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The purity of SAM product was higher than 95%, and the overall recovery of SAM sulfate and SAM double salt of sulfate and p-tosylate were 60% and 50%, respectively.

通过筛选,获得了对SAM有较好选择性离子交换能力、较易洗脱和再生的争光D113弱酸型阳离子树脂,研究了温度、pH等对SAM离子交换的影响,根据SAM在弱酸阳离子树脂D113上的等温交换平衡行为表现出较强的可逆性,考虑到交换基的弱电解质性质以及结合Donan膜平衡理论,建立了考虑pH影响的可逆离子交换平衡模型,该模型可以较好地描述SAM平衡浓度、pH对离子交换平衡的影响;通过对动态离子交换过程的研究,得到了SAM在D113树脂内的有效扩散系数的数量级为1.0E-9cm〓/s~1.0E-8cm〓/s。

The effect of ferrous iron on the leaching rate of gallium and phosphorus was not significant.

镓和二价铁离子的沉淀率随磷酸根离子浓度的增加而增加,当磷酸根离子与金属离子摩尔比大于1:1后,磷酸根离子浓度对沉淀率的影响不再变化;温度对镓离子沉淀过程的影响较小,对二价铁离子的沉淀过程影响较显著。

The influences of three instrumental parameters of ICP-MS spectrometer(radio frequenceypower, nebulization gas flowrate and ion lens voltage)on signal intensity and productivity of a few kinds ofions formed from 15 rare earth elements in the plasma(single element ions RE+,oxide ions REO+,hydroxideions REOH+ and hydride ions REH+)have been investigated.

研究了电感耦合等离子体质谱法的仪器主要参数(射频功率、雾化气流量、离子透镜电压)对15种稀土元素的离子、氧化物离子、氢氧化物离子和氢化物离子信号强度及各多原子离子产率的影响,并对各稀土元素多原子离子产率与各稀土元素性质的关系进行了探讨。

With the mixed bacteria after aerated as the research subject,the effects of the different iron valences and concentration on hydrogen production capacity were discussed.

以驯化后的混合菌种为研究对象,在间歇实验的基础上探讨了不同价态的铁及不同浓度的二价铁离子对其产氢效能的影响。

The main influence of sulfide ions on the SS is that they increase the passive current density I.

离子对不锈钢耐蚀性能的影响主要是使不锈钢的钝态电流密度I。

The influence of K(superscript +), Na(superscript +), Ca(superscript 2+) upon the regenerative velocity of the planarians head was carried out with the anatomical lens by appearrance of two eyespots as regeneration finished mark.

用解剖镜观察,以眼点的出现为完成再生的标志,在恒温10℃条件下研究了钠、钾、钙离子对日本三角涡虫头部再生速度的影响。

Based on both the strong-weak model and the strong-strong model, the instability caused by ions in equilibrium is simulated, some useful results are obtained. The results include the relation between instability growth rate and neutralization factor, the relation between instability threshold and neutralization factor, and the incoherent tune shift, the tune spread, the ion cloud distribution, the ion loss mechanism, as well as the ion accumulation limitation in the storage ring. With this understanding, we have carried out theoretical and experimental study for some ion clearing methods and their effects for the HLS ring. The minimum static clearing voltage is determined through calculating beam electric field and measuring ion current.

在上述基础上,我们对各种离子清洗的方法及清洗效果进行了理论和实验的研究:通过计算束流电场和测量清洗电极上的离子流来确定直流清洗电极所需的最小清洗电压;通过测量离子引起的频移来计算储存环的中性化系数;用模拟计算和实验测量证实了高频清洗能有效地克服储存环上离子俘获不稳定性;对由高频剔除系统形成的储存环部分束团填充模式下的离子俘获问题进行了初步研究,证实采用束团部分填充模式能在一定范围内克服离子俘获效应;并对各种离子清洗方法进行了比较。

Ion-pair solid phase extraction ; Photometry ; Cobalt ; Nitroso R salt

离子对固相萃取;光度法;钴;亚硝基R盐

In an acetate buffer of pH 6.0,and in the presence of CTMAB,a stable complex,having the mole ratio of 1 to 3,was formed between cobalt ion and nitroso R salt,which was concentrated on C18 solid phase extraction column,achieving a concentration multiplication of 100 times.

研究了用亚硝基R盐离子对固相萃取光度法测定钴,在pH 6.0的HOAc-NH4OAc缓冲介质中,溴化十六烷基三甲基铵存在下,亚硝基R盐与钴反应生成3∶1稳定络合物,该络合物可用C18固相萃取小柱富集,富集倍数达100倍,小柱上富集的络合物用乙醇洗脱后用光度法测定,钴的质量浓度在0.05~5.0 mg.L-1内符合比耳定律。

Firstly, the analysis method of purines in beer was established with the reverse- phase ion pair chromatography.

本文首先建立了啤酒中嘌呤类物质的反相离子对色谱分析方法。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。