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The main applications in the spectroscopic studies and lifetime measurement of highly ionized ions are summarized.2 The experimental principle and method of beam-foil spectroscopy are presented, andthe application of the isoelectronic sequence in the analyses of spectra is described, Cowan program for the theoretical calculations is introduced.3 The main facilities in our experiment are introduced.

本文对高离化态Cu和Ge离子的光谱进行实验研究，得到了一些新的实验结果，论文的主要内容如下： 1 回顾了束箔光谱法的发展历史，介绍了束箔光谱法的优点；总结了束箔光谱法在高离化态原子能级研究，高离化态原子能级寿命测量等方面的主要用途。

At first it may seem rather strange to treat the chemistry of the halogens and the noble gases,two groups that represent the extremes of chemical activity and inertia ,in the same section .the superficial differences between the halogens and the noble gases are much reduced,however if we focus our attention on the comparison of halide ions(particularly F-) with the isoelectronic noble gas atoms and the noble gas compounds with halogen atoms or the halogens in their higher positive-oxdation states.

起初它可能看起来非常奇怪对待的卤素化学和惰性气体，两个团体代表在同1节的化学活性和惯性的极端。与卤素和惰性气体的表面差异大大减少，但是，假如偶们着眼于（非常是架F -等电子与惰性气体原子和原子与卤素或在卤素稀有气体化合物）卤离子的比较，我们的注意力较高的正- oxdation国家。

ER is well characterized as a mobilizable calcium store that sequesters excess cytosolic calcium and a reservoir for calcium signaling to maintain intracellular Ca2+ homeostasis.

2钙离子的检测 1、细胞内质网是[Ca~(2+)]_i的主要储存场所，以及[Ca~(2+)]_i在细胞凋亡的信号转导通路中所具有的重要作用，本实验研究了SfaMNPV诱导SL-1细胞凋亡过程中细胞内[Ca~(2+)]_i的变化以及[Ca~(2+)]_i可能在凋亡信号转导通路中的意义。

To improve the yield of an Amide-type Tripodal Ligand and investigate its coordination with rare earth ion under mild condition,a series of Amide-type Tripodal Ligands(L1—L4) have been prepared by the reactions of nitrilotriacetic acid and oxalyl chloride with four kinds of amides,respectively.

为了提高酰胺型三脚架型配体的产率，进一步研究其与稀土离子的配位形式及配合物的荧光性能，以氨三乙酸为母体，草酰氯为氯化试剂，与4种胺在较温和的条件下合成了具有三脚架型结构的配体(L1—L4)，并考察了实验条件、反应温度、反应体系溶剂、缚酸剂、反应时间及催化剂对反应产率的影响。

Kinetic spectrophotometric method for the determinationof trace nitrilotriacetic acid;2. To improve the yield of an Amide-type Tripodal Ligand and investigate its coordination with rare earth ion under mild condition,a series of Amide-type Tripodal Ligands(L1—L4) have been prepared by the reactions of nitrilotriacetic acid and oxalyl chloride with four kinds of amides,respectively.

为了提高酰胺型三脚架型配体的产率，进一步研究其与稀土离子的配位形式及配合物的荧光性能，以氨三乙酸为母体，草酰氯为氯化试剂，与4种胺在较温和的条件下合成了具有三脚架型结构的配体(L1—L4)，并考察了实验条件、反应温度、反应体系溶剂、缚酸剂、反应时间及催化剂对反应产率的影响。

The study showed that the biosorption process could be described well by pseudo-second-order kinetic model and Freundlich isotherm model.Higher cell concentration was favorable to the biosorption.Temperature's effect on the biosorption was not obvious.The oxygenous and nitrogenous functional groups on the cell wall played a very important role in the process of biosorption.Microdeposits were formed by int...

结果表明，菌体对银的吸附量可达91.75 mg/g，吸附过程符合Pseudo-second Order吸附动力学模型，相关系数高达0.999 9；吸附热力学很好地符合Freundlich吸附等温模型，相关系数为0.99；考察菌体浓度和温度对吸附的影响发现，菌体浓度增加有利于对银离子的吸附，温度对吸附影响较小；FTIR、SEM及EDAX实验结果表明吸附存在2种吸附机理，一为菌体表面一些含氮氧的基团对Ag+的络合作用，二为菌体分泌的胞外多糖等物质对Ag+的微沉淀成晶作用。

In the second part of this work, a computor program is developed to calcalate〓L〓energy levels, reduced matrix elements, crystal field energy levels, oscillator strengths of f-f transition and theoretical f-f absorption spectra of f-ions. The calculation results of the f-f absorption spectra of Nd in water coordination sphere and H di (2-ethylhexyl phosphinic acid coordination sphere with different symmetric structure are shown and compared with observed spectra.

在第二部分中，编制了计算f离子的〓L，能级、约化矩阵元、晶体场中Stark能级分裂、f-f跃迁振子强度及f-f理论吸收光谱的计算机程序，以此程序分别计算了Nd在不同结构对称的水配位层及烷基磷酸配位层中的f-f吸收光谱，通过与实验谱比较，识别了可能的配位层结构，并讨论了f-f跃迁的强度机理。

The results from ultraviolet spectroscopy and photo -luminescence spectroscopy revealed that:(1) Europium complexes based on neutral ligands, such as azaphenanthroline 2-aryl-5-(α-pyridyl)-1,3,4-ozadiazole had a strong UV absorbance at the wavelength of 290-350 nm and the characteristic PL spectrum of europium ion at 613 nm respectively;(2) The structures of ligands had a critical role influence on PL intensity of europium complexes.

紫外光谱和光致发光光谱研究表明：(1)以氮杂邻菲罗啉、2-芳基-5--1，3，4-噁二唑为中性配体的铕配合物在290～350nm左右都有强烈的紫外吸收，且在紫外光的激发下都能产生铕离子的特征光谱(613nm)；(2)配体的结构是影响铕配合物发光强度的关键因素之一。

Previous studies by others and this laboratory on the allosteric effect of hem oglobins have suggested that the electrostatic replusive cavity at the center of tetrameric moiety plays a substantial role in regulating O2 transport prope rties, including chloride binding, and Bohr effect .

中文摘要过去对血红蛋白异位调节效应的研究指出，在血红蛋白四合体中央空腔的区域的静电排斥效应对分子机能的调节如氧合时氯离子的键结和波尔效应，扮演著一个很重要的角色。

In order to investigate the relationship between the open-chain ligands and metal ions, and the possibility of the metal complexes used as electroluminescent materials, a new naphthol schiff base ligand which is a open-chain crown and its four transition metal complexes, a new amide type tripodal ligand containing heterocyclic ring, two tripodal ligands (H〓L〓 and H〓L〓) containing phenol schiff bases and their rare earth complexes were synthesized and characterized.

为了进一步研究和探讨开链配体与金属离子的配位作用，以及金属配合物作为电致发光材料的可能性，我们设计合成了含萘酚环的Schiff碱开链冠醚H〓L〓及四种过渡金属(Zn、Ni、Co、Cu)配合物，两个含酚羟基的Schiff碱三足配体H〓L〓和H〓L〓及稀土配合物，一个含杂环的酰胺型三足配体L〓，培养了配体L〓的单晶，确定了其晶体结构。

By the time of its fall, most of the prisoners were writers who had written against the corruptions of the government.

到它被攻陷的时候，里面多数的犯人是写了反对政府贪污文章的作家。

The most obvious variation to ovum morphological character was that the color was changed from light green to sepiaceous in embryonic development, and all the ovums were almost hatched after 96h.

在胚胎发育过程中卵的形态特征最明显的变化是颜色从淡绿到深褐色，卵在发育96h后卵基本全部孵化。