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The results show that magnesium and aluminum theoretically can be thoroughly dissolved from the blast furnace slag by diluted sulfuric acid pretreatment on the blast furnace slag even if the ended concentration of sulfuric acid is 0.001mol/L, while the titanium basically could not be dissolved. Therefore it is theoretically indicated that the separation of the magnesium and aluminum from the slag with the least titanium loss by diluted sulfuric acid pretreatment is possible.

结果表明,采用稀硫酸对高炉渣进行预处理,当终酸浓度即使为0.001mol·l~(-1)时,镁、铝理论上也能全部被酸浸出,而钛在0.001 mol·l~(-1)的酸浓度条件下基本不被浸出,从而从理论上可以说明对高炉渣采用稀酸预处理可以很好的将炉渣中的镁、铝等杂质分离出来,而钛极少被浸出。

The factors which mostly affect the quality and output of the product including molar proportion of reagents, reaction temperature, alkaline concentration and reaction time are analyzed. After orthogonal experiment, it is concluded that the optimized reaction condition is that acetone and furfural are charged with equal molar quantities at 40 with sodium hydroxide (0.10 mol/L) and the operation time 5 h.

通过对影响亚糠基丙酮质量和收率的主要因素原料配比、反应温度、碱浓度、反应时间等单因素实验,探索出合成亚糠基丙酮的优化反应条件为:原料配比n:n=1.0:1.0、反应温度40℃、氢氧化钠溶液浓度为0.01 mol/L、反应时间5h。

The influences of the kinds and concentration of buffer and organic modifier, the pH value of buffer, column length and column temperature on the separation were examined.

考察了缓冲溶液的种类、浓度和pH值,有机改性剂的种类和浓度,柱长和柱温等对手性分离的影响。

The cold-flow field in the gasifier chamber is studied.

本文对水煤浆气化炉喷嘴进行了简化处理,在此基础上,对气化室内的冷态流动过程进行了研究,发现:整个气化室都处于流动的回流区长度范围以内;水煤浆气化炉中,由于操作压力很高,气相密度很大,所以即使对于d〓=150μm的较大煤颗粒,其对流体的跟随特性也很好,没有发生流动特性突跃的现象;两相的最大回流速度、回流强度,颗粒相的浓度分布,以及气化室内的静压力损失等,均与气化炉的负荷、水煤浆浓度、煤粒直径、O〓在喷嘴两个流道中的分配比例。

The examination made known, when consistence of acetic acid glacial at the 2%, dairy salt concentration 8%~12%, the best way was to be elected.

研究了采用冰乙酸和食盐的混合液作为汤汁的香菇酸盐渍生产工艺、产品检验等,研究表明,冰乙酸浓度2%、食盐浓度8%~12%是香菇酸盐渍的最佳生产工艺条件。

Methods The DNA chip was fabricated,on which oligonucleotide bougies′length was 19 base pairs,and the concentration was above 15 μmog/L.

方法自制DNA芯片,每条寡核苷酸探针片段长度为19bp,点样浓度在15μmol/L,以痰液为待检标本,分别用不同引物、Mg2+、核苷酸、DNA聚合酶浓度等进行多重聚合酶链反应;分别在不同时间、温度下进行杂交,分别在不同酶作用时间和显色时间进行分析,比较不同条件芯片检测结果。

The study of plating process showed the influences of bath components, such as complexing agent and reducing agent, and operation conditions, such as pH value and temperature, on deposition rate.

对镁合金化学镀镍工艺的研究表明,镀液组成如配体浓度、还原剂浓度和操作条件如pH值、温度等影响镀液的沉积速度。

Based on this, four DBP concentrations(0.38, 0.85, 1.90, 4.25mg·L-1)were confected using the same distance of logarithmic distance, and 20 days' sub-acute toxicity test was carried out. The weights of the liver and gill of B. rerio were measured every 5 days.

在此基础上,等对数浓度差设置4个质量浓度0.38、0.85、1.90、4.25mg·L-1进行20d慢性染毒,期间每5d测定斑马鱼的体重、肝重和鳃重,同时测定斑马鱼肝脏、鳃中SOD酶和ATPase活性。

The test results of acute toxicity were examined with Pearson's degree of fitting. The results indicated that the silkworm was extremely sensitive to Chlorantraniliprole. The median lethal concentration (LC50) was 4.0905×10^(-3) mg/L and median lethal dose (LD50) was 1.1435×10^(-8) mg/larva for the 3rd instar newly exuviated larvae. No toxicity was observed when normal concentrations of Chlorantraniliprole were used to fumigate the silkworm rearing room. Both irrigation and leaf spraying with 1.25×10^(-4) mg/L Chlorantraniliprole solution showed strong systemic transmission properties in root, leaf and whole plant. The residual toxic period of this insecticide to silkworm was very long. Mulberry leaves sprayed with 1.25×10^(-4) mg/L Chlorantraniliprole solution could still cause 100% mortality of the 3 and 5 instar larvae after 60 d. Furthermore, toxic reaction was very quick. The poisoning symptoms emerged within 1~5 h after feeding on the poisonous leaves. The poisoned larvae experienced such symptoms as stopping ingestion, remaining still, vomiting slightly and body atrophy sequentially, and died ultimately.

食下毒力试验结果经Pearson拟合度检验表明,氯虫苯甲酰胺对3龄起蚕的食下致死中浓度(LC50)为4.0905×10^(-3)mg/L,致死中量(LD50)为1.1435×10^(-8)mg/头;药剂在常规浓度下对家蚕无熏蒸毒性;1.25×10^(-4)mg/L稀释药液对桑树根灌和喷叶处理,表现极强的根部、叶部和全株性内吸传导特性;药液对家蚕的残毒期很长,1.25×10^(-4)mg/L稀释药液田间喷雾桑叶,间隔60 d后采叶饲喂3龄和5龄蚕的死亡率均为100%,且中毒反应极快,添食毒叶后1~5 h出现中毒症状,经停止食桑、静伏、少量吐液、蚕体萎缩等过程后陆续死亡。

On the basis of summarizing separation method of acetic acid-water system, we studied the azeotropic distillation process of acetic acid-water system, selecting butyl acetate, isobutyl acetate and isopropyl acetate as entrainers. The influence of packing height, ratio of water to entrainer and acetic acid initial concentration to separation effect of azeotropic distillation was studied in detail. Simulation calculations of general distillation and azeotropic distillation were carried out. The influence of reflux ratio, theoretical plate, feed position, feed temperature and feed concentration to distillation process were discussed. Preferred process operation parameter, which had guiding meaning to practical production of distillation process were obtained. Basic data for the process amplifying design of azeotropic distillation tower were provided. Invest and operation energy consumption of two distillation methods were compared. The elementary technical design of azeotropic distillation tower was carried out on the basis of result of simulation calculation. The type of major auxiliary equipments and inner parts of packed tower were selected.The research results are as follows:(1) Butyl acetate, isobutyl acetate and isopropyl acetate could be selected as entrainer, and separation effect was near.

本文在综述醋酸-水体系分离方法的基础上,以醋酸丁酯、醋酸异丁酯、醋酸异丙酯为挟带剂,对醋酸水溶液进行共沸精馏过程研究,详细研究了填料高度、水与挟带剂的配比、醋酸初始浓度等对共沸精馏分离效果的影响;对醋酸-水体系进行普通精馏和共沸精馏过程模拟计算,讨论了回流比、理论板、进料位置、进料温度和浓度对精馏过程的影响,获得了对醋酸-水体系精馏过程实际生产具有指导意义的较佳的工艺操作参数、共沸精馏塔的工艺设计放大的基础数据,并对两种精馏方法的投资、操作能耗进行了比较;同时在共沸精馏模拟计算的基础上进行了共沸精馏塔的初步工艺设计计算,并对填料塔的主要辅助设备及塔内件进行了初步选型。

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