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The questing for acidic middle-temperature electroless Nickel technology leads to the preferable prescription as follows:Proportion of Nickel Sulphate and Sodium Hypophosphate 0.36; Sodium Acetate 15g/L; Stabilizer A lmg/L(Stabilizer B Img/L for continual experiment); Composite complexing agent Lactic Acid 10ml/L and acetic acid 10 ml/L; Accelerator organic acid G 6g/L; pH value 5.0; Loading Capacity ldm2/L; Temperature 70C (Temperature 75C for continual experiment); Proportion of supplement for Nickel Sulphate and Sodium Hypophosphate 1:1.2; Testing the consumed ion of Nickel solution and supplement inspissations solution every 60min by the proportion of 15% fresh solution.

最后,通过研究得出最佳工艺配方为:硫酸镍与次亚磷酸钠的摩尔比为0.36;乙酸钠15g/L:稳定剂Almg/L(周期实验加稳定剂B10mg/L);复合络合剂组合为乳酸10ml/L+冰乙酸10ml/L:促进剂为有机酸G6g/L;pH值为5.0;装载量为1.0dm~2/L;施镀温度为70℃(周期实验为75℃):主盐与还原剂的添加比例1:1.2;每60分钟对镀后液进行镍离子浓度的测定并按镍离子的消耗量添加浓缩液,添加比例按开缸液的15%。

This suggested that the H(superscript +) for initiating the reaction was supplied partly by the 2-H of imidazole.

通过对反应后液体产物的GC-MS分析,提出了离子液体催化的苯与乙烯烷基化反应的正碳离子机理。

An ion implanter and an ion implanting method compatible for both positive and negative ions.

一种离子注入机和一种对正离子和负离子均适用的离子注入方法。

Recently open-chain marocyclic ligand and then lanthanide complexes have attracted much attention mainly because the ligands have the unique molecular structures: changeable chain, inflexibly terminal group and high selectivity and coordination to lanthanide ions.

一个优良的发光器件必须具备以下几个条件:配体对金属离子有较高的选择识别性能;配体含有共轭发色团有利于能量从配体向中心离子转移;配合物具有相对较高的动力学和热力学稳定性。

A device with high temperature Cr inside is made to reduce water to hydrogen.The method for reducing the interferer of H3+ to HD+ is discussed.

自制了高温铬还原制氢装置;探索了降低复合氢离子H3+对氘化氢离子HD+干扰的方法。

The studies about the effect of ion-pair reagents on charged metal chelates are limited, and have no definite conclusions.

流动相中引入对离子试剂使反相HPLC的应用范围扩大到离子型化合物。

The influences of alkali concentration, temperature, polymer and additive on ionic conductivity and electrochemical stability were studied with orthogonal experiments and single factor experiments design, the relation of structure and ionic conductibility is researched by FIRT, XRD,DSC and SEM analysis ways.

结合正交设计实验和单因素实验研究了碱浓度、温度、聚合物以及增塑剂对固体电解质离子电导率、电化学稳定性的影响,用红外光谱、X衍射分析和差热分析等手段研究其结构与离子导电性能的关系,摸索出了本实验条件下的最优方案。

The main content of this paper as follows: The acidic strength, reaction temperature, reaction time of Chlorine-aluminate Ionic Liquids with different structure of cation on the activity of transalkylation of MN with TeMB and the selectivity of 2,6-DMN were studied. The optimum reaction condition was obtained: the molar fraction of AlCl_3 is 0.71, molar ratio of 2-MN and TeMB is 1, the amount of ionic liquid is 32wt%, reaction temperature is 20℃and reaction time is 8h using X-xAlCl_3 and X-xAlCl_3 as catalysts; the optimum reaction time is shortened 6h using Et_3NHCl-xAlCl_3 as catalyst.

本文主要研究了以下内容:分别考察了不同阳离子结构的氯铝酸盐类离子液体的酸强度、反应温度、反应时间等因素对MN和TeMB转移烷基化的催化反应活性和2,6-DMN选择性的影响,优化得到适宜的反应条件为:以X-xAlCl_3和X-xAlCl_3为催化剂时,AlCl_3的摩尔分数x=0.71,2-MN和TeMB摩尔比为1∶1,离子液体用量为32wt%,反应温度为20℃,反应时间为8h;以Et_3NHCl-xAlCl_3为催化剂时,反应时间缩短到6h。

Structures of their lanthanide complexes which were obtained by simulating the pseudo-contact shifts of the complexes are presented.

在此基础上,通过对镧系离子诱导位移的分析和模拟,计算了氨基酸镧系离子配合物的13^C NMR作接触位移,模拟了配合物的分子结构。

We compared the spectral and its secondary structure of endostatin with and without of zinc, heparin and lanthanides. It demonstrated that the pH has strong effect on the interaction of endostatin and heparin.

研究了内皮抑素与锌离子、肝素、稀土离子作用后蛋白质的光谱学性质和二级结构的变化,首次发现偏酸性pH对肝素与内皮抑素的结合作用有特殊影响,为研究内皮抑素特异抑制肿瘤组织新生血管的生成提供了实验依据。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。