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Pyruvaldehyde was synthesized with acetone or 1,2 propanediol as starting material respectively.With n∶n=1 00∶0 79,3 0-4 0 g potassium chlorate as catalyst,and water and glacial acetic acid as solvent,refluxing on water bath of 60-75 ℃ for 4 h,bromoacetone was obtained in 63 5% yield.

分别用丙酮和 1,2 丙二醇做原料合成了丙酮醛。n∶n =1 0 0∶0 79,加入 3 0~4 0g氯酸钾做催化剂,水和冰醋酸做溶剂,水浴温度为 6 0~ 75℃,回流 4h ,制得产率为 6 3 5 %的溴丙酮。V∶V =11 9∶1 0 ,通入空气,在 6 5~ 70℃反应 5~ 8h ,制得产率为 5 9 6 %的丙酮醛。

In order to improve thermal efficiency of gaseous suspension calciner ,after calculating and analyzing the heat balance,the result shows that:the main factors of influence of output and energy utilization of furnace are air surplus coefficient,aluminium hydroxide moisture and temperature of the main furnace.

为进一步提高气体悬浮焙烧炉的热效率,对某厂氧化铝焙烧系统进行了热工测试和热平衡计算,分析结果发现,影响焙烧产量和能耗的主要因素为空气过剩系数、氢氧化铝水分和主炉温度。

In order to improve thermal efficiency of gaseous suspension calciner ,after calculating and analyzing the heat balance,the result shows that:the main factors of influence of output and energy utilization of furnace are air surplus coefficient,aluminium hydroxide moisture and temperature of the main furnace.

为进一步提高气体悬浮焙烧炉的热效率,对某厂氧化铝焙烧系统进行热工测试和热平衡计算,分析结果发现,影响焙烧产量和能耗的主要因素为空气过剩系数、氢氧化铝水分、主炉温度。

The relative release rate of capsulated camphor oil was studied with the method of losing weight under normal pressure and temperature.

在常温、常压下用失重法研究了樟脑油微囊的相对释放速率,并考察了释放速率与样品合成时水相pH、水相离子强度、微囊化、温度及空气相对湿度的关系。

Carbon-nitrogen co-doped titanium dioxide (TiO2) nanoparticles were synthesized by calcining titanium carbonitride powder in air at different temperatures.

采用TiCN粉末在空气气氛中不同温度下焙烧制得C-N共掺杂的纳米TiO2光催化剂。

Storage of drug products after release;(9) Control and laboratory operations;(10) Aseptic processing, which includes as appropriate: I Floors, walls, and ceilings of smooth, hard surfaces that are easily cleanable; II Temperature and humidity controls; III An air supply filtered through high-efficiency particulate air filters under positive pressure, regardless of whether flow is laminar or nonlaminar; IV A system for monitoring environmental conditions; V A system for cleaning and disinfecting the room and equipment to produce aseptic conditions; VI A system for maintaining any equipment used to control the aseptic conditions.

无菌操作及有关要求: I 地板,墙壁和天花板平滑,坚硬,表面易清洁; II 温度与湿度控制; III 空气经高效过滤器,在正压下过滤,层流或非层流均可; IV 环境检测系统; V 创造无菌环境,房间和设备的清洁,消毒系统; VI 控制无菌环境的设备维修系统。

And the feasibility of the two measurement methods is demonstrated.3 Computer simulation is performed in the situation of air passing by a heating columned thermistor through a round pipeline. The fluid velocity and temperature distributions under different mass flowrate are shown. They reflect the impact the heating thermistor has on the fluid. The velocity distribution on the surface of the heating thermistor is studied and the impact of natural convection is revealed. The lower limit of measurement based on the simulation result is given.

仿真实验结果给出了不同空气质量流量下加热元件周围流体的速度和温度分布,直观反映了加热元件对流动产生的影响;研究了发热元件表面流体的速度分布,揭示了由浮升力引起的自然对流对流量测量的影响,给出了测量下限值的仿真结果;并通过仿真实验数据验证了恒功率热消散式热式流量计的流量方程。

In the system the prepare heating area is compart from high temperature area,and there is a board to separate the outside airs.The temperature curve of the system is quite good, and it works well when drawing diversified structures MPOF.

文章介绍了一种分区加热系统,该系统将预热区和高温区隔离开来,并采用隔板与外界空气隔离,可以达到比较理想的温度曲线,满足了制作不同结构MPOF时的需要。

Sulfur corrodible sites and their characteristics were introduced of the prefractionation system, air preheaters of heating furnace and product air coolers etc,and chlorine corrodible sites and their characteristics were also presented of the thermocouple casing tubes, product air coolers and fire arrestors of heating furnace etc in the catalytic reforming and diesel hydrogenated unit s.

介绍了中国石油哈尔滨石化公司催化重整及柴油加氢装置在预分馏系统、加热炉空气预热器、加氢装置反应产物空冷器等处易发生硫腐蚀和在预加氢热偶套管、加氢反应产物空冷器、加热炉阻火器等处易发生氯腐蚀的部位及其表现特征,指出装置在低温(不高于120℃)、含水、容易被堵塞的部位易形成HCl-H2S-H2O腐蚀体系,分析了腐蚀原因和介质来源,总结和提出了开好原油的电脱盐、采用脱氯技术、加强对加热炉的排烟温度控制和腐蚀介质的精制与净化、加大空冷器的注水量等针对性防腐经验和措施。

There are three kinds of drying systems: hot air drying, dehumidify ing drying, and natural drying; however, hot air drying is the most popular drying system.

本研究的目的为探讨热能回收技术的效能,在热风干燥系统中设计和研制排放湿热气和进入空气接触的热能回收装置,达到加热进气温度,减少干燥作业所需能源。

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Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气,收缩臀部肌肉;拱起身体,尽量抬起头来,右腿伸直朝向天花板(膝微屈,以避免肌肉紧张)。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化,但却比去年同期高8%。

However, to get a true quote, you will need to provide detailed personal and financial information.

然而,要让一个真正的引用,你需要提供详细的个人和财务信息。