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Amino-monomethoxypoly(ethy1ene glycol)(mPEG-NH2) was synthesized based on the principle of Gabriel synthesis.Monomethoxypoly(ethy1ene glycol) tosylate was prepared at first,and then reaction with potassium salt of phthalimide as nucleophile to produce the monomethoxypoly(ethy1ene glycol)phthalimide derivative.

摘 要:首先合成了单甲氧基聚乙二醇对甲苯磺酸酯,然后根据盖布瑞尔合成法原理,以邻苯二甲酰亚胺钾盐为亲核试剂与mPEG-OTs反应,生成单甲氧基聚乙二醇的邻苯二甲酰亚胺衍生物,mPEG-PI与水合肼反应肼解生成伯胺,合成了一端为氨基的单甲氧基聚乙二醇(mPEG-NH2)。

The hydroxide value and viscidity of lignin-based polyhydric alcohol are 450~550mgKOH/g and 500~1000mPa.s respectively while 20 parts lignosulfonate calcium dissolves in common polyhydric alcohol for 2 hours.

4在160~170℃,20份木质素磺酸钙与GR-4110G多元醇互溶2小时得到羟值为450~550mgKOH/g、粘度在500~1000mPa.s的木质素多元醇。

The FTIR of lignin-based polyhydric alcohol shows new characteristic peak of carbonyl is formed and the characteristic peak of aromatic ring and polyether at 1600cm-1 and 1110cm-1 respectively, which induce there is linkage of chemical bond.

所得木质素多元醇通过红外光谱图表明在1750cm-1附近有新的酯羰基生成,并且在1600cm-1含有木质素的芳香环和1110cm-1的聚醚链,表明木质素磺酸钙与聚醚多元醇在互溶过程中有化学键的接合。

In the present paper,the use of 8-hydroxyquinolinecomplexs in precipitate flotation to separate and preconcentrate Cu and Mn,using SDBS as collector,followed by AAS spectrophotometric determination is proposed.

提出了以8-羟基喹啉为沉淀剂,十二烷基苯磺酸钠为浮选剂,沉淀浮选预分离富集与火焰原子吸收光谱法联用测定痕量Cu和Mn的新方法。

Objective To observe the effect of Traditional and Western Medicine therapy on chronic prostatitis. Methods 150 patients with prostatitic of Ⅲa type were randomly divided into two groups.

目的 观察体外超短波联合野菊花栓及甲磺酸多沙唑嗪控释片治疗Ⅲa型前列腺炎的临床疗效。

Methods 150 patients with prostatitic of Ⅲa type were randomly divided into two groups. Patients in treatment group (n=75) were treated by combination of extraorgan short wave therapy (once 20 mins/day), wild chrysanthemum suppos.(a piece, once a day, take by anus) and controlled release tablets of Doxazosini Mesylas (40 mg, once a day). Patinets in control group (n=75) were treated by extraorgan short wave therapy.

将150例Ⅲa型前列腺炎患者随机分为2组,治疗组75例予体外超短波(每次20 min,每日1次)联合野菊花栓(每次1枚,每晚1次肛门给药)及甲磺酸多沙唑嗪控释片(每次4 mg,每晚1次睡前服)治疗,对照组75例单纯予体外超短波治疗。2组均14日为1个疗程,1个疗程后统计临床疗效和治疗前后慢性前列腺炎症状评分。

Methods 150 patients with prostatitic of ⅲa type were randomly divided into two groups. patients in treatment group (n=75) were treated by combination of extraorgan short wave therapy (once 20 mins/day), wild chrysanthemum suppos.(a piece, once a day, take by anus) and controlled release tablets of doxazosini mesylas (40 mg, once a day).

将150例ⅲa型前列腺炎患者随机分为2组,治疗组75例予体外超短波(每次20 min,每日1次)联合野菊花栓(每次1枚,每晚1次肛门给药)及甲磺酸多沙唑嗪控释片(每次4 mg,每晚1次睡前服)治疗,对照组75例单纯予体外超短波治疗。2组均14日为1个疗程,1个疗程后统计临床疗效和治疗前后慢性前列腺炎症状评分。

Conducting Polyaniline that can be fully soluble in chloroform was prepared by emulsion polymerization and extraction method, doping with different dopants of macro-molecule functional protonic acids.

系统探讨了有机功能质子磺酸对聚苯胺的各种掺杂方法,采用乳液聚合-萃取法制得了在氯仿中完全溶解的导电聚苯胺。

The effect of the toxin on protoplasmic membrane protein was studied by the method of fluorescence, using 8-anilino-1 -naphthalene-sulfonic acid as probe and taking the mesophyll protoplasts from maize leaves as the research system.

以玉米叶片原生质体为研究对象,以ANS(1-苯胺基-8-萘磺酸)作荧光探针,用荧光法研究了Ⅱ-3与质膜蛋白的互作。

Two different fading procedures were studied. One is the oxidation procedure on polyester fibers,the other is the reduction procedure on wool fibers.The study of oxidation procedure mainly focused on 11 disperse azo dyes and 11 disperse anthraquinone dyes. The study of reduction procedure mainly focused on 7 pyrazolone coupled acid azo dyes and 10 azo disperse dyes which has sulfonic group on the couple component.

本论文研究了11支偶氮型分散染料,11支蒽醌型分散染料在聚酯纤维上的分子结构与光牢度的定量关系,同时研究了7支以吡唑啉酮为偶合组份的偶氮型酸性染料和10支偶合组份上带有磺酸基的偶氮型酸性染料在羊毛纤维上的分子结构与光牢度的定量关系。

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