated and screened out. The result showed that under the same reduction conditions, the reduction of Cr6+ has better effect to use lead-antimony alloy as anode, iron plate as cathode, which area ratio is 7:1 and potassium sulphate as electrolyte.

本文首先对影响电解还原效果的阳极材料、阴极材料、阴阳极面积比和支持电解质加入的种类等因素进行了研究筛选,结果表明:在同样电解还原条件下,实验中阳极采用铅-锑合金,阴极采用铁板,阴阳极面积比取7∶1,支持电解质取为硫酸钾时,具有较好的Cr~(6+)还原效果;同时在采用铅-锑合金作阳极的条件下,通过正交实验,对影响直接在碱性介质中电解还原低浓度含铬废水的其他因素进行了研究,即研究了在电化学还原过程中,Cr~(6+)的初始浓度、极板间距、支持电解质的加入量、搅拌情况等因素对还原效果的影响程度,确定出了主要的影响因素。

The related reaction conditions and factors such as catalysis of some catalysts etc were discussed. In the procedures, 2-pentylidene cyclopentanone intermediate, which could be isomerizated into a 2-pentyl cyclopentenone under acidic conditions, was effectively prepared in the presence of a phase transfer promotor.

讨论了正戊醛和环戊酮在碱性条件下缩合生成2-亚戊基环戊酮的反应温度、碱浓度、相转移催化剂等因素对反应的影响。2-亚戊基环戊酮中间体化合物能在酸催化剂作用下,异构成2-戊基环戊烯酮,其中酸浓度和溶剂等参数对反应影响明显。

MIPC was photocatalytically transformed to 3,4-dihydroxyl hypnone, 2-iso-butyl phenol and acetic acid, and mineralized ultimately in oxygenated TiO2 slurries. The photocatalytic degradation processed according to first order kinetics with the apparent rate constant depending on initial concentration, light intensity and the amount of catalyst. The amount of catalyst had an optimum value (0.5g/L). The apparent rate was inversely proportional to square root of the initial concentration approximately.

MIPC能被光催化转化成3,4-二羟基苯乙酮、2-异丁基苯酚和乙酸等产物并最终被矿化,MIPC的光催化反应过程符合一级动力学规律,其表观速率常数与MIPC的起始浓度、TiO2量和光强等因素有关,MIPC降解的反应速率与入射光强成正比,与MIPC初始浓度的平方根成反比。

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