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Novozym 435 was used for the synthesis of vitamin A plamitate. The influences of solvent, the molar ratio of substrates, the reaction temperature and time, and the water concentration were optimized and the best result was obtained by interesterification from 0.200 g vitamin A acetate and 0.468 g palmitic acid, at 30℃, in 10 mL hexane, containing 0% of water, with 10% of lipase(mass ratio, immobilized lipase to vitamin A plamitate). In these conditions, 75% of vitamin A acetate was converted into vitamin A plamitate. The immobilized lipase was reused about 6 batches.

对催化合成维生素A棕榈酸酯反应的脂肪酶和反应介质比较,同时对影响合成维生素A棕榈酸酯反应的因素(温度、初始水含量、底物摩尔比、反应时间和酶量等)进行了探讨,优化了反应条件:在10 mL不含水分的正己烷中,0.200 g 维生素A醋酸酯和0.468 g棕榈酸在酶量为10%(指固定化酶与维生素A醋酸酯的质量比)的固定化脂肪酶催化下,在 30℃、190 r/min下反应6 h,转化率可以达到75%,固定化酶可连续使用6次以上。

In Chapter 2, a microwave land emissivity model by Weng etc is introduced, and the sensitivity of the emissivities model to various land parameters is tested.

第二章引入Weng等人的复杂地表比辐射率模式,运用该模式对不同地表类型的地表比辐射率进行了各敏感性参数的实验,以研究其变化的规律。

Is a natural evolution from realism, from development, which has the features of realism and realism, realism, it is further than reality; naturalist on the environment, scenery, the people, the psychological aspects of the activities described in a more objective than reality and, more specifically, more nuanced, as Zola answered some of his critics, said:"I say the things I saw, I put it down, so it…… my work is not political parties and advocacy works, it is true performance works."

自然主义是从现实主义演变、发展而来,它具备现实主义的写实特征,就写实而言,它比现实主义更进一步;自然主义对环境、景物、人物的心理活动等方面的描写比现实主义更客观、更具体、更细腻,正如左拉回答一些人对他的批评时所说的那样:&我说出我看见过的东西,我把它记录下来,如此而已……我的作品不是党派和宣传的作品,它是表现真实的作品。&

The primary amine of DETA is closed by ethyl methyl ketone to reduce the reactivity of –NCO group and –NH2 group and smooth the reaction process. The mole ratio value of –NH2/-NCO should be 2.2 to make sure that –NCO group is completely closed in by –NH2 group and amine terminate compound is prepared. The reaction temperature, reaction time and the way of adding raw materials to vessel are discussed. Structure and performance of the resin are analyzed with infrared ray spectrum.

用甲乙酮封闭DETA分子中的伯胺基团,降低-NCO与-NH2的反应活性,使反应平稳进行;研究投料比和投料方式对反应的影响;为确保生成以氨基封端的聚氨酯树脂,并将游离的异氰酸酯反应完全,最佳原料投料比控制在-NH2/-NCO=2.2;确定合理的合成条件如反应温度、时间等;利用红外光谱分析端氨基聚氨酯树脂的结构与性能。

"Ontology" in the Chinese etymology means "the highest","the most fundamental","the most popular" and "the most important". Although it is a loan word, it has great difference from the oringinal meaning of ontology when translated into Chiness and has abvously "transferred meaning". If the "original meaning" of ontology is a "transcendental" purely logic stipulation" and a unique morphology of "the Western Philosophy", a field of idea world, absolute spirit, pure reason which is isolated from the experience world or prio to the experience world", and "a pure principle unable to be proven from the real world", then in Chiness,"ontology" has richer transferred meanings unparalleled with ontology in the West.

&本体&在中文词源里,有&最高&、&最根本&、&最普遍&、&最重要&等含义;本体论虽然是外来词,但翻译为中文后,与原来的ontology已经有了很大的区别,产生了明显的&转义&:如果说ontology的&本义&是一种&是论&或&存在论&,是一种超验的&纯粹的逻辑规定性&,是&西方哲学特有的一种形态&,是&与经验世界隔绝或者先于经验世界的理念世界、绝对精神、纯粹理性的领域&,是&不能从现实世界得到验证的纯粹的原理&,是比一切其他哲学思维都更纯正的&第一哲学&的话,那么在中国的&水土&上,&本体论&已经具有了比西方的ontology丰富得无可比拟的&转义&。

The esterification reaction was carried out in isooctane solvent at 50℃, with 0.15mol/L of substrate and 1:1.4 of acid-alcohol molar ratio.

研究了反应温度、溶剂、底物浓度、底物摩尔比、吸水剂用量等因素对酯化反应的影响,确定了正戊酸异戊酯的最佳合成条件为:反应温度为50℃,异辛烷为反应介质,底物浓度为0.15mol/L,酸醇摩尔比为1:1.4。

The separation purities by new method were determined and compared with those of some traditional methods by SDS-PAGE gradient electrophoresis.

其次,采用中性蛋白酶、碱性蛋白酶等几种常用的蛋白酶对分离的7S和11S球蛋白进行酶解比较实验,发现在相同条件下,7S比11S酶解后的酸溶多肽得率高,7S比11S相对更容易被酶解;通过扫描电镜和SDS-PAGE电泳分析7S和11S的酶解产物,表明7S和11S分子酶解前后的变化明显,但两种大豆蛋白经酶解作用后,均有相当部分未被酶解的蛋白分子残留在酶解残渣中,而酶解离心后的上清液中则已基本不存在原来的蛋白质大分子。

The main research contents are as follows:1. Through massive calculation, analysis and comparison, sum up the similarities and differences between the special-shaped cross sections and rectangular cross sections in mechanical features, between reinforced concrete special-shaped columns and rectangular columns in load-bearing capacity, ductility performance and provide necessary basic concepts and data for further understanding the characteristics of the special-shaped columns;2. Through massive elastic calculations and elasto-plastic analysis, under the preconditions of satisfying the code's requirements for axial compression ratio, limit value of lateral displacement and load-bearing capacity of normal section,oblique section and beam-column joint, under circumstances of different intensity of earthquake, structure dead weight, sort of site and column grid bay dimension, the variation regularity of maximum suitable height of structure, and thus sum up the maximum suitable height of structure for code for the purpose of macro-control while deciding the design scheme;3. Make a preliminary study on the stress feature of reinforced concrete special-shaped column and Z-shaped column of which the ratio of limb length to limb thickness is between 4~5 ,and the preliminary design method is suggested;4. Through elato-plastic time history dynamic analysis of typical projects, check up the weak storey of the special-shaped column structure and yielding, breaking and collapse mechanism to satisfy the earthquake resistant requirement to buildings of remaining stand under strong earthquake;5. Derive for project use simplified calculation formula of vibration period, suitable vibration period, suitable rigidity of special-shaped column structure through theoretical analysis, and provide an easy and practical method for deciding the structure scheme economically, safely and reasonably;6. Based on the study achievements in theory and massive analysis and calculations of this paper, sum up the regularities of inner force, deformation of special-shaped column structure and seismic conceptual design, and thus the suggection of seismic design of special-shaped column structures is presented.

本文研究的主要内容如下:通过大量的计算、分析和对比,总结出异形截面与矩形截面在力学特性、钢筋混凝土异形截面柱与矩形截面柱在承载能力、延性性能等方面的异同,为深入了解异形截面柱的特点提供必要的基本概念和数据;通过大量的弹性及弹塑性计算分析,在满足规程对轴压比、侧移限值及正截面、斜截面、节点承载力抗震验算要求的前提下,在不同抗震设防烈度、结构自重、场地类别及柱网开间尺寸情况下最大适宜高度的变化规律,并在此基础上总结归纳出异形柱结构的最大适用高度规定,可用于规程,以便于在确定方案时起到宏观控制的作用;对肢长与肢厚比在4~5的钢筋混凝土异形截面柱及Z形柱的受力特点进行初步探讨,提出初步的设计方法;通过对典型工程的弹塑性动力时程分析,检验异形柱结构的薄弱层及屈服、破坏、倒塌机制,以达到建筑物大震不倒的抗震设防要求;通过理论分析,推导出异形柱结构自振周期,以及适宜自振周期、适宜刚度的工程实用简化计算公式,为经济、安全、合理地确定结构方案提供简便实用的方法;在本文理论分析、计算以及大量的研究成果基础上,总结归纳出异形柱结构内力、变形的规律及抗震概念设计内容,并在此基础上提出异形柱结构的抗震设计建议。

Based on the method of neural network the relationship between the water demand ratio and the geometric and rheological characteristic parameters of fly ash was studied.

通过建立BP神经网络模型,处理了粉煤灰颗粒群特征参数(比表面积、形状因子、分数维、烧失量)和流变学参数(屈服应力、塑性粘度等)与其需水量比之间的关系。

These complexes showed modest catalytic activity, and the PDIs of the polymers obtained were relatively broad.6. Reaction of CpjLn with MBMPHa in THF in 1 :1 molar ratio, isopropanol was added to the system in 1 equiv., after workup, a new kind of neutral lanthanide complexes [LnCw-OiPrXTHF2]2 Ln = La (14, Nd (15),Yb (16) were gained.

配合物cp3Ln与MBMPH:按卜1的摩尔比在THF中反应1小时,然后再原位按卜1的摩尔比加入异丙醇,合成了中性的桥联双芳氧基稀土烷氧基配合物 [L城犷0,P以THF2]2Ln=La(14,Nd(15),Yb(16),产物经红外光谱,元素分析和核磁共振氢谱(配合物14)等表征。

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Singer Leona Lewis and former Led Zeppelin guitarist Jimmy Page emerged as the bus transformed into a grass-covered carnival float, and the pair combined for a rendition of "Whole Lotta Love".

歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车,和一双合并为一移交&整个lotta爱&。

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