磺酸

Monodispersive Au nanoparticles were synthesized via the redox reaction between diphenylamine sulfonate and HAuCU-The effect of the amount of sodium diphenylamine sulfonate and polyon the morphology and size of Au nanoparticls were examined.

利用四氯合金酸和二苯胺磺酸钠反应，制备了大小均匀的金纳米粒子。考察了还原剂二苯胺磺酸钠和保护剂聚乙烯吡咯烷酮的用量的变化对金纳米粒子形貌和大小的影响。

The synthesis methods of dibutyl succinate catalyzed by p-toluene sulfonic acid, amino sulfonic acid,strongly acidic cationic exchange resin, ferric chloride hexahydrate, stannic chloride pentahydrate, copper sulfate , ammonium ferric sulfate dodecahydrate, titanium sulfate, sodium bisulfate monohydrate,and solid super acid et al were reviewed.

本文评述了对甲苯磺酸、氨基磺酸、强酸性阳离子交换树脂、六水三氯化铁、五水四氯化锡、十二水合硫酸铁铵、硫酸钛、一水硫酸氢钠和固体超强酸等催化剂催化合成丁二酸二丁酯的方法。

Based on the basic principle of acid and alkali in this article, acid and alkali of environment outside synthesized aminobenzene sulfonate high performancing water-reducing was analysized.

本文分析了氨基苯磺酸高效减水剂合成环境中酸碱性影响，运用重量实验和红外光谱的方法，研究证实了氨基苯磺酸高效减水剂的合成反应机理。

Objective To observe the effects of calcium dobesilate on the expression of CD34 and von Willebrand factor in peritubular capillary in renal tissues of rats with chronic arisolochic acid nephropathy and to explore the probable mechanism concerned. Methods Sixteen Wistar rats were infused with Caulis aristolochia manshuriensis decoction for 12 weeks, then randomly divided into 2 groups.

目的 观察羟苯磺酸钙对慢性马兜铃酸肾病大鼠肾小管周毛细血管内皮细胞特异抗原CD34和血管性血友病因子表达的影响，探讨羟苯磺酸钙改善CAAN大鼠模型肾脏微循环障碍的作用和机制。

In the fifth chapter, six compounds formed between nitrogen-containing ligands such as 2, 2'-bipyridyl, isonicotinamide and 1, 4, 8, 11-tetraazacyclotetradecane and the solution cadmium sulfonates such as 1, 5-naphthalenedisulfonate, 2, 6-naphthalenedisulfonate, 4, 4'-bipenyldisulfonate and 4, 4'-penyletherdisulfonate have been synthesized and structurally characterized. Besides, another compound has been synthesized with cadmium carbonate reacting with 1, 5-naphthalenedisulfonate acid.

第五章以2，2'-联吡啶、异烟酰胺和1，4，8，11-四氮杂环十四癸烷与含有Cd〓和1，5-萘二磺酸根离子、2，6-萘二磺酸根离子、4，4'-联苯二磺酸根离子和4，4'-苯醚二磺酸根离子的水溶液反应，合成了六个化合物，另外以1，5-萘二磺酸与碳酸镉反应合成出一个化合物。

Synthesis process of 2,6-dichloro-3-methylaniline was investigated 3-methylaniline was first N-acetylated with acetic anhydride,then treated with chlorosulphonic acid and ammonia yielding the 2-methyl-4--benzenesulfonic amide,which wasin turn deacetylated,chlorinated and hydrolyzed to the title compound.Hydrochloric acid was used instead of sodium hydroxide in deacetylation and sodium chlorate instead of hydrogen peroxide as oxidant in chlorination.

合成工艺2，6-二氯-3-甲基苯胺调查3-甲基首次N-乙酰与醋酸酐，然后与氯磺酸和氨产量 2-甲基-4--苯磺酰胺基，而擅转乙酰，氯化和水解的标题compound.hydrochloric酸代替氢氧化钠乙酰氯酸钠代替双氧水为氧化剂，加氯。

First,the content of surfactant should be more than 18 percent and the content of anion surfactant should be kept in proper proportion to the content of nonionic surfactant. Second,the content of zinc naphthenate should be kept in directly proportional to the content of other surfactant. Third,the content of rosin shouldnt too higher and the content of oleic acid should be kept in directly proportional to the content of rosin. Fourth,the content of water should be kept in a low level (less than 8%);otherwise emulsifier oil will delaminate. In addition,the requisite content of sodium heavy alkyl benzene sulfonate is higher than petroleum sulfonate.

试验表明在以松香、重烷磺酸钠、石油磺酸钠为主要乳化剂时，要获得优良的乳化液，需满足以下几个条件：(1)需在乳化油配方中加入适量的乳化剂，且其中阴离子乳化剂总量与非离子乳化剂总量的应保持适当的比例；(2)乳化油中环烷酸锌的量与其它乳化剂总量要保持正比关系；(3)乳化油中松香的量不易过大，且油酸的加入量应与松香量成正比；(4)乳化油中水分含量不易过高(一般不能大于8％)，过高时稳定性不好，易分层。

The composition comprises: 35 to 65 wt % of an anionic detergent or surfactant selected from alkyl benzene sulphonic acids, alpha olefine sulfonates, long chain fatty acid sulphates, higher fatty acids, as well as the alkali metal and alkaline earth metal salts thereof, and natural detersive agents, and mixtures of any of these; 3 to 15 wt % of a non-ionic detergent or surfactant selected from alkoxylated alkyl phenols and alkoxylated fatty alcohols; 5 to 10 wt % of a water-swellable cellulose derivative or a salt thereof, wherein the cellulose derivative exhibits a viscosity of at least about 1500 cps, measured in a 1 % aqueous solution at 25 DEG C with a Brookfield viscometer having spindle 3, speed 30rpm, factor 40 for viscosities of 2500-3500 cps; 6 to 20 wt % of a solubility regulator selected from alkali metal and alkaline earth metal chlorides, carbonates and sulphates, aluminosilicates and starch; and 0 to 20 wt % of a fragrance or perfume in solid, liquid or microencapsulated form.

该组合物包含：a35―65％重量的阴离子洗涤剂，其选自烷基苯磺酸、α－链烯烃磺酸盐、长链脂肪酸硫酸盐、高级脂肪酸以及其碱金属和碱土金属盐和天然的去污剂，和任何这些组分的混合物；b）3―15％重量的非离子洗涤剂，选自烷氧基化烷基酚和烷氧基化脂肪醇；c）5～10％重量的水可溶涨的纤维素衍生物或它们的盐，其中纤维素衍生物按1％水溶液在25℃下用Brookfield粘度计（3号转轴，转速30rpm，2500―3500cps粘度的因子是40测定；具有粘度至少约1500cps；d）6―20%重量的溶解性调节剂，选自碱金属和碱土金属氯化物、碳酸盐和硫酸盐、硅铝酸盐和淀粉；和e）0～20％重量的为固体、液体或微囊包封形式的香精。

At first, Polyaniline was synthesized by the improved chemical oxidation technique, then, PANI/HCl, PANI/TSA and PANI/DBSA were obtained by doping emeraldine with HCl, 4-methyl benzene sulfonic acid and dodecylbenzene sulfonate acid, separately. Leucoemeraldine was obtained in the N-dimethylformamide by using phenylhydrazine deoxidizing emeraldine in N_2 atmosphere.

本文首先通过改进合成条件的化学氧化法合成了聚苯胺，经氨水脱掺杂获得本征态聚苯胺，再经盐酸、对甲苯磺酸、和十二烷基苯磺酸掺杂，分别获得到质子酸掺杂的聚苯胺样品，然后在N，N-二甲基甲酰胺中，利用苯肼，在N_2氛围下还原本征态聚苯胺得到还原态的聚苯胺。

The superplasticizer CS-SR3 is completely different from traditional formaldehyde or lignosulphonate based water-reducing admixtures.CS-SR3 is a new kind of high performance polycarboxylate water-reducing admixture without any formaldehyde.

超塑化剂CS-SR3与传统的由甲醛、萘磺酸缩聚而成的萘系和木质素磺酸盐减水剂是完全不同的，是一种新的完全不含甲醛的高性能聚羧酸系高效减水剂。

On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.

另一方面，更重要的是由于城市住房是一种异质性产品。

Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.

气候直方图是将所收集的降水量测定值，分为几个相等的区间作为横轴，并将各区间内所测定值依所出现的次数累积而成的面积，用柱子排起来的图形，也叫做柱状图。